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I.
REACTOR TO RECEIVING TANK The determination of the pipe diameter will be based on the vapors that come from
the main reactor to the receiver. The density of the hydrocarbon vapors is 1.2 g/L and steam is 0.804 g/L (www.wikipedia.com). The transfer of the products from the main reactor to the receiver tank is pressure driven and it is assumed to be in turbulent flow.
Receiving Tank
Properties of Vapors and Steam m (kg) p(g/L) X 415.9122 1.2 0.6246 250.00 0.804 0.3754 665.9122
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It should take 18 minutes to draw off all the gases and vapors inside the reactor then,
[7.1]
According to Perry s Chemical Engineering Handbook, the available pipe standard that will fit to the calculated optimum inside diameter is a 12 in nominal Sched 80 having pipe dimensions of
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[7.3]
It is assumed that the viscosity of the gas is 0.01cP then the Reynolds number using is, [7.4]
Table 7.2
Summation of Pipe Length from the Main Reactor to the Receiving Tank Type Number L/D in Ft m R due to Entrance 2.8435 0.23696 0.0722 Valve 1 5 56.87 4.7392 1.4445 Pipe 1 36.00 3.00 0.9144 Pipe 2 36.00 3.00 0.9144 L 131.7135 10.97616 3.3455
[7.5]
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where D2 is the diameter of the receiving tank calculated in chapter 6 and v2 is the velocity inside the receiving tank then, with diameter of the receiving tank equal to 0.7393 m.
Therefore the flow from the main reactor to the receiver tank is turbulent. The assumed turbulent flow in the beginning of the calculation is verified.
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II.
3 Receiving Tank
Condenser
Due to the lowering of temperatures, it is assumed that the condensable vapors and steam are condensed inside the tubes. Table 7.3 Properties of Water and Condensable Gases m (kg) X (kg/m3) X (kg/m3) water 250 0.4201 1000 420.0843 condensables 345.1186 0.5799 760.488 441.0189 Total 595.1186 861.1032
To maintain the velocity from the reactor to the receiving tank, the pipe from the receiving tank to the condenser must be smaller compared to the pipe from the reactor to the receiving tank. It is assumed to have a pipe diameter of 6 in (0.1524 m). Rearranging equation [7.1], volumetric flow-rate inside the pipe is,
From Perry s Chemical Engineering Handbook the nominal pipe size diameter that will fit to the assumed diameter is Di = 6.065 in.
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Given that the tubes inside the condenser has an inside diameter of Di = 0.019 m, the volumetric flow-rate and the velocity can be calculated using the equation, [7.8]
This equation holds true for pipe diameter, Di < 0.0254 m, with
Solving for volumetric flow-rate inside the tubes using the equation [7.1]
The fluid velocity inside the condenser tubes using equation [7.3],
The above calculated velocity is observed to be big because there is a sudden contraction of the tube, but actually this value will decrease as the temperature is decreasing in the condenser, until the velocity of the liquid becomes small in the discharge of the condenser. A tube length of 3.66 meters is assumed to be sufficed for the diesel vapor to condense.
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Table 7.4 Properties of the Condenser Tube Pipe Diameter tube Length Fluid Velocity Volumetric Flow rate 0.019 in 12 ft 0.7124 m/s 0.2794 m3/s
III.
Condenser
Centrifuge
To find the volumetric flow rate of the condensate using equation [7.1]. The pipe diameter of the discharge of the condenser to the centrifuge is assumed to be 3 in (0.0762 m) to maintain turbulence.
Based on the standard dimensions from Perry s Chemical Engineering Handbook, the appropriate size of the pipe that fits to the calculated diameter is 3 in nominal pipe Sched 40 whose inside diameter is 3.068 in (0.0779 m).
Production of Industrial Diesel Oil from Waste Thermoplastics by Hydrous Pyrolysis
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Table 7.5 Summation of Pipe Length from Condenser to Centrifuge Type Number L/D in ft M 90 Elbow 1 30 92.04 7.67 2.3378 Pipe 5 36 3 0.9144 Pipe 6 60 5 1.524 L 188.04 15.67 4.7762
IV.
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Cooling water requirement is 15,479.6392 kg/hr with density equal to To solve for the volumetric flow rate use equation [7.2].
Assuming turbulent flow, use the equation [7.1] to get the optimal inside diameter of the pipe,
Based on pipe standards on Perry s Chemical Engineering Handbook, 3 in nominal pipe schedule 40 is appropriate.
The friction loss due to expansion is, with A1/A2 approaches zero since A2 >>> A1 [7.10]
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Friction loss due to contraction, With =1 for turbulent flow and 0.5 for laminar flow
[7.11]
Skin friction: Solve for Reynold s number first using equation [7.4] to know the value of the friction fanning factor, f.
The flow is turbulent and assumed that it flows on a smooth pipe. From the Moody Chart , fouling factor, f is 0.0058 for the Reynolds Number or 70,211.2700.
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[7.12]
90o elbow
To find the shaft work of the pump, Bernoulli s equation is used where
[7.15]
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The efficiency of a centrifugal pump is, n= .80 then the work of the pump done is, [7.16] rearranging the equation above,
[7.17]
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V.
10 Cooling Tower
11
Calculating the Volumetric flow-rate based on the mass flow-rate intended for make-up water using equation [7.2],
Assuming smooth pipe is used, the optimum pipe diameter using equation [7.1] is ,
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The standard pipe to be used is a 1 in nominal pipe schedule 40 having an inside diameter of, from Perry s Chemical Engineering Handbook,
The fluid velocity of make-up water inside the pipe is, using equation [7.3]
Table 7.6
Summation of Pipe Length from Make-Up Water to Cooling Tower Type Number L/D In ft 90 Elbow 1 30 31.47 2.6225 Pipe 10 60 5 Pipe 11 48 4 L 139.47 11.6225
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VI.
The desired time to drain out 250 kgs of water to be fed to the reactor is 10 minutes, [7.18]
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The available pipe standard having a nominal pipe diameter of 1.25 and schedule 40, from Perry s Chemical Engineering Handbook, assuming smooth pipe is use with, Solving for Area using equation [7.9],
The fluid velocity of water inside the pipe using equation [7.3] is
VII.
WATER RESERVOIR TO WATER TANK (PROCESS) Based on the given parameters and the calculations above, the friction losses on the
pipeline from the reservoir prior to entry in the water storage tank (process) can be solved. The velocity to be used can be solved using equation [7.3] is,
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Assume that the velocity of the water out of the storage tank is equal to the water velocity in of the storage tank, Skin Friction: Solving for the Reynold s number first,
Since the solved Reynolds number is laminar, the friction fanning factor is 16/ NRe.
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Friction loss due to fittings: One 45 elbow and one globe valve are used. The friction loss due fittings can be solved using equation [7.13]
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The efficiency of a centrifugal pump is, n= .80 then the work can be determined using equation [7.16].
The power consumed by the pump can be also known using equation [7.17].
VIII.
Slaked Lime
14
15
Main Reactor
The slaked lime tank should drain out 58.5101 kg within 10 minutes The mass flow-rate,
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Assuming turbulent flow and using a smooth pipe, the optimal inside diameter is, using equation [7.1]
The pipe standard dimensions available is a 3 in nominal pipe schedule 10S. It s inside diameter is, from Perry s Chemical Engineering Handbook, The fluid velocity of the slaked lime inside the pipe is
Table 7.7
Summation of Pipe Length from Slaked Lime Tank to Main Reactor Type Number L/D in Ft 90 Elbow 1 30 14.79 1.2325 Pipe 14 36 3 Pipe 15 60 5 L 110.79 9.2325
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