Application of Precision Data MS BSII IS 2796

Test Requirements
Characteristic
Method Limits
Repetabil Reprodu
Upper Lower
ity cibility
(A1) (A2)
770 710
Density @ 15oC, Kg/m3 P:16 0.5 1.2
P:18/ 45 10 1 3
Distillation:(E-70), % v
D:86 70 40 1 3
Distillation:(E-100), % v
90 1 3
Distillation:(E-180), % v  
215 1 4
FBP  
88 0 1
RON P:27  
88 0.2 0.7
D:2699  
40
Existent Gum, g/m3 P:29   11.87 23.33
0.05
Sulphur, Total % mass P:34   0.005 0.0112
60 35
(RVP) at 38oC kPa P:39 0.02 0.04
1   0.04 0.18
Benzene, % by Vol. D:3606
3   0.03 0.84
0.013
Lead, g/lit IP:352  
0.002 0.008
ata MS BSII IS 2796
Acceptable Not OK Margins,
A1- Margins, Supplier Recipient
A2>4R; , ,
A1,A2>2
R A1-0.59R A2+0.59R A1+0.59R A2-0.59R Remarks

60>4.8 769.29 710.71 770.71 709.29 OK 769.29 710.71 770.71 709.29

35>12 43.23 11.77 46.77 8.23 OK 43.23 11.77 46.77 8.23
30>12 68.23 41.77 71.77 38.23 OK 68.23 41.77 71.77 38.23
90>6 91.77 88.23 OK #VALUE! 91.77 #VALUE! 88.23
215>8 212.64 217.36 OK 212.64 #VALUE! 217.36 #VALUE!
88>2 88.59 87.41 OK #VALUE! 88.59 #VALUE! 87.41
88>1.4 88.41 87.59 OK #VALUE! 88.41 #VALUE! 87.59

40>46.66 26.24 53.76 NOT OK 26.24 #VALUE! 53.76 #VALUE!

0.5>0.224 0.0434 0.0566 OK 0.0434 #VALUE! 0.0566 #VALUE!

25>0.16 59.98 35.02 60.02 34.98 OK 59.98 35.02 60.02 34.98

1>0.36 0.89 1.11 OK 0.89 #VALUE! 1.11 #VALUE!
3>1.68 2.5 3.5 OK 2.50 #VALUE! 3.50 #VALUE!
0.013>0.0
15 0.008 0.0177 OK 0.008 #VALUE! 0.018 #VALUE!
 Application of Precision Data MS BSIII IS 2796
Test Requirements A1-
Characteristic A2>4R;
Method Limits Repetabil Reprodu A1,A2>2
Upper Lower
ity cibility R
(A1) (A2)
775 720 0.5 1.2 55>4.8
Den @ 15oC, Kg/m3 P:16
P:18/ 45 10 1 3 35>12
Distill:(E-70), % v
D:86 70 40 1 3 30>12
Distill:(E-100), % v
75 1 3 75>6
Distill:(E-150), % v  
210 1 8 210>16
FBP  
91 0.2 0.7 91>1.4
RON D:2699  
5   2.1 4.04 5>8.08
Ex Gum, mg/100ml P:29 0.015>0.0
0.015
Sulphur, Total % m D:4294   18
0.005 0.009
60 0.02 0.04 60>0.08
RVP at 38oC kPa P:39  
1   0.04 0.18 1>0.36
Benzene, % by Vol. D:3606
42   1.6 3.5 42>7.0
Aromatics, % Vol P:23
21   1.6 6.8 21>13.6
Olefins, % Vol P:23 0.005>0.0
0.005
Lead, g/lit IP:352   15
0.002 0.008
 Acceptable
MS BSIII IS 2796
Margins, Supplier Not OK Margins,
Recipient

A1-0.59R A2+0.59R A1+0.59R A2-0.59R Remarks

774.29 720.71 775.71 719.29 OK
43.23 11.77 46.77 8.23 OK
68.23 41.77 71.77 38.23 OK
76.77 73.23 OK
205.28 214.72 OK
91.41 90.59 OK
2.62 7.38 NOT OK

0.0097 0.0203 NOT OK

59.98   60.02   OK
0.89 1.11 OK
39.94   44.07   OK
16.99   25.01   OK

0 0.0097 NOT OK
 Application of Precision Data HSD IS 1460 BSIIAcceptable
A1- Margins, Supplier
Test Requirements
Sl. Characteristic A2>4R;
Method Limits Repetabil Reprodu A1,A2>2
Upper Lower
ity cibility R A1-0.59R
(A1) (A2)
1 860 820 0.5 1.2 40>4.8 859.29
Density @ 15oC, Kg/m3 P:16
2 0.01
Ash, % by Mass P:4 0.01=0.01
0.003 0.005 0.007
3 0.3
RCR, %by mass P:8 0.3>0.124
0.04 0.062 0.263
4 0.25 0.04 0.05 0.25>0.1 0.22
Sulphur, Total % m P:33 0.05>0.09
5 0.05
Sulphur, Total % m IP:336 4
0.014 0.047 0.0223
6 3 3 6 15>12 0
Pour Point,oC,winter P:10
7 15 3 6 3>12 11.46
Pour,oC,summer P:10
8 48 0 2 48>4  
Cetane Number P:9  
9 35 1 1.5 35>3  
Flash Point P:20  
10 5 2 0.018 0.035 3>0.14 4.98
K V, cSt at 40 oC P:25
5 2 0.007 0.014 3>0.06 4.99
11 P:18/ 85 2 5 85>10  
Distill(E-350), % v  
D:86 95 2 5 95>10  
Distill:(E-370), % v  
12 0.2 0.1 0.2 0.2>0.4 0.08
Acidity -T, mgKOH/g P:2
13 0.05 0.1 0.2 0.05>0.4 -0.07
Water Content, % v P:40
14 0.05
Sediment P:30 0.05=0.05
0.03 0.05 0.02
BSIIAcceptable
Margins, Supplier Not OK Margins,
Recipient

A2+0.59R A1+0.59R A2-0.59R Remarks

820.71 860.71 819.29 OK

0.013 BORDER

  0.337   OK
  0.28   OK

  0.0777   NOT OK
  6.54   OK
  18.54   NOT OK
49.18   46.82 OK
35.89   34.12 OK
2.02 5.02 1.98 OK
2.01 5.01 1.99 OK
87.95   82.05 OK
97.95   92.05 OK
  0.32   NOT OK
  0.17   NOT OK

  0.08   BORDER
 Acceptable
Application of Precision Data HSD IS 1460 BSIII
A1- Margins, Supplier
Test Requirements
Characteristic A2>4R;
Method Limits Repetabil Reprodu A1,A2>2
Upper Lower
ity cibility R A1-0.59R
(A1) (A2)
845 820 0.5 1.2 25>4.8 844.29
Density @ 15oC, Kg/m3 P:16
0.01 0
Ash, % by Mass P:4 0.01=0.01
0.003 0.005 0.007
0.3 0
RCR, %by mass P:8 0.3>0.124
0.04 0.062 0.26
0.035>0.0
0.035 0
Sulphur, Total % mass D:4294 22
0.006 0.011 0.0285
0 51 0 2 51>4 49.82
Cetane No P:9
0 35 1 1.5 35>3 34.12
Flash Point P:2
4.5 2 0.016 0.032 3>0.14 4.48
K V, cSt at 40 oC P:25
4.5 2 0.007 0.014 3>0.06 4.49
0 95 2 5 95>10 92.05
Distillation(E-360), % v P18/ D:86
0.02 0
Water Content, %(v/v) P:40 0.02=0.02
0.003 0.01 0.01
6 0 1 2 6>4 4.82
CFPP,oC,winter P:110
18 0 0.5 1 18>2 17.41
CFPP,oC,summer P:110
0 25 6.7 13.1 25>26.2 17.27
Oxidation Stability D:2274
11 0 1.77 3.83 11>7.66 8.74
PAH, % m IP:391
0 460 63 120 460>204 389.2
Lubricity, Mu IP:450
 Acceptable
0 BSIII
Margins, Supplier Not OK Margins,
Recipient

A2+0.59R A1+0.59R A2-0.59R Remarks

820.71 845.71 819.29 OK

0.013 0.013 0.007 BORDER

0.34 0.34 0.263 OK

0.041 0.041 0.029 OK

52.18 1.18 49.82 OK
35.89 35.89 34.12 OK
2.02 4.52 1.98 OK
2.01 4.51 1.99 OK
97.95 97.95 92.05 OK

0.01 0.03 -0.01 BORDER

7.18 7.18 4.82 OK
18.59 18.59 17.41 OK
32.73 32.73 17.27 NOT OK
13.26 13.26 8.74 OK
530.8 530.8 389.2 OK
 Seven Critical Parameters for MS BSII- Rail/Road and Pipeline
BIS BIS Precision Test Rail/Roa Rail/Roa P/L Mfg
Characteristic
BSII BSIII Limits Margins d Mfg d Mfg Specs
(Repet./ as per Specs Specs BSIII
Specs Specs
ISO {2000
Repro) BSII BSIII
4259 ppm SKO
based on interface
single
}
test
result
Density @ 15oC, Kg/m3 710.72-
710 – 770 720-775 0.5/0.12 711-768* 721-773 721-773
769.28
Nov-38 Nov-38
Distill-Rec, 70oC , % v 10 – 45 10 – 45 - 11.8-43.2 11-38*

100oC , % v 40 – 70 40 – 70 - 41.8-68.2 41-70 41-70 41-70

75 76 76
150oC , % v -      
90 91.8 91 92
180oC , % v Min   -  

215 210 212 200 200 200

FBP, oC, Max. -
88 91 88.42 88.2 91.2 91.2
RON, Min. 0.2/0.7
500 150 225 480 145 125
Sul % m, Max. 145/467

60 58 58
RVP at 38oC kPa 35 – 60 3.2/5.2 37.1-57.6 38-58*

1 1 0.892 0.9 0.9 0.9

Benz, % v. Max. 0.04/0.18

3 0.03/.84 2.504 2.8

  - -

Cu Corr, Max. 1 max   NA NA Dropped - -

and Pipeline
Justification/Remarks

To take care of addition of 5%

ethanol
LL to take care of storage and
handling impact and upper limit
to take care of addition of
ethanol
LL to take care of storage and
handling impact.
 
LL to take care of storage and
handling impact.
 
To take care of test margin

To take care of Testing Margin

LL to take care of testing
margin. UL to facilitate
absorption of ethanol

To take care of Testing Margin

and production constraints
 Seven Critical Parameters for HSD- Rail/Road and Pipeline
BIS Precision Test Margins as per Rail/Roa
Sl. Characteristic
Limits ISO 4259 based on d Mfg
Specs
(Repetability
single test result Specs
/
Reproducibili
ty)
1 46 47.98 47
Cetane Index, Min F(Den,Dist)
2 Distillation :Recovery up to 370oC 95 96.2 96
-
(E-370), % by Vol. Min

3 35 36.8 37
Flash Point, Deg C, Min 1/1.5
4 Sulphur, Total Percent by mass, 0.05 0.7 225 450
Max.
5 460 388 420
Lubricity, Mu, Max 60/120
7 Copper Strip Corrosion, for3 hrs 1 Qualitative test. No
NA 1a
Precision limit
at 50 C, Max.
o

applicable
d Pipeline
Justification/Remarks

To take care of test margin

To take care of Test margin
recovery higher than 95% to be
ensured.
To take care of test margin for
safety considerations.
To take care of Testing Margin

To take care of Testing Margin

To improve product quality
further
 Four Critical Parameters for SKO- Rail/Road and Pipeline
BIS Precision Test Rail/Roa
Sl. Characteristic
Limits Margins d Mfg
Specs
(Repeta as per
Specs
bility/ ISO
Reprodu 4259
based on
cibility)
single
test
result
1 18 2-Jan 19.8 19
Smoke Point, mm, Min.

2 300 297 290

Distillation : FBP, Deg C, Max -

4 2500 2160 2400

Sulphur, Total % mass, Max. 175/580
oad and Pipeline
Justification/Remarks

To take care of test margin. 20

for Rlys and 22 for Defence

To take care of Testing Margin

Specs inferior to ISO 4259
owing to production difficulty.
 Eight Critical parameters for ATF- Rail/Road
BIS Precision Test Rail/Road
Sl. Characteristic
Limits Margins
Specs Mfg Specs
(Repeta as per
Aromatics, percent by volume, 25 23.2 20
1.4/3.0
bility/ ISO
###
Max Reprodu 4259
Sulphur mercaptan, percent by 0.003/0.0 0.00297
based on 0.002
NA
cibility)
### single
mass, Max 02
Sulphur Total, ppm by mass, 3000 2700
test 2500
50/175
###
Max result
### 300 297 290
Final Boiling Point, oC, Max -
### 38 38.9 40
Flash point ( Abel ), oC, Min 1/1.5
### -47 -48.38 -49
Freezing point, oC, Max 0.7/2.6
0.778 0.65
Lubricity: WSD, mm, Max 0.85/ 0.65 -
###
ATF- Rail/Road
Justification/Remarks

Def Reqmt 20. Since product cannot be segregated

Def Reqmt 0.002

Def Reqmt 2500

To take care of Test Margin
To take care of Test Margin
To take care of Test Margin

Def reqmnt-0.65
 S Prod Characteristic Road/Rail Movement Coastal
1 MS Density +/-0.002 @ 15 oC +/-0.002 @ 15 oC
RON 0.5 unit > BS-II -88 0.5 unit > BS-II -88

BS-III-91 BS-III-91
Distillation 1% above of Min Range 1% above of Min Range

FBP Min 10oC < BS-II:215 oC; Min 10oC < BS-II:215 oC;
BS-III:210 oC BS-III:210 oC

Benzene 0.2<3 BS-II 0.2<3 BS-II

0.1< 1 BS-III 0.1< 1 BS-III
RVP BS-I:38 Min; 58 Max BS-I:38 Min; 58 Max
BS-II: 58 Max BS-II: 58 Max
Sulfur 20 ppm < BS-II:500 ppm; 20 ppm < BS-II:500 ppm;

5 ppm<BS-III:150 ppm 5 ppm<BS-III:150 ppm

2 SKO Density +/-0.002 @ 15 oC +/-0.002 @ 15 oC

Flash point 38 oC Min of individual T/L; 38 oC Min

T/W
3 HSD Density +/-0.002 @ 15 oC +/-0.002 @ 15 oC

K. Vis @ 40 oC - 0.2 Cst > 2 Cst for BS-II,

BS-III

Distillation 0.5>BS-II: 95% Vol 0.5>BS-II: 95% Vol

Recovery

Cetane Index - 0.5 unit > BS-II: 46; BS-III

51

Cetane No - 0.4>BS-II:48;BS-III:51

Flash Point 2> 35 oC 2> 35 oC

Lubricity 40< BS-II/BS-III: 460 mu 40< BS-II/BS-III: 460 mu

Oxidation stability 3<BS-III: 25 3<BS-III: 25

Particulate matter 24 mg/Kg 24 mg/Kg

Sulfur 20 ppm < BS-II:500 ppm; 20 ppm < BS-II:500 ppm;

10ppm< BS-III:350 ppm 10ppm< BS-III:350 ppm

nce by Marketing/OMC under various modes of transport: Road/Rail, Coastal and Pipeline Transfers
 4 ATF Density +/-0.002 @ 15 oC +/-0.002 @ 15 oC
Particulate Visual inspection- free from Visual inspection- free
Contamination sediments from sediments

Water 30 ppm through Aquadis Free from dissolved water

check using aquadis check

Silver Strip Corr. Test H after loading TT / Test E after loading

Tank Wagon
Copper Strip Corro Test H after loading TT / Def-1; Civil-1 as per Test
Tank Wagon E after loading
Lubricity Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85
Conductivity 250-450 PS/M using 250-450 PS/M
conductivity meter
Using conductivity meter

S Test E:
1 Appearance
2 Density @ 15 oC
3 Flash Point
4 Existent Gum
5 Copper Strip Corrosion Test
6 Distillation
7 Doctor Test
8 Water Reaction
9 Freezing Point
Note: The Customer may take product Coastally and push into cross country pipelines at the destination. In such a eventuality, the man
have to take care of the Max/Min limits of the most stringent requirement. In ATF conductivity insisted ex Mktg Company is 250 PSM Mi
ref Tanks it has to be in the range of 350 + as per our experience factor.
Pipeline Transfers Guarantee to Customer

+/-0.002 @ 15 oC BS-II :710-770; BS-

III: 720-775
1 unit > BSII -88(93); BSIII-91 {when BS-II -88
SKO is intermediate Product}

BS-III-91
1% above of Min Range BS-II Rec@70:10-45%;@100:40-70%
@180: 90% Min
BS-III Rec@70:10-45%;@100:40-70%
@150: 75% Min
Min 20 oC < BS-II:215 oC; BS-III:210 oC BS-II:215 oC;
{when SKO is intermediate Product}

BS-III:210 oC
0.2<3 BS-II 0.1< 1 BS-II: 3 Max
BS-III BS-III : 1 Max
BS-I:38 Min; 58 Max BS-I 35-60 Kpa BS-
III 60 Kpa Max
BS-II: 58 Max
50 ppm < BS-II:500 ppm; BS-II:500 ppm; BS-
III:150 ppm
25 ppm<BS-III:150 ppm
{when SKO is intermediate Product}

+/-0.002 @ 15 oC 775-840

42 oC Min {when interfaced with MS/ 35 oC Min

Naphtha}
+/-0.002 @ 15 oC BS-II: 820-860;
BS-III 820-845
0.2 Cst > 2 Cst for BS-II, BS-III BS-II: 2-5 Cst;
BS-III: 2-4.5 Cst
0.5>BS-II: 95% Vol BS-II: 95% Vol @370 oC

BS-II: 95% Vol @360 oC

0.5 unit > BS-II: 46; BS-III 51 BS-II: 46;

BS-III 51
0.4>BS-II:48;BS-III:51 BS-II: 48;

BS-III 51
2> 35 oC BS-II/BS-III: 35 oC Min
40< BS-II/BS-III: 460 mu BS-II: 460;

BS-III 460
3<BS-III: 25 BS-II:NA

BS-III: 25 g/m3, Max

24 mg/Kg BS-II: NA
BS-III:NA
50 ppm < BS-II:500 ppm; BS-II:500 ppm;

BS-III:350 ppm BS-III:350 ppm

 +/-0.002 @ 15 oC 775-840
Visual inspection- free from sediments 0.22 mg/lit

(Qtly Millipore gravimetric test)

Free from dissolved water using aquadis 15 ppm using aquadis check
check

Test H after commencement of PLT Def-1; Civil-2

Test H after commencement of PLT Def-1; Civil-1

Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85

250-450 PS/M 50-450 PS/M
Using conductivity meter

Sr Test H:
1 Density @ 15 oC
2 Temperature
3 Appearance
4 Water / Sediments
We are producing only one Grade of ATF. Since the Defence Grade is more
stringent, the Defence specs needs to be met so that we can supply to both civil as
well as defence requirements.

country pipelines at the destination. In such a eventuality, the manufacturing specs will
ent. In ATF conductivity insisted ex Mktg Company is 250 PSM Min by OMCs. Therefore at
r.
S Prod Characteristic Refinery to Mkt Road/Rail Coastal
Movement
1 MS Density <+/-0.0025 @ 15 oC +/-0.0025 @ 15 oC +/-0.0025 @ 15 oC

RON(AKI) - 0.5 unit > BS-II 0.5 unit > BS-II -88(93)
-88(93)

BS-III-91 BS-III-91
FBP - - Min 10oC < BS-II:215 oC;
BS-III:210 oC

Sulfur - 20 ppm < BS- 20 ppm < BS-II:500 ppm;

II:500 ppm;
5 ppm<BS-III:150 5 ppm<BS-III:150 ppm
ppm

2 SKO Density <+/-0.0025 @ 15 oC +/-0.0025 @ 15 oC +/-0.0025 @ 15 oC

Flash point 38 oC Min 38 oC Min of 38 oC Min

individual T/L; T/W

3 HSD Density <+/-0.0025 @ 15 oC +/-0.0025 @ 15 oC +/-0.0025 @ 15 oC

K. Vis @ 40 oC - - 0.2 Cst > 2 Cst for BS-II, BS-

III
Cetane No. - - 0.2 unit > BS-II: 48; BS-III 51

Sulfur - - 20 ppm < BS-II:500 ppm;BS-

III:350 ppm
4 ATF Density <+/-0.0025 @ 15 oC +/-0.0025@ 15 oC +/-0.0025@ 15 oC

Particulate 1.0 mg/lit Visual inspection- Visual inspection- free from

Contamination free from sediments
sediments
Water Free from undissolved 30 ppm through Free from dissolved water
water Aquadis check using aquadis check
Silver Strip Corr. Def-0; Civil-1 Test H after Test E after loading
loading TT / Tank
Wagon
 Copper Strip Def-1; Civil-1 Test H after Def-1; Civil-1 as per Test E
Corro loading TT / Tank after loading
Wagon
Lubricity Def- 0.65; Civil-0.85 Def- 0.65; Civil- Def- 0.65; Civil-0.85
0.85
Conductivity 300-450 PS/M using 250-450 PS/M 250-450 PS/M
conductivity meter using conductivity Using conductivity meter
meter
s Test E: sr
1 Appearance 1
2 Density @ 15 oC 2
3 Flash Point 3
4 Existent Gum 4
5 Copper Strip Corrosion Test We are producing only on
6 Distillation more stringent, the Defen
supply to both civil as wel
7 Doctor Test
8 Water Reaction
9 Freezing Point
Note: The Customer may take product Coastally and push into cross country pipelines at the desti
manufacturing specs will have to take care of the Max/Min limits of the most stringent requirement
Company is 250 PSM Min by OMCs. Therefore at ref Tanks it has to be in the range of 350 + as per
 Pipeline Transfers Guarantee to
Customer
5 @ 15 oC +/-0.0025 @ 15 oC BS-II :710-770;
BS-III: 720-
> BS-II -88(93) 775
1 unit > BSII -88(93); BSIII-91 BS-II -88(93)
{when SKO is intermediate
Product}
BS-III-91(95)
< BS-II:215 C; o
Min 15 C < BS-II:215 C; BS- BS-II:215 oC;
o o

:210 oC III:210 oC {when SKO is

intermediate Product}

BS-III:210 oC
< BS-II:500 ppm; 50 ppm < BS-II:500 ppm; BS-II:500 ppm;
BS-III:150
S-III:150 ppm 25 ppm<BS-III:150 ppm ppm

{when SKO is intermediate

Product}
5 @ 15 oC +/-0.0025 @ 15 oC 775-840

n 42 oC Min {when interfaced 35 oC Min

with MS/ Naphtha}

5 @ 15 oC +/-0.0025 @ 15 oC BS-II: 820-860;

BS-III 820-845
2 Cst for BS-II, BS- 0.2 Cst > 2 Cst for BS-II, BS- BS-II: 2-5 Cst;
III BS-III: 2-4.5 Cst
> BS-II: 48; BS-III 51 0.5 unit > BS-II: 48; BS-III 51 BS-II: 48;
BS-III 51
< BS-II:500 ppm;BS- 50 ppm < BS-II:500 ppm;BS- BS-II:500 ppm;
pm III:350 ppm BS-III:350 ppm
5@ 15 oC +/-0.0025@ 15 oC 775-840

spection- free from Visual inspection- free from 0.22 mg/lit

s sediments (Qtly Millipore
gravimetric test)
m dissolved water Free from dissolved water 15 ppm using
uadis check using aquadis check aquadis check
fter loading Test H after commencement Def-1; Civil-2
of PLT
 vil-1 as per Test E Test H after commencement Def-1; Civil-1
ding of PLT

5; Civil-0.85 Def- 0.65; Civil-0.85 Def- 0.65; Civil-0.85

PS/M 250-450 PS/M 50-450 PS/M

nductivity meter Using conductivity meter
Test H:
Density @ 15 oC
Temperature
Appearance
Water / Sediments
We are producing only one Grade of ATF. Since the Defence Grade is
more stringent, the Defence specs needs to be met so that we can
supply to both civil as well as defence requirements.

ntry pipelines at the destination. In such a eventuality, the

ost stringent requirement. In ATF conductivity insisted ex Mktg
the range of 350 + as per our experience factor.