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Mettler-Toledo
Conductivity Calibration Training
Victor M. Braga
Mettler-Toledo Thornton, Inc.
Bedford, MA 01730 USA
www.thorntoninc.com
Topics
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
THORNTON
Leading Pure Water
Analytics
Definition of Calibration
THORNTON
National Standards
ASTM
American Society for
Testing and Materials
NIST
National Institute of Standards
and Technology
THORNTON
Leading Pure Water
Analytics
What Is ASTM
What Is NIST
THORNTON
Leading Pure Water
Analytics
Established in 1901 to strengthen the U.S. economy and improve the quality
of life by working with industry to develop and apply technology,
measurements, and standards.
THORNTON
Leading Pure Water
Analytics
Calibration Traceability
Sensors
-
Cell Constant Traceable to American Society for Testing and Materials (ASTM)
and Ultrapure Water at 15, 25 and 40 C
Temperature - Traceable to National Institutes of Standards (NIST)
Instrument Calibration
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
THORNTON
Leading Pure Water
Analytics
Auto Range
Range Manually Selected
THORNTON
Leading Pure Water
Analytics
Instrument Calibration
10
Traceability
THORNTON
Leading Pure Water
Analytics
NIST
Cal Labs
Multi-Meters
Manufacturers
Calibrators (Decade Box)
Process Instrument
11
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
12
Cell Constants
THORNTON
Leading Pure Water
Analytics
1cm
0.1cm
1cm
0.1 constant
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THORNTON
Leading Pure Water
Analytics
ASTM D1125
Primary Standard
and Pure Water
at 15, 25, 40C
Standards Lab
Cell Constant
14
Production Cell
Constant
THORNTON
Leading Pure Water
Analytics
Standard D1125
Conductivity @ 25 C
111,342* S/cm (8.98 -cm)
12,856* S/cm (77.78 -cm)
1,408.8* S/cm (709.82 -cm)
146.93* S/cm (6,805.96 -cm)
*Plus conductivity of water used
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Fundamental Standard
THORNTON
Leading Pure Water
Analytics
100
18.18 M-cm
0.055 S/cm
31.87 M-cm
0.031 S/cm
80
8.85 M-cm
0.113 S/cm
60
40
20
0
0
10
20
30
40
50
60
70
Temperature (Deg C)
16
80
90
100
THORNTON
Leading Pure Water
Analytics
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Traceability
THORNTON
Leading Pure Water
Analytics
NIST
ASTM
(Ultrapure Water)
Manufacture's
Standard
Product
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Calibration Options
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
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THORNTON
Leading Pure Water
Analytics
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THORNTON
Leading Pure Water
Analytics
Nearly 20%
difference!!!
Standard
Solution
21
THORNTON
Leading Pure Water
Analytics
Reasons for the difference between the Standard and what the meter
displays
22
THORNTON
Leading Pure Water
Analytics
23
THORNTON
Leading Pure Water
Analytics
Reasons for the difference between the Standard and what the meter
displays
24
Field Calibration
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
25
Verify/Calibrate
THORNTON
Leading Pure Water
Analytics
26
Portable Cond./Res
Calibration Kit
THORNTON
Leading Pure Water
Analytics
Calibration Sequence
Portable Cond./Res
Calibration Kit
27
Data Collections
THORNTON
Leading Pure Water
Analytics
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Verify/Calibrate
THORNTON
Leading Pure Water
Analytics
A STD Re 1.
000 M-cM
B STD Tp
26.3 C
C UUT Re 1.
000 M-cM
D UUT Tp
26.3 C
29
THORNTON
Leading Pure Water
Analytics
Calibration Steps
Calibrate Uncompensated/Compensate
30
THORNTON
Leading Pure Water
Analytics
Compensation Algorithm
Temperature
Compensation
Algorithm
Uncompensated
Resistance
31
Compensated
Compensated
Readings
Readings
THORNTON
Leading Pure Water
Analytics
Uncompensated Mode
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THORNTON
Leading Pure Water
Analytics
n Inc,
o
t
n
r
s
Tho
ertifie
c
y
b
e
Her
e
that th g
in
follow ent/sensor
m
Instru
w ithin
s
m
r
o
perf
ns
ficatio
i
c
e
p
s
33
Specialized Calibration
THORNTON
Leading Pure Water
Analytics
Instrument Traceability
Sensor Traceability
Instrument Calibration
Sensor Calibration
Calibration options
Field Calibration
Specialized Calibrations
Field Calibration Demo
34
THORNTON
Leading Pure Water
Analytics
35
THORNTON
Leading Pure Water
Analytics
36
THORNTON
Leading Pure Water
Analytics
S/cm
1,000
100
10
0.01 S/cm
USP waters
Solution C
Solution D
37
25C
UPW
THORNTON
Leading Pure Water
Analytics
38
THORNTON
Leading Pure Water
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System Calibration
39
THORNTON
Leading Pure Water
Analytics
Thank You
Victor M. Braga
Mettler-Toledo Thornton, Inc.
40