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concentracion de ppm area (cafeina)

20 364.77
Grafi
40 720.84
60 1120.15 2500
80 1551.8
100 1943.15 2000
f(x) = 19.9386x - 56.174
R² = 0.9990521687
1500
muestra area

area
1000
1 110.91618
2 111.36897 500

0
10 20 30 40

muestra 1: 1 ml en 10 ml 1 ppm=1 mg/l


solución original: 0.0388 g en 50 ml

(8.38 ×10 𝑚𝑙)/(1 𝑚𝑙)=83.8 𝑝𝑝𝑚 =83.8 𝑚𝑔/𝑙


C1V1=C2V2:

83.8 𝑚𝑔/𝑙×0.050 𝑙=4.19 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎


mg de cafeina:

(4.19 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎)/(0.0388 𝑔 )×0.8537 𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=92.2 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎/𝑡𝑎𝑏𝑙𝑒𝑡𝑎


mg de cafeina en tableta

una tableta de cafiaspirina contiene: 65 mg de cafeina

% 𝑒𝑟𝑟𝑜𝑟=(92.2−65)/65×100=41.8%
% de error
Grafica de cafeina
ecuacion:×=(𝑦+56.174)/19.939

muestra
f(x) = 19.9386x - 56.174 1
R² = 0.9990521687
2

muestra 1:

𝑥=(111.36+56.174)/1
muestra 2:
20 30 40 50 60 70 80 90 100 110
concentracion

muestra 2 1 ml en 10 ml
solucion original 0.0390 g en 50 ml

(8.40 ×10 𝑚𝑙)/(1 𝑚𝑙)=84.0 𝑝𝑝𝑚 =84.0 𝑚𝑔/𝑙


C1V1=C2V2:

84.0 𝑚𝑔/𝑙×0.050 𝑙=4. 2𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎


mg de cafeina:

2 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎/𝑡𝑎𝑏𝑙𝑒𝑡𝑎 (4.2 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎)/(0.0390 𝑔 )×0.8537 𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=91.9 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎/𝑡𝑎𝑏


mg de cafeina en tableta

% 𝑒𝑟𝑟𝑟𝑜𝑟=(𝑣𝑎𝑙𝑜𝑟 𝑒𝑥𝑝𝑒𝑟𝑖𝑚𝑒𝑛𝑡𝑎𝑙 −𝑣𝑎𝑙𝑜𝑟 𝑡𝑒𝑜𝑟𝑖𝑐𝑜)/(𝑣𝑎𝑙𝑜𝑟 𝑡𝑒𝑜𝑟𝑖𝑐𝑜 )×100

% 𝑒𝑟𝑟𝑜𝑟=(91.9−65)/65×100=41.3%
% de error
×=(𝑦+56.174)/19.939

concentracion (ppm)
8.38
8.40

𝑥=(110.91+56.174)/19.939=8.38 𝑝𝑝𝑚

𝑥=(111.36+56.174)/19.939=8.38 𝑝𝑝𝑚

𝑚 =84.0 𝑚𝑔/𝑙

𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=91.9 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎/𝑡𝑎𝑏𝑙𝑒𝑡𝑎

100=41.3%
concentracioarea (AAS)
20 179.92 Ácido acetilsal
40 398.09
1400
60 710.14
80 983.19 1200
f(x) = 13.107x - 92.538
100 1198.07 R² = 0.9961656171
1000

800

area
muestra area 600
1 570.25763
400

2 550.59015 200

muestra 1: 1 ml en 10 ml 0
10 20 30 40 50 60
solución origi0.0388 g en 50 ml
concentrac

(50.6 ×10 𝑚𝑙)/(1 𝑚𝑙)=506 𝑝𝑝𝑚 =506 𝑚𝑔/𝑙


C1V1=C2V2:

506 𝑚𝑔/𝑙×0.050 𝑙=25.3 𝑚𝑔 𝐴𝐴�

mg de AAS:

mg de AAS en tableta (25.3 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎)/(0.0388 𝑔 )×0.8537 𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=556 𝑚𝑔 𝐴𝐴�/𝑡𝑎𝑏𝑙𝑒𝑡𝑎

una tableta de cafiaspirina contiene: 650 mg de acido aceltasilicilico


% 𝑒𝑟𝑟𝑜𝑟=(556−650)/650×100=14.5 %

% de error
Ácido acetilsalicilico

f(x) = 13.107x - 92.538


R² = 0.9961656171

20 30 40 50 60 70 80 90 100 110
concentracion

muestra 2 1 ml en 10 ml
solucion original 0.0390 g en 50 ml

(49.1 ×10 𝑚𝑙)/(1 𝑚𝑙)=491 𝑝𝑝𝑚 =491 𝑚𝑔/𝑙


C1V1=C2V2:
𝑙𝑒𝑡𝑎=556 𝑚𝑔 𝐴𝐴�/𝑡𝑎𝑏𝑙𝑒𝑡𝑎

491 𝑚𝑔/𝑙×0.050 𝑙=24.5 𝑚𝑔 𝐴𝐴�


mg de AAS:

(24.5 𝑚𝑔 𝑐𝑎𝑓𝑒𝑖𝑛𝑎)/(0.0388 𝑔 )×0.8537 𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=540 𝑚𝑔 𝐴𝐴�/𝑡𝑎


mg de AAS en tableta

% 𝑒𝑟𝑟𝑟𝑜𝑟=(𝑣𝑎𝑙𝑜𝑟 𝑒𝑥𝑝𝑒𝑟𝑖𝑚𝑒𝑛𝑡𝑎𝑙 −𝑣𝑎𝑙𝑜𝑟 𝑡𝑒𝑜𝑟𝑖𝑐𝑜)/(𝑣𝑎𝑙𝑜𝑟 𝑡𝑒𝑜𝑟𝑖𝑐𝑜 )×100

% 𝑒𝑟𝑟𝑜𝑟=(540−650)/650×100=16.9 %
% de error
×=(𝑌+92.538)/13.107
ecuacion:

muestra concentracion (ppm)


1 50.6
2 49.1

𝑥=(570.25+ 92.538)/13.107=50.6 𝑝𝑝𝑚


muestra 1:

𝑥=(550.59+ 92.538)/13.107=49.1 𝑝𝑝𝑚


muestra 2:

𝑔 𝑡𝑎𝑏𝑙𝑒𝑡𝑎=540 𝑚𝑔 𝐴𝐴�/𝑡𝑎𝑏𝑙𝑒𝑡𝑎