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UNIT-IV
FILTRATION
Filtrationis the removal of solid particles
from a fluid , by passing the fluid through a
filtering medium or septum on which the
solids are deposited.
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Should retain the solids giving a clear filtrate
Should not plug or blind
Should be mechanically strong
Should be corrosion resistant
Should be able to discharge cake easily ans
cleanly
Should be cheap, long life, offer little
resistance to filtrate
Materials used:
Canvas cloth, woollen cloth, metal cloth, nylon
(alkaline), PP(acidic).
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Filter aid is added to increase the porosity of
the cake and to permit the liquor at a
reasonable rate.
Diatomaceous silica, perlite, purified wood
cellulose are commonly used filter aids.
Methods of using filter aids
Adding a filter aid to the slurry before
filtration
Precoating ,i.e. by depositing a layer of filter
aid on the filter medium before filtration.
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Based on nature of filtration
Filters
Feed of suspension
flows under
Remove large Remove small
pressure at fairly
amount of solid amounts of solids
high velocity across
the filter medium
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Dead end Filtration Cross flow Filtration
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Based on application of external force:
Filters
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Feed in
Plates and frames are arranged alternately and Plate
supported on a pair of rails.
Plate - solid with ribbed surface; 6 to 50 mm thick
Frame - hollow; provides space for cake accumulation;
6 to 200 mm thick
Chambers are formed due to alternate arrangement of
plates and frames
Shape: square/ rectangle Filtrate
Material: cast iron, stainless steel, nickel, aluminium,
plastics
Cake
Filter cloths over both sides of each plate
Circular holes on corners of plates, frames, and filter
cloth for feed and discharge
Press is closed using a hand screw or hydraulically; A
continuous channel is formed along the whole length of
press
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Plate and frame Cake formation
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Slurry is pumped into The thickness of the
the feed channel and The solid forms a filter cake is half of the frame
passes through the filter cake and remain in the thickness, because on
medium on the surface frame each side of frame
of the plate filtration occurs
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When washing of cake is also required modified plate and
frame filter is used.
For this purpose an additional channel is included called as
washing plate and are identified by 3 dots.
The sequence of arrangement of plates and frames can be
represented by dots as 1.2.3.2.1.2.3.2.1 so on (between 1
and 1, 2.3.2 must be arranged.
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• Filtration proceeds in the ordinary way until the frames are filled with cake.
Step 1
• To wash the filter cake, the outlets of washing plates are closed.
Step 2
• Water passes through the filter cloth and enters frame which contains the
cake.
Step 4 • Then water washes the cake, passes through the filter cloth and enters the
plate down the surface.
Step 5 • Finally washed water escapes through the outlet of that plate.
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Water wash is efficient only if the frames are full with
filter cake.
If the solid do not fill the frame completely, the wash
water causes the cake to break (on the washing plate side
of the frame), then washing will be less effective.
This helps not only in emptying the frames but also helps
in washing the cake correctly.
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Simple construction
Low capital cost and maintenance cost
Large filter area per unit area of floor space
High operating pressures are easily developed
Capacity can be altered
Majority of joints are external, so easy detection of leakage
Construction:
The leaf filter consists of a frame enclosing a drainage screen or
grooved plate.
The frame may be any shape circular, square or rectangular.
The whole unit is covered with filter cloth.
The outlet for the filtrate connects to the inside of the frame through
suction.
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Working:
Use:
Used for the filtration of slurry which do not contain high
solid content, about 5%, i.e. dilute suspensions.
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Simplest form of filter used for batch process.
A number of units can be connected in parallel to increase
the surface area of filtration.
High pressure filtration - Pressure difference can be
obtained either with vacuum or using pressure up to the
order of 800 kilopascals.
Labour costs for operating the filter leaf are fairly
moderate.
The efficiency of washing is high.
The slurry can be filtered from any vessel.
The cake can be washed simply by immersing the filter in a
vessel of water.
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Principle:
Slurry filtered through sieve like mechanism on the rotating
drum surface, under vacuum.
Filtration, washing, air drying of cake and cake discharge (using
knife) all in one cycle.
Construction:
It consists of a metal cylinder mounted horizontally.
The outer drum may be up to 3 meters in diameter and 3.5
meters in length and gives surface area of 20 m2
The curved surface being a perforated plate, supports a filter
cloth.
A second inner solid drum
Radial partitions between drums divide the annular space into
compartments; connected to a hole in the rotating valve
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The drum is dipped into the slurry and vacuum applied to
the rotary valve, which is connected to the filtrate
receiver.
A layer of solids builds on the face of outer drum as the
liquid is drawn through the cloth into the compartment,
internal pipe, valve, and collecting tank
When the cake has formed, the cake is drained or partially
dried by vacuum.
The drum is sprayed with water to wash the cake.
Retaining the vacuum connection drains the cake and
produces partial dryness then, removed by a doctor knife.
Little air is blown to belly out the cloth; cake cracks away
from the cloth; now, knife does not scrape the drum face
After cake is dislodged, cycle is repeated - continuous
operation
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Less labour requirement
Large capacity
Changing speed to get cake of varying thickness
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Working
Slurry is fed centrally to a rotating basket
Liquor passes the filter medium and solids are retained by the
medium
After cake build up, feed is stopped, cake of solids are spun
for a short time to remove residual liquid from cake
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Principle:
Uses centrifugal force to separate
1) solids from liquids
2) immiscible liquids of different densites
Construction:
1) Basket with perforated sides
Diameter: 750 to 1200 mm; Depth: 450 to 750 mm; Speed:
600 to 1800 rpm
2) Basket is held at lower end by a vertical shaft
3) Shaft driven by motor
4) Perforated walls of basket covered with filter cloth
5) Casing with filtrate discharge connection at bottom
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Working:
Slurry fed is forced against basket sides
Liquid passes through filter medium and into casing,
discharge pipe
Solids form a cake against filter medium
Cake is washed by spraying was liquid to remove soluble
material
Cake spun at high speeds
Cake is discharged by cutting with unloader knife
Knife peels off cake and discharges through bottom
opening
Rinse filter medium and repeat
Uses:
Sugar refining
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ROTARY DRUM FILTER
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ROTARY DRUM FILTER
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