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Composition of Unknown
Nanomaterial
Group members:
Haris Irfan (29)
Saba Sohail (19)
Siddiqa Batool (09)
Hamza Ashfaq (39)
1
Contents:
• Introduction
• Equipment Used
• Results and Discussions
• Applications
• Conclusions
• References
2
Introduction:
• Nano materials is the most renowned field of science
nowadays and on which daily advancements are being
made. It helps us in textiles, electronics, food & health etc.
• Nanomaterials hold potential to make supercomputers that
are small enough to be carried in a shirt pocket or machines
that can repair damaged tissues by travelling through the
human body
• The unique properties of nanoparticles arise from their size
reduction.
3
Equipment Used:
• Energy Dispersive Spectroscopy (EDS):
MIRA 3 TESCAN Scanning Electron Microscope was used
for EDS elemental analysis.
It depends on the investigation of a sample through
interactions between light and matter, analyzing X-rays in
its case.
Determination of composition
4
Contd..
5
Contd..
6
Results and Discussions:
1. Results obtained from Energy Dispersive Spectroscopy
2. Results obtained from Scanning Electron Microscope
3. Results obtained form X-ray Diffraction
7
1. Energy Dispersive Spectroscopy
8
2. Scanning Electron Microscopy
9
Comparison with Literature:
Figure 1. Figure 2.
SEM image at 5µm SEM image at µm obtained form
Literature [13]
• The size of our sample is approximately 4-6µm where the SEM image of
literature comes out to be 4.5µm. This also proves our sample to be graphene
nanosheets [13]. 10
3. X-Ray Diffraction:
11
Comparison with Literature:
13
Contd..
14
Conclusions:
• The sample given to us was Graphene nanosheets.
• The sample in the form of sheets as observed from SEM and
compared with literature.
• We predict the size of Graphene nanosheet to be almost
6µm.
• The sample has shown crystallinity and this was observed
from XRD. The XRD and literature both show peak of 002
and 100.
15
References:
• [1] “Nanomaterials,” Wikipedia. 13-Nov-2017.
• [2] “History and Development of Nanomaterials.” [Online]. Available:
https://www.azonano.com/article.aspx?ArticleID=3393. [Accessed:
20-Nov-2017].
• [3] Dongguang Wei, Rajesh Dave and Robert Pfeffer, “Mixing and
characterization of nanosized powders: An assessment of different
techniques,” Kluwer Acad. Publ., pp. 21–42, Nov. 2001.
• [4] “MIRA3.” TESCAN.
• [5] “GNR Explorer.” Analytical Instrument Group.
• [6] Richa Srivastava, “Synthesis and Characterization Techniques of
Nanomaterials,” Taylor Francis Group, pp. 17–27, Mar. 2012.
• [7] “Energy-dispersive X-ray spectroscopy,” Wikipedia. 27-Aug-2017.
• [8] “How an SEM works.” [Online]. Available:
http://www.nanoscience.com/technology/sem-technology/how-
sem-works/. [Accessed: 20-Nov-2017].
• [9] “X-ray Powder Diffraction (XRD),” Techniques. [Online]. Available:
https://serc.carleton.edu/research_education/geochemsheets/techni
ques/XRD.html. [Accessed: 20-Nov-2017].
16
References:
• [10] “jp-2012-03121n_0001.gif (GIF Image, 500 × 246 pixels).”
[Online].
Available:http://pubs.acs.org/appl/literatum/publisher/achs/journals
/co ntent/jpccck/2012/jpccck.2012. 116.issue
23/jp303121n/production/images/medium/jp-2012-
03121n_0001.gif. [Accessed: 20-Nov-2017].
• [11] Sunil Meti , Udaya Bhat K. , Rahman M. R. , Jayalakshmi M.,
“Photocatalytic Behaviour of Nanocomposites of Sputtered Titanium
Oxide Film on Graphene Oxide Nanosheets,” Sci. Acad. Publ., pp. 12–
18, 2015.
• [12] “SEM Lab,” Institute of Space Technology, Ismlamabad.
• [13] Alireza Ashori, “Effects of Graphene on the Behavior of Chitosan
and Starch Nanocomposite Films,” Wiley Online Libr.
Impact Factor = 1.449
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“Large-scale production of high-quality graphene using glucose and
ferric chloride,” R. Soc. Chemsitry, 2014.
Impact Factor = 8.668
17
References:
• [15] P.Noorunnisa Khanam, Anton Popelka, Maryam Alejji, and
M.A.Al Maadeed, “Biotechnological Production Process and Life Cycle
Assessment of Graphene,” Hindawi, vol. Volume 2017, pp. 1–10, Dec.
2017.
Impact Factor = 1.871
• [16] Guoxiu Wang,* Juan Yang, Jinsoo Park, Xinglong Gou, Bei Wang,
Hao Liu, and Jane Yao, “Facile Synthesis and Characterization of
Graphene Nanosheets,” J. Phys. Chem. C, vol. 112,no. 22, pp. 8192–
8195, 2008.
Impact Factor = 4.536
• [17] “XRD lab.”
• [18] “Graphene,” Wikipedia. 16-Nov-2017.
• [19] M.-G. Kim, J. Y. Park, Y. Shon, and G. S. and Y.-K. Oh,
“Pharmaceutical Applications of Graphene-based Nanosheets,”
Current Pharmaceutical Biotechnology, 31-Oct-2013. [Online].
Available: http://www.eurekaselect.com/119665/article. [Accessed:
20-Nov2017].
Impact Factor =1.61
18
References:
• [20] M. Zhong et al., “Interface coupling in graphene/fluorographene heterostructure
for highperformance graphene/silicon solar cells,” Nano Energy, vol.28, noSupplement
C, pp. 12– 18, Oct. 2016.
Impact Factor = 12.343
• [21] “Could hemp nanosheets topple graphene for making the ideal supercapacitor?,”
American Chemical Society. [Online]. Available:
https://www.acs.org/content/acs/en/pressroom/newsreleases/2014/august/could-
hempnanosheets-topple-graphene-for-making-the-ideal-supercapacitor.html.
[Accessed: 20-Nov2017].
• [22] Marappan Sathish*, Satoshi Mitani, Takaaki Tomai, and Itaru Honma*, “Ultrathin
SnS2 Nanoparticles on Graphene Nanosheets: Synthesis, Characterization, and Li-Ion
Storage Applications,” ACS Publ., vol. 116, no. 23, pp. 12475–12481, 2012.
Impact Factor = 4.530
• [23] M. Zeng et al., “Aqueous Exfoliation of Graphite into Graphene Assisted by
Sulfonyl Graphene Quantum Dots for Photonic Crystal Applications,” ACS Appl. Mater.
Interfaces, vol. 9, no. 36, pp. 30797–30804, Sep. 2017.
Impact Factor = 7.504
• [24] M. Q. Israr et al., “Structural Characterization and Biocompatible Applications of
Graphene Nanosheets for Miniaturization of Potentiometric Cholesterol Biosensor,” J.
Biosens. Bioelectron., vol. 2, no. 3, Nov. 2011.
Impact Factor = 7.47 19