PACKAGE C

SPEAKERS

M UHAM M AD HANIFATIN PUTRI

BADRUL AZIZAH ANGGRAENI R.
UYUN
 Recrystallization
Tools
1. Erlenmeyer flask 125 ml 1 piece
2. Stirrer 1 piece
3. Buchner funnel 1 piece
4. Pipettes 3 piece
5. Electrical stove 1 piece
6. Thermometer 1 piece
Recrystallization
Materials
1. Salicylic acid 3,5 gram
2. Aquades enough
3. Norit 1-2%
4. Acetic acids anhydrous 3,75 gram
5. Sulfuric acid concentrate 3 drops
6. Ethanol 96% 7,5 ml
7. FeCl3
Recrystallization

Measure 1 gram of salicylic

acid + 5 mL Aquades

- Included into erlenmeyer flask 125 mL

- Heated on the spirtus burner until boil
at the same time shaken
- Added aquades until the crystal
dissolve
- Calculate the required volume of
aquades
Mix solution

- Filtered in a hot state with buchner funnel

Filtrate Residue
Recrystallization

Filtrate

- Cooled until crystall

formed
- Filtered again with
buncher funnel
White Crystal

- Dried on the desicator

- Measure the mass
- Compared the melting point
with first substance

Result
Synthesis of
Measure 2,5
Aspirin
gram of salicylic
acid
- Put into erlenmeyer flask 125 mL
- Added 3,75 gram of acetic acid
anhydride
- Added 3 drops of concentrated
H2SO4
- Stirred until homogeneous
- Prepared the electrical stove
- Heated above the bath 50o - 60oC
while stirring sometimes
- Cooled residue added 37,5 mL of
aquades and stirring
- Filtered precipitated with a Buchner
funnel when the solution still warm

Filtrate Residue
Synthesis of Aspirin

Aspirin Crystal

- Added 7,5 mL of ethanol 96% + 25 mL of

aquades
- Heated until homogen
- Filtered with a Buchner funnel when the
solution still warm
- Recrystallized
- Dried minimal 3 days
- Determined mass and melting
point of aspirin
- Tested purity with FeCl3

Result
GINGER OIL INSULATION
TOOLS

1. 1 set of Extraction soxhlet

2. Evaporatore 1 piece
3. Mortar 1 piece
4. Separating funnel 1 piece
5. Beaker glass 1 piece
6. Refractometer 1 piece
7. Burner spirtus 1 piece
8. Filter paper 2 pieces
MATERIALS

1. Sodium sulphate anhydrous

2. Dried Ginger 50 grams
3. Petroleum ether ±100 ml
GINGER OIL INSULATION
Old enough
Ginger
- Cleaned
- Dried
- Grinded into a smooth powder

Ginger Powder

- Weighed 30-50 gram ginger powder

- Wrapped with filter paper that has been
on the top and bottom ropes
- Put into extraction soxhlet
- Added petroleum ether ± 100 mL into
extractor flask
- do extraction until extraction result is
colorless
Colorless
extraction
 Colorless
extraction
- Waited until the soulution fell into extraction flask
- Opened the soxhlet and taken the sample
- Closed as before
- Evaporated the solvent into extraction flask
- Keep the solvent volume

Filtrate Residue
- Added anhydous Na2SO4
- Filtered using filter paper

Filtrate Residue
 Filtrate

- weighed - measured

Mass Index bias

rendemen of
ginger oil

Determine the mass of water

Ginger powder 1
gram
- Heated at 100°C and measuring
again
- Note the weigh repeat again until
weigh constan

Mass of water’s ginger

THANK YOU
H A V E A NICE DAY!