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To determine the melting point of certain compounds using the Thomas-Hoover melting point apparatus. To assess the purity of these compounds. 01-10-14 and 01-17-14
Objectives
Brief statement of objectives.. ala ku manual ):
Theoretical Background
Phase change from solid to liquid
defined as
Melting
Kinetic Molecular Theory
Melting Range
Theoretical Background
Melting Range
Molecular Structure
affected by
Intermolecular Forces
Purity of Solids
= 55.929 1.5
where y is the temperature x & k is the knob setting
= 55.929 1.5
where y is the temperature x & k is the knob setting
We obtain,
We obtain,
= = .
= = .
Conclusions
Packing
H-bonding
Intermolecular Forces
Dipole-dipole
London Dispersion
Pure
1-2 degrees C
Purity of solids
Impure > 1-2 degrees C