PROSEDUR KERJA PENGUJIAN

KADAR NITROGEN DI
LABORATORIUM PT. HOK TONG
JAMBI ( SCL )

NITROGEN TEST
PROCEDURE FOR
LABORATORY
PT. HOK TONG JAMBI( SCL )

1
PENYERAGAMAN CONTOH UJI
( SAMPLE HOMOGENIZATION )

LAKUKAN PENYERAGAMAN
MENGGUNAKAN LAB MILL (
Homogenization using a Lab Mill )

Giling 5 kali secara vertikal (Milling

done five times in a Vertical
manner)

Giling 1 kali secara horizontal

(Milling done one time in a
Horizontal manner)

Setelah dilakukan penyeragaman ,

Contoh uji dipotong seberat 5-10
gram . (After Homogenization , the
sample is cut with a weight of 5-10
grams )

2
Timbang dengan teliti kira –
kira 0,1 gram contoh yang telah
diseragamkan. Weight with
accuracy 0,1 gr sample has
been uniforming

Sample yang sudah ditimbang

dimasukkan ke dalam labu
mikro kjedahl. (The sample has
weight then enter into micro
kjedhal squesh’s)

3
Timbang kira – kira 0,65
gram campuran katalis.
(Weight 0,65 gram mixture of
catalyst)

Masukkan
Masukkankataliskataliskedalam
kedalam
labu
labumikro
mikrokjedahl
kjedahlyang
yang
berisi
berisisample
sample. Enter
. Entercatalyst
into
catalyst
micro into microsquash’s
kjedahl kjedahl
squash’s
has has filled sample)
filled sample)

4
Ambil 3 – 5 ml asam sulfat
pekat . (Take 3 – 5 ml
sulfuric acid)

Kemudian masukkan asam

sulfat kedalam labu mikro
kjedahl yang berisi sample
dan katalis. (Then Enter
sulfuric acid into micro
kjedahl squash has been
filling sample and catalyst)

5
 Kemudian bakar diatas heating
mantle . then Burn it on heating
mantle)

Tutup jendela lemari asam sampai

labu mikro kjedahl didalam heating
mantle tidak bewarna . Closed acid
chamber until micro squash kjedahl
on heating mantle green colour or
color less)

6
Apabila tidak bewarna,
angkat labu mkiro kjedahl
kemudian dinginkan. (If it
less colour, Take micro
kjedahl squash then cool it)

Masukkan contoh ke dalam

Alat Markham still . ( Put the
Sample in to Markham Still )

7
Masukkan Larutan Natrium
Hidroksida sebanyak 10 ml.
( Put Liquid of Natrium
Hidrokcid 10 ml )

Kemudian bilas dengan air

suling kira-kira 5 ml. ( Then
wash by clean water about 5
ml )

8
Tunggu kira-kira 5 menit,
Saat itulah destilasi keluar. (
Wait about 5 minutes , at the
time Destilation out )

Titrasi dengan Larutan 0,01 N,

sampai berubah warna dari
hijau menjadi ungu . ( Titration
by Solution of 0,01 N, until the
colour change from green to
Violet )

9
Setelah warna berubah catat
nilai hasil titrasi , kemudian
hitung kadar Nitrogen. ( After
the colour change record the
value of Titration , then count by
Solution of 0,01 N, until the
colour change from green to
Violet )

Count the Nitrogen Test using Formula :

N : ( V1 – V2 ) N x 0.0140
------------------------------- x 100 %
W

V1 = ml H2SO4 untuk Titrasi Larutan berisi contoh

V2 = ml H2SO4 untuk Titrasi Larutan Blanko
N = Normalitas H2SO4
W = Bobot contoh ( gram )

10
 Cara pembuatan Bahan
Hasil Analisa ( Test
Kimia . ( The method of
Result )
calculation 0,01 N )

11