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Application in Orthodontics.
By
1
Synopsis
Introduction
History of stainless steel
Metallurgy
Composition and functions of each ingredient.
Types and grade of stainless steel.
2
Synopsis
General properties of stainless steel.
Sensitization.
Stabilization.
Ductility and malleability.
Soldering and welding.
Strain hardening.
Heat treatment.
Annealing.
Hardening heat treatment
3
Synopsis
Strength Properties
Stiffness
Strength
Stress, Strain, Proportional Limit
Elastic Limit
Yield Point and Yield strength
Plastic deformation
Tensile strength
Fatigue Strength
Impact Strength
Ultimate Tensile Strength
4
Synopsis
Mechanical Properties based on clinical significance
1. Elastic Modulus
2. Resilience
3. Flexibility
4. Poisson’s Ratio
5. Spring back
6. Load deflection Rate
7. Stress Relaxation
8. Working Range
9. Friction
5
Synopsis
Other Properties
Toughness
Modulus of resilience
Brittleness
Bio-host ability
Stainless Steel wires
Ideal requirement of orthodontic wires
Properties of stainless steel orthodontic wires
Variation of properties
6
Synopsis
Australian orthodontic arch wire.
Unique characteristics.
Manufacture, grading and color
coding.
Nomograms
Other Applications
Conclusion.
7
Introduction
Steel is an alloy of Iron and Carbon. Carbon
content should not exceed 0.2% max.
8
History
First developed accidently by Harry Brearley in
Sheffield, England.
Stainless steel entered dentistry in 1919, introduced
at Krupp’s dental poly clinic in Germany by F. Haupt
Meyer.
In 1930 Angle used it to make ligature wires.
By 1937 the value of stainless steel as an orthodontic
wire had been confirmed
Stainless steel today is used to make arch
wires,ligature wires, band material, brackets and
buccal tubes 9
Metallurgy
Crystal imperfections.
10
Composition
In addition to Iron
TYPES CHROMIUM NICKEL CARBON
FERRITIC 11.5-27% 0 0.2% MAX
11
Functions
Chromium:
Increases tarnish and corrosion resistance. A thin
transparent, tough, impervious oxide layer of Chromium
oxide forms on the surface of the alloy when subjected to
room air - “Passivating film effect”
Nickel:
Increases strength
Increases tarnish and corrosion resistance
12
Functions
Cobalt:
Decreases hardness
Manganese:
Scavenger for Sulphur
Increases hardness during quenching
Silicon:
Deoxidizer and scavenger.
Titanium:
Inhibits the precipitation of Chromium carbide.
13
Grades of Stainless Steel
SOFT
HARD
14
Austenitic Stainless Steel
Most corrosion resistant of all types of stainless steel
Formed between 912 – 13940C
AISI 302,304 – Chromium18%, Nickel 8% and Carbon
0.15%(302) 0r 0.08%(304) – 18-8 stainless steel
Austenite is preferred to Ferritic because of greater ductility,
ability to undergo more cold work without fracture.
Increased strength during cold working, ease of welding,
readily overcomes sensitisation, less critical grain growth
and ease of forming FACE CENTERED
CUBIC LATTICE
When austenite is allowed to cool slowly to room
temperature it forms Fe3C and ferrite. The iron carbide
compound is called cementite and the solid solution of
ferrite along with cementite is called pearlite
15
Ferritic Stainless Steel
Stable between room temperature and 912 C.
Carbon has low solubility in this structure.
Interstices in BCC are very small.
AISI 400
Good corrosion resistance at low cost provided increased
strength is not required.
BODY CENTERED
Temperature change does not induce phase change in solid
state CUBIC LATTICE
The alloy is not hardenable by heat treatment.
Not readily work hardenable.
Little application in Dentistry.
16
Martensitic Stainless Steel – Body
centered tetragonal
If austenite is cooled rapidly (Quenched) it will undergo
spontaneous diffusion less transformation to a Body Centered
Tetragonal
The lattice is highly distorted, strained resulting in a hard strong
brittle alloy
Martensite decomposes into ferrite and carbide
Decomposition is accelerated by appropriate heat treatment to
reduce hardness but this is counter balanced by increased
toughness – “Tempering”
AISI 400
17
Properties of Martensite
Increased strength and hardness – used for surgical and
cutting instruments
Yield strength of 492 MPa (annealed). Hardened – 1898
Mpa
Brinell’s hardness range- 230 – 600
Reduced ductility
18
General Properties
SENSITISATION:
When heated between 400 and 900 C 18-8 stainless
steel loses it’s resistance to tarnish and corrosion.
19
General Properties
Stabilization:
Introduction of any element which precipitates
as carbide instead of chromium
20
Soldering
A group of process of fusing two similar or dissimilar
metals by heating them to a suitable temperature
below the solidous of the substrate metals and
applying filler metals having a liquidous not exceeding
4500C that melts and flows by capillary attraction
between the parts without appreciably affecting the
dimension of joined structure
21
Soldering
Flux:
Material used to prevent formation of, or to
dissolve and facilitate removal of oxides,
impurities that may reduce the quality or strength
of the solder metals.
Functions of Flux
Aids in removing the oxide coating so as to
increase the flow.
Dissolves any surface impurities.
22
Flux
Composition:
Borax glass – 55%
Silica – 10%
1:1 concentration
23
Welding
Joining of two or more similar metal pieces by applying heat,
pressure without introduction of an intermediary or a filler
material to produce localized union across the interface thro’
fusion or diffusion
Spot welding is used to join various components in
orthodontics. A heavy current is allowed to pass through a
limited area on the overlapping metals to be welded
The resistance of the material to the flow of current produces
intense localized heating and fusion of metals
The welded area becomes susceptible to corrosion due
Chromium carbide precipitation and loss of passivation
The grain structure is not affected
Increased weld area increases the strength
24
Heat treatment
As a result of cold working the stainless steel
is strain hardened. The method of treatment
to remove the unwanted strain hardening is
heat treatment. The effect of such treatment
depend entirely on temperature
25
Annealing
The effect associated with cold working such as strain
hardening, low ductility and distorted grains can be
reversed by simply heating the metal
The greater the amount of cold working the more
rapidly the effects can be reserved by annealing
Temperature: 399 0 C for 11 minutes. Metal should have
a straw colored appearance on optimum heat treatment.
- Funk
Stages of annealing:
Recovery
Recrystallisation
Grain growth
26
Annealing
Recovery:
Cold work properties begin to disappear.
Slight decrease in tensile strength and no change in ductility.
All the residual stress is relaxed
Recrystallisation:
Old grains disappear totally and are replaced with strain free grains.
Occurs mostly in regions where defects have accumulated.
It attains it’s soft and ductile condition at the end of this stage.
Grain Growth
The Grain size and number of the recrystallised structure depends on the
amount of prior cold working.
On repeated annealing larger grains consume smaller grains. At the end of
annealing the number of grains decrease and size increases.
27
Hardening heat treatment
There is no hardening heat
treatment for austenitic steel due
to it’s stability
It can only be hardened by cold
working.
28
General Properties
Ductility:
Ability of a material to be drawn into wires.
Ability of a material to withstand permanent
deformation under tensile load without
fracture
Malleability:
Ability of metal to be made in sheets
Ability of a metal to withstand permanent
deformation under compressive forces
without fracturing
29
Mechanical Properties
30
Mechanical properties of Stainless Steel
31
Strength Properties
Stress:
Internal distribution of the load
Force per unit area.
Tensile, compressive or shear stress.
Strain:
Internal distortion produced by the load
Deflection per unit length
Proportion of change in dimension to the applied stress.
Elastic strain: Original shape is regained.
Plastic strain: Original shape is not regained.
Elasticity:
Ability of the stressed material to return to it’s original form
Elastic limit:
The greatest stress to which a material can be subjected so that it will return to it’s
original dimension when the forces are released.
Hooke’s law:
Stress is proportional to strain within the proportional limit.
Proportional limit:
Greatest possible stress that can be induced in a material such that stress is directly
proportional to strain.
32
Strength Properties
Modulus of Elasticity: It is the measure of relative stiffness or rigidity of
the material. The mechanical property that determines the load deflection rate
is the modulus of Elasticity 179 GPa
Strength: Capacity of a material to resist a deforming load without exceeding
the limits of plastic deformation. Strength is proportional to the resiliency of the
material
Yield strength: The stress at which increase in strain is disproportionate to
stress. 1579 MPa 0.2% plastic deformation.
Ultimate strength: The strength at which the material fractures. 2117 MPa
Tensile strength – 200 MPa
Resilience: Total energy storage capacity. The amount of energy absorbed by
a structure when it is stressed within it’s proportional limit.
Knoop hardness: 600
33
Stiffness: Force/ distance. It is the measure of resistance to deformation
Property and Uses: British standard
3507:1962
DIAMETER TENSILE APPLICATION
STRENGTH
(tons/in)
0.9 TO 100-120 BOWS AND ARCHES
1.5mm
0.5mm to 120-130 CLASPS, FINGER SPRINGS AND
0.8mm SELF SUPPORTING SPRINGS
0.3 to 130-140 SPRINGS SUPPORTED ON
0.4mm HEAVY ARCHES
0.15 to 140-150 COIL SPRING
0.25mm
0.4 to 160 or more. ARCHES FOR MULTIBAND
0.55mm APPLIANCE
34
Characteristics of Clinical
relevance
Spring back (maximum elastic deflection):
The extent to which the range recovers upon
deactivation of an activated arch wire.
A measure of how far a wire can be deformed
without causing permanent deformation or
exceeding the limits of the material.
Higher the spring back, grater the working range
and lesser are the requirements of frequent
activations.
Stainless steel has a spring back lesser than
Nickel-titanium or beta titanium
35
Characteristics of Clinical
relevance
Resilience:
The capacity of a material to absorb
energy when the material is elastically
deformed
36
Characteristics of Clinical
relevance
Load deflection rate:
For a given load the deflection observed
within the elastic limit
The force magnitude delivered by an
appliance and is proportional to the modulus
of elasticity
Low load deflection rate provides ability to
apply low forces, a more constant force over
time while deactivation, greater ease and
accuracy in applying a given force
37
Working range and Flexibility
The distance a wire will bend elastically
before permanent deformation occurs
D x PL3 / T4
38
39
Formability
40
Stress relaxation
When a wire has been deformed
and held in a fixed position the stress may
diminish with time even though the total
strain may remain constant.
41
Other Properties
Toughness: The amount of elastic and plastic
deformation energy required to fracture. It is the
measure of resistance to fracture
43
Properties of Stainless steel
arch wires:
High stiffness.
Low resiliency.
Moderate spring back.
Moderate range of action.
Low friction.
Good formability.
Biocompatible.
Good joinability.
Less springy.
44
Variation of properties of
Stainless Steel wires
Variation in diameter
The force that can be developed in a given length of wire increases 16
increase by 8 times.
Range decreases as the diameter is doubled.
Variation in Length
The force that can be developed decreases 1/8
th when the length of
increases 4 times.
Modification in arch wire – Multistranded arch wires:
Low load deflection rate.
45
Variation of properties of
Stainless Steel wires
Cold working:
Increased hardness.
Reduced ductility.
Increased yield strength.
Increased modulus of elasticity.
Annealing.
46
Australian Orthodontic arch wires
47
Unique characteristic of A J
Wilcock wire different from usual
stainless steel wire
Ultra high tensile austenitic stainless steel arch wire
The wire is resilient – certain bends when
incorporated into the arch form and pin to the teeth
become activated by which stress are produced within
the wire which generates the force.
The stress relaxation of Wilcock wire are significantly
lesser than Elgiloy wires.
48
Australian Orthodontic arch
wires
Types:
Regular
Regular plus
Special
Special plus
Extra special plus
Supreme
Premium plus
49
Regular Grade – white Label
Lowest grade and easiest to bend
Used for practice bending and forming axillaries
52
NOMOGRAM
Nomograms are fixed charts which display the
mathematical functions, provided each scales is
adjusted in space appropriately with normal range
from one
when constructed properly the relationship
between the parameters will be given in a straight
line
In other words the extended the line between the
two will yield the third
Strength = stiffness x range
53
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Conclusion
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