Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
Needed Accessories
For simple Troubleshooting:
nothing
Flowmeter (optional)
P/N: 630-08646-51
Dilution Water
(HCL)
ASI-V
0-Port
2
1
NDIR-Detector
8-Port-Valve
7
8
Drain
TC-Port
Filter
5mL-Syringe
SpargeGas
IC-Port
Cooling Loop
CO2Absorber
Pump
HalogenScrubber
~ 80mL
Pressure
Regulator
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
Filter
5mL-Syringe
150mL
IC-Port
Cooling Loop
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
Filter
5mL-Syringe
cell
space purge
650mL
IC-Port
Cooling Loop
NOXAbsorber
Pump
HalogenScrubber
TNM-1
Pressure
Regulator
150mL
Dehumidifier
Humidifier
Carrier Gas
to cell space
purge
BlankCheck
Vessel
Phosphoric
Acid
O3Deact.
Drain
Vessel
O3-Gen.
150mL
CLM
Det.
500mL
no
Peaks
6 8-Port-Ventil
ASI-V
Baseline 2(in test7 mode) much too high
1
0-Port
8
Peaks much too
low
TC-Port
Flowmeter show normal flow rate
5 mL-Spritze
1. Step:
Snap of/bent inlet(L) tube from CO2Absorber
Watch Drain-Vessel (at the same time
check water level)
Result:
(a) Water level o.k., but no air bubbles to see
Druckregler
big leakage in System
Befeuchter
(b) Water level o.k., air bubbles
to see
possible little leakage in System
Trgergas
BlankCheck
NDIR-Detector
Filter
IC-Port
CO2Absorber
HalogenScrubber
Dehumidifier
Phosphoric
Acid
Drain
Vessel
NDIR-Detector
Filter
IC-Port
CO2Absorber
HalogenScrubber
Druckregler
Dehumidifier
Befeuchter
Trgergas
BlankCheck
Phosphoric
Acid
Drain
Vessel
NDIR-Detector
0-Port
8
3. Step:
TC-Port
Remove upper end connection of
Halogen-Scrubber
5 mL-Spritze
Shut opening at Halogen-Scrubber
Watch Drain-Vessel
Filter
IC-Port
Result:
(a) No air bubbles in Drain-Vessel
big leakage in flow line before HalogenScrubber
(b) Air bubbles in Drain-Vessel to see
Druckregler
leakage in flow line behind HalogenScrubber
Befeuchter
Trgergas
BlankCheck
CO2Absorber
HalogenScrubber
Dehumidifier
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
Filter
5mL-Syringe
IC-Port
Cooling Loop
150mL
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Humidifier
Carrier Gas
Dehumidifier
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
TC-Port
5
6
NDIR-Detektor
8-Port-Valve
TC-Port
Drain
5mL-Syringe
O-Ring, Teflon (036-11408)
IC-Port
O-Ring, Viton 4DP10A (036-11209)
Khlschleife
CO2Absorber
Absorber
SchlauchSchlauchpumpe
pumpe
Pressure
Regulator
150mL
Humidifier
Carrier Gas
HalogenHalogenScrubber
Scrubber
BlankBlankCheck
Check
Gef
PhosphorPhosphorsure
sure
DrainDrainGef
Dilution Water
(HCL)
ASI-V
0-Port
5
6
8-Port-Valve
Combustion Tube
TC-Port
Drain
Filter
Filter
Nut screw
5mL-Syringe
Khlschleife
Khlschleife
IC-Port
Teflon-Sealing
(035-62994-03)
CO2Absorber
Absorber
SchlauchSchlauchpumpe
pumpe
HalogenHalogenT-Piece (638-40152)
Scrubber
Scrubber
Pressure
Regulator
150mL
Entfeuchter
feuchter
Humidifier
Carrier Gas
BlankBlankCheck
Check
Gef
PhosphorPhosphorsure
sure
Cooling Loop
(638-41314)
Teflon-Sealing for
connection of Loop
(035-62972-05)
DrainDrain-
Gef
Dilution Water
(HCL)
ASI-V
0-Port
5
6
8-Port-Valve
Drain
TC-Port
5mL-Syringe
Cooling Loop
Pump
Pressure
Regulator
150mL
Humidifier
Carrier Gas
BlankCheck
Vessel
Acid
Gef
Verdnnungswasser
NDIR-Detector
Drain
Filter
150mL
Khlschleife
upper connector Halogen-Scrubber
connections Filter
Schlauchconnections measurement cell
Consumable:
Druckregler
Halogen-Scrubber (630-00992)
Membrane Filter (046-00044-12)
Befeuchter
CO2-Absorber (630-00999)
Trgergas
IC-Port
CO2Absorber
pumpe
HalogenScrubber
Dehumidifier
BlankCheck
Gef
Drain
Vessel
Verdnnungswasser
Structure:
ASI-V
0-Port
NDIR-Detector
5
6
Chopper
/ 7
2
Light
1 Source
8
8-Port-Ventil
Short Cell
5 mL-Spritze
Short Cell inlet
Drain
TC-Port
150mL
Filter
Detector
Khlschleife
IC-Port
CO2Absorber
Motor
Schlauchpumpe
Micro Flow
HalogenScrubber
Sensor
to L of CO2 Absorber
from Short Cell outlet
Druckregler
Entfeuchter
Due to slightly
increased position
of real baseline, there
is nothing to see in
view 20mV.
Baseline adjusted
to approximately 5mV
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
Filter
5mL-Syringe
150mL
IC-Port
Cooling Loop
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
TC-Port
View : 1000mV
Filter
5mL-Syringe
IC-Port
Khlschleife
CO2Absorber
Schlauchpumpe
Pressure
Regulator
HalogenScrubber
150mL
Entfeuchter
Befeuchter
Carrier Gas
150mL
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
5mL-Syringe
Realisation:
Connect outlet
Drain of carrier gas
Flowmeter directly to inlet of
measurement cell.
Filter
150mL
IC-Port
Cooling Loop
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
TC-Port
View: 20mV
5mL-Syringe
Filter
150mL
Khlschleife
CO2Absorber
Schlauchpumpe
Pressure
Regulator
150mL
Carrier Gas
Befeuchter
1. Baseline
normal
2. Air Peak from changing
tube connections
Dilution Water
(HCL)
3
ASI-V
2
1
0-Port
NDIR-Detector
8-Port-Valve
7
8
TC-Port
Drain
Filter
5mL-Syringe
~ 230mL
Cooling Loop
CO2Absorber
~ 80mL
HalogenScrubber
~ 150mL
Pressure
Regulator
Dehumidifier
~ 130mL
Humidifier
Carrier Gas
Mist
Trap
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
5mL-Syringe
Filter
150mL
TC/NPOC
Measurement
IC-Port
Cooling Loop
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
ASI-V
0-Port
8-Port-Valve
bad recovery for repeated injections of one sample
Drain
possible
leakage at 8-Port-Valve or Syringe
TC-Port
Filter
5mL-Syringe
TC/NPOC
Messung
Nut Screw
IC-Port
Cooling Loop
Schlauchpumpe
HalogenScrubber
8-Port-Valve complete,
inclusive Rotor (638-56135)
21 87
Pressure
Regulator
150mL
Entfeuchter
5mL-Syringe
Humidifier
Carrier Gas
NDIR-Detektor
BlankCheck
Gef
Phosphorsure
DrainGef
(638-59213)
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detektor
8-Port-Valve
TC-Port
5mL-Syringe
DrainUse
TC/NPOC
Messung
2-3 cuts
Cooling Loop
Schlauchpumpe
Pressure
Regulator
HalogenScrubber
150mL
Plunger
new Tip
feuchter
Humidifier
Carrier Gas
BlankCheck
Gef
DrainGef
O-Rings
Dilution Water
(HCL)
ASI-V
0-Port
8-Port-Valve
e.g. appearance of double Peaks
NDIR-Detektor
TC-Port
5mL-Syringe
Drain
Filter
TC/NPOC
Messung
Cooling Loop
IC-Port
CO2Absorber
Schlauchpumpe
Pressure
Regulator
HalogenScrubber
150mL
Entfeuchter
Humidifier
Carrier Gas
BlankOK
Check
Gef
not OK
(side Injection) DrainPhosphorsure
Gef
not OK
(liquid sprays)
(HCL)
ASI-V
0-Port
Exchange of Catalyst:
5
6
8-Port-Valve
e.g. decreasing sensitivity
TC-Port
5mL-Syringe
Drain
ca. 100 mm
TC/NPOC
Messung
TC-CombustionFilter
Tube
(631-41524SE)
IC-Port
Quartz Wool
(630-00557)
Schlauchpumpe
2 Platinum Sheet
(630-00105-01)
150mL
CO2Absorber
HalogenScrubber
Entfeuchter
Humidifier
Carrier Gas
ca. 5 mm
Cooling Loop
Pressure
Regulator
NDIR-Detektor
ca. 130 mm
Acid
BlankNormal Sense
Check
Gef Catalyst Phosphorsure
(638-60116)
High Sense
Drain- Catalyst
Gef(630-00996)
Dilution Water
(HCL)
ASI-V
0-Port
NDIR-Detector
5
6
8-Port-Valve
Drain
TC-Port
5mL-Syringe
Filter
150mL
IC
Measurement
IC-Port
Cooling Loop
CO2Absorber
Pump
Pressure
Regulator
HalogenScrubber
150mL
Dehumidifier
Humidifier
Carrier Gas
BlankCheck
Vessel
Phosphoric
Acid
Drain
Vessel
Verdnnungswasser
Regeneration of IC-solution:
4 5
3
6 8-Port-Ventil
ASI-V
2
7
e.g. decreasing
sensitivity,
broad IC-Peaks
1
0-Port
8
TC-Port
5 mL-Spritze
NDIR-Detector
Drain
Filter
150mL
IC
Measurement
Khlschleife
Valve
switches
(click)
peristaltic
Pump
IC-Port
CO2Absorber
HalogenScrubber
Druckregler
Trgergas
150mL
25%
Befeuchter
Phosphoric
Acid
(630-00710SE)
Dehumidifier
BlankCheck
Gef
Phosphoric
Acid
Drain
Vessel
Dilution Water
(HCL)
3
ASI-V
2
1
0-Port
NDIR-Detector
8-Port-Valve
7
8
TC-Port
5mL-Syringe
Drain
Filter
~ 230mL
IC
Measurement
Cooling Loop
CO2Absorber
~ 80mL
HalogenScrubber
~ 150mL
Pressure
Regulator
Dehumidifier
~ 130mL
Humidifier
Carrier Gas
Mist
Trap
Drain
Vessel
Dilution Water
(HCL)
3
ASI-V
5
6
2
1
0-Port
5mL-Syringe
~ 80mL
~ 150mL
Pressure
Regulator
Carrier Gas
7
8
NDIR-Detector
Check
of acid addition:
8-Port-Ventil
Observation:
Drain
TC-Port
IC-results generally
too low
Peak of 1. injection lower then following Peaks
IC
1. Step:
Messung
check filling of acid container,
Khlschleife
check correct
acid sampling tube position
Filter
2. Step:
Are there air bubbles/no liquid in acid sampling tube
(especially near 8-Port Valve) to observe ?
=> check if tube connection at 8-Port Valve is tight
=> exchange possible defective tube (638-41337-03)
~ 130mL
Ent=> exchange possible defective Rotor (631-20265)
feuchter
=>Befeuchter
exchange complete
8-Port
Valve
(638-56135),
Schmutzinclusive RotorFalle
DrainGef
~ 230mL
CO2Absorber
Good luck
for
(hopefully seldom)
Troubleshooting