(Centre Sarame inna ne Paper Reference (complete below) [Candiaate Signature No. ae Ree) Examiner's use only 6243.P02 Edexcel GCE jeder ee Chemistry Advanced Subsidiary Unit Test C3b ts) Monday 10 June 2002 — Afternoon 1 Time: | hour 2 3 Materials required for examination Items included with question papery Ni Nu a 5 6 Instructions to Candidates In the boxes above, write your centre number, candidate number, surname and initials, the paper reference and your signature. The paper reference ix shown above. Answer ALL questions in the spaces provided in this book. Calculators may be used. Show all the steps in any calculations and state the units. Information for Candidates ‘The total mark for this paper is 50. The marks for the various questions are shown In round brackets: e.g. (2) All blank pages are indicated. A periodic table is printed on the back cover of this question paper. ‘You are reminded of the importance of clear and orderly presentation in your answers. Total] Turn over N11698 eH Edexcel or Success through qualifications1. The process of reerystallisation is detailed below (a) (b) Step A Add a little solvent to the sample. B__ Dry the product. C__ Allow the solution to cool. D Filter cold. E_ Wash the residue with a small amount of cold solvent. F Warm until the sample dissolves. G Filter whilst the solution is still hot. Put these steps for recrystallisation in the correct order Give the reasons for the words in bold type in Step A. (2) (2) (Total 4 marks) Leave blank a NI169s2. This question is about the tests used for gases. Leave Blank (a) Complete the table below. | Observation expected for a Gas Reagents or test positive result Hydrogen Burning splint Oxygen Glowing splint Carbon dioxide Potassium dichromate(VD) | Solution turns from orange Sulphur dioxide solution acidified with w Sad epee ; Turns red and is then | Moist blue litmus paper bleached white ©) (b) Describe the test you would use to distinguish between ethane, C:Hg, and ethene, CoHy. Give the expected results of the test. | @ (Total 9 marks) Nios 3 Turn over