Avergage of

Sample 1 Sample 2
(Sample 1 &2)
Temperature 'C Viscosity(Pa.s) Viscosity (Pa.s) Viscosity (Pa.s)2
135 0.54 0.53 0.535
145 0.33 0.35 0.34
155 0.22 0.23 0.225
165 0.14 0.13 0.135

Compaction And Mixing Temperatures

1
Viscosity (Pa.s)

0.1
130 140 150 160

Temperature
 Mixing Range Compaction Range
Viscosity (Pa.s)3 Viscosity (Pa.s)4 Viscosity (Pa.s)5 Viscosity (Pa.s)6
0.17 0.19 0.28 0.31
0.17 0.19 0.28 0.31
0.17 0.19 0.28 0.31
0.17 0.19 0.28 0.31

Mixing Temperatures

Sample 1
limit 0.17
limit 0.19
limit 0.28 Sample 1
limit 0.31
Sample 2
Sample 2
Average Sample Average

0 160 170 180

Temperature
 Mixing Range Compaction Range
lower higher lower higher
158 161 146.5 149
158 160 147.5 150
158 160.5 147 149.5
 Mesh # Diameter (mm) % Passing D^0.45
Max 11/2" 37.5 100 5.108743
Nominal 1" 25 98 4.2567
3/4" 19 82 3.762176
1/2" 12.5 71 3.116087
3/8'' 9.5 66 2.754074
Superpave 25 mm No.4 4.75 50 2.0161
Designation No.8 2.36 34 1.47167
No.16 1.18 22 1.077325
No.30 0.6 14 0.794636
No.50 0.3 10 0.581707
No.100 0.15 7 0.425835
No.200 0.075 4.5 0.311729
Pi=100(di/ Control pt Control Pt max
100 100 100
83.32186 90 100
73.64191
60.99517 120
53.90903
39.46372 100
28.80689 19 45
21.08788 80
%Passing

15.55443
60 Gradation.
11.38651 Max density
8.335411 40 Control min
6.101878 1 7 Control Max

20

0
0 1 2 3 4 5 6
Diameter ^0.45
Gradation.
Max density
Control min
Control Max
 Temperature
Sample Lab ID % AC
Correction Factor

Sample 1 1.0005
Sample 2 4% 1.0005
Sample 3 1
Sample 1 0.99973
Sample 2 3.50% 1
Sample 3 1.00073
Sample 1 1.00025
Sample 2 3% 1.00025
Sample 3 0.9995
Sample 1 1.00037
Sample 2 4.50% 1.00117
Sample 3 1.00013

N(gyration Sample ID % AC Dry Weight (KG)

Sample 1 4.6673
100 Sample 2 4 4.6655
Sample 3 4.6631
Sample 1 4.6714
100 Sample 2 3.5 4.6676
Sample 3 4.6726
Sample 1 4.667
100 Sample 2 3 4.6672
Sample 3 4.6737
Sample 1 4.6634
160 3.5
Sample 2 4.6632
GSb= 2.861 Sample 1 4.6551
160 4.5
Sample 2 4.6557

%PS % AC %Gmm % Va
96 4 0.976556 2.34435122815407
96.5 3.5 0.958255 4.17448688509999
97 3 0.94103 5.89695085994899
96.5 3.5 0.974064 2.59355265475673
95.5 4.5 0.991874 0.812611279550501

optimum binder
7
6
f(x) = − 12.3190109771245 ln(x) + 19.4867273432335
 optimum binder
Vma at A
7
13
6 12.5
f(x) = − 12.3190109771245 ln(x) + 19.4867273432335 f(x) = − 0.996
5 12

%Vma
+ 4.3493816
4 11.5
11

Va
3 10.5
2 2.5 2.7 2.9 3

1
0
2.5 2.7 2.9 3.1 3.3 3.5 3.7 3.9 4.1
% Binder

% Gmm at optimum AC
0.98
0.97 f(x) = 0.035525996317949 x + 0.834273049643167
0.96
%Gmm

0.95
0.94
0.93
0.92
2.5 2.7 2.9 3.1 3.3 3.5 3.7 3.9 4.1
%Binder
 Weight of
Weight of Flash + Gmm Gmm Average
weight of sample (KG) Flash+Sample+Water(K
Water(KG) calculated corrected Gmm
G)
2.4784 7.9257 6.3636 2.704791007 2.706143
2.4817 7.9295 6.3636 2.709871151 2.711226 2.703828
2.4767 7.921 6.3636 2.694115088 2.694115
2.4804 7.932 6.3636 2.719736842 2.719003
2.4819 7.9291 6.3636 2.708315146 2.708315 2.714523
2.4822 7.9313 6.3636 2.714270093 2.716252
2.4834 7.9392 6.3636 2.735624587 2.736308
2.4853 7.944 6.3636 2.746491325 2.747178 2.738558
2.4848 7.9394 6.3636 2.733553355 2.732187
2.4715 7.9147 6.3636 2.685245545 2.686239
2.4555 7.9045 6.3636 2.684780232 2.687921 2.688478
2.4961 7.9321 6.3636 2.690922812 2.691273

Submerged Weight Average

SSD Weight (KG) Gmb calculated
(KG) Gmb
2.9057 4.672 2.64241635056332
2.9064 4.6712 2.64364233907525 2.640440963
2.8977 4.6672 2.63526419892625
2.8968 4.6893 2.60608089260809
2.8927 4.6859 2.60294445683694 2.601205648
2.889 4.6899 2.59459159309234
2.8862 4.7087 2.56076817558299
2.8949 4.7015 2.58341636222739 2.577066273
2.9004 4.707 2.58701428096978
2.9091 4.6742 2.64200328593281
2.644120472
2.9088 4.671 2.64623765747361
2.9134 4.6575 2.66905567341322
2.666630841
2.9108 4.6583 2.66420600858369

%VMA %VFA N des

11.4007925780935 79.436945176437 100
12.2627245770877 65.9579169469417 100
12.6265541859868 53.2972276276807 100
10.8152305070396 76.0194417209269 160
10.9880302987233 92.6045773677479 160
 Vma at AC optimum VFA at AC optimum
13 90
12.5 80
f(x) = − 0.9962047801901 x² + 5.7476718534374 x f(x) = 26.1397175487564 x − 25.2583148369609
12 70
%Vma

+ 4.3493816473856
11.5 60
11 50

% VFA
10.5 40
2.5 2.7 2.9 3.1 3.3 3.5 3.7 3.9 4.1 30
% Binder 20
10
0
2.5 2.7 2.9 3.1 3.3 3.5 3.7 3.9 4.1
% Binder

Superpave 25 mm Designation
Design Mixture Properties at 3.51 % Binder Content
Mix Property Result Criteria
% Air voids 4% 4%
%VMA 12.25% 12% min
%VFA 66.49% 65-75%
%Gmm at N design=100 95.89% 96% max
%Gmm at N max=160 97.40% 98% max
m

− 25.2583148369609

3.7 3.9 4.1

t
Criteria
4%
12% min
65-75%
96% max
98% max
Reduced time Temp phase angle Freq log Freq at log at Red Freq
1.9905359E-05 5 6.4 20 1.30103 2511.886 3.4 50237.72863
3.9810717E-05 5 7.4 10 1 2511.886 3.4 25118.864315
0.00039810717 5 8.2 1 0 2511.886 3.4 2511.8864315
0.00398107171 5 9.5 0.1 -1 2511.886 3.4 251.18864315
0.03981071706 5 11.5 0.01 -2 2511.886 3.4 25.118864315
0.05 20 11 20 1.30103 1 0 20
0.1 20 11 10 1 1 0 10
1 20 13.7 1 0 1 0 1
10 20 17.2 0.1 -1 1 0 0.1
100 20 20.1 0.01 -2 1 0 0.01
31.547867224 40 18.3 20 1.30103 0.001585 -2.8 0.0316978638
63.095734448 40 18.3 10 1 0.001585 -2.8 0.0158489319
630.95734448 40 23.1 1 0 0.001585 -2.8 0.0015848932
6309.5734448 40 26.6 0.1 -1 0.001585 -2.8 0.0001584893

n a
-0.0729884083 14.1158
35000

30000

25000
Dynamic modulus E*

20000
5C
20 C
15000
40C
5 to 20
10000
40 to 20 C
5000

0
0.0001 0.001 0.01 0.1 1 10 100 1000 10000 100000
Fr Frequency

30

25

20
Temp phase angle Freq log Freq at log at Red Freq
7 20 1.30103 2511.886 3.4 50237.72863
15
7 10 1 2511.886 3.4 25118.864315
7 1 0 2511.886 3.4 2511.8864315
7 0.1 -1 2511.886 3.4 10
251.18864315
7 0.01 -2 2511.886 3.4 25.118864315
20 20 1.30103 1 0 20 5

0
0.0001 0.001 0.01 0.1
 10

5
20 10 1 1 0 10
20 1 0 1 0 1 0
0.0001 0.001 0.01 0.1
20 0.1 -1 1 0 0.1
20 0.01 -2 1 0 0.01
45 20 1.30103 0.001585 -2.8 0.0316978638
45 10 1 0.001585 -2.8 0.0158489319
45 1 0 0.001585 -2.8 0.0015848932
45 0.1 -1 0.001585 -2.8 0.0001584893

35000

30000

25000

20000

15000

10000

5000

0
0.0001 0.001 0.01 0.1 1 10 100 1000 10000 100000

temperature 7 20 45 7 to 20 45 to 20

7
350

300

250

200

150

100

50

-2.5 -2 -1.5 -1 -0.5

Temp phase angle Freq log Freq at log at

5 6.4 20 1.30103 2511.886 3.4

5 7.4 10 1 2511.886 3.4
5 8.2 1 0 2511.886 3.4
5 9.5 0.1 -1 2511.886 3.4
5 11.5 0.01 -2 2511.886 3.4
20 11 20 1.30103 1 0
20 11 10 1 1 0
20 13.7 1 0 1 0
20 17.2 0.1 -1 1 0
20 20.1 0.01 -2 1 0
40 18.3 20 1.30103 1
40 18.3 10 1 1
40 23.1 1 0 1
40 26.6 0.1 -1 1

35000

30000

25000
35000

30000

25000

20000

15000

10000

5000

0
0.01 0.1 1 10
 log Red Freq E* from actual data log E* Log E* Pred Pred E* Error=e²
4.701029995664 31581 4.499426 4.49437335963 31215.72 2.55279E-05 6.4059668352
4.4 31086 4.492565 4.48275502481 30391.7 9.62325E-05 6.7383937698
3.4 27394 4.437655 4.4372208566 27366.6 1.88873E-07 7.9715870766
2.4 23426 4.369698 4.37886268278 23925.59 8.39889E-05 9.4304670653
1.4 19886 4.298547 4.30434857498 20153.41 3.36532E-05 11.156336651
1.301029995664 19504 4.290124 4.29594854144 19767.35 3.39289E-05 11.34345295
1 18197 4.26 4.26914317548 18584.17 8.36014E-05 11.932102469
0 14526 4.162146 4.16509861744 14625.09 8.71771E-06 14.115796299
-1 10771 4.032256 4.03405947535 10815.82 3.25243E-06 16.699127892
-2 7820 3.893207 3.87040163069 7419.961 0.000520074 19.755234948
-1.498970004336 9217 3.96459 3.9568461752 9054.119 5.99604E-05 18.159873428
-1.8 8307 3.919444 3.90602792485 8054.302 0.000179997 19.102249686
-2.8 4877 3.688153 3.71196650595 5151.889 0.000567095 22.598152012
-3.8 2977 3.473779 3.47454090404 2982.228 5.8075E-07 26.733839352
0.001696798

3.56E-05
0.437723
0.052172
0.004835
0.118104 35000

0.11796 30000
5C 0.868815
20 C 0.172887 25000
40C
0.250873 20000
5 to 20
40 to 20 C 0.118863
0.019635 15000
0.643605
10000
0.251851
10000 100000
0.017913 5000
3.075272
0
30
0 1E-05 0.0001 0.00
0
0
25
0
0
20 3000
log Red Freq E* from actual data log E* Log E* Pred fit 0 Error=e²
2500
4.701029995664 31581 5' 0 2000
log at

15 20' 1500
4.4 31086 0
40' 1000
3.4 27394 0 500
10 d
2.4 23426 0 0
0 5
1.4 19886 0
5 1.301029995664 19504 0

0
0.0001 0.001 0.01 0.1 1 10 100 1000 10000 100000
 d 500
10 0
0 5

5
1 18197 0
0 0 14526 0
0.0001 0.001 0.01 0.1 1 10 100 1000 10000 100000
-1 10771 0
-2 7820 0
-1.498970004336 9217 0
-1.8 8307 0
-2.8 4877 0
-3.8 2977 0
0
#VALUE!
0

00 1000 10000 100000

o 20 45 to 20

7
35000

30000

25000

20000

15000

10000

5000

0
-1.5 -1 -0.5 0 0.5 1 1.5
 E* from
Red Freq log Red Freq actual log E* Log E* Pred Pred E* Error=e²
data
50237.72863019 4.70102999566398 31581 4.49942587765 4.494373 31215.72022 2.552794E-05
25118.8643151 4.4 31086 4.49256484267 4.482755 30391.70218 9.623253E-05
2511.88643151 3.4 27394 4.43765545142 4.437221 27366.60077 1.888727E-07
251.188643151 2.4 23426 4.36969813895 4.378863 23925.59146 8.398886E-05
25.1188643151 1.4 19886 4.29854743508 4.304349 20153.41161 3.365322E-05
20 1.30102999566398 19504 4.29012368827 4.295949 19767.35407 3.392891E-05
10 1 18197 4.25999979508 4.269143 18584.17025 8.360141E-05
1 0 14526 4.16214603983 4.165099 14625.09236 8.717715E-06
0.1 -1 10771 4.03225602589 4.034059 10815.82061 3.25243E-06
0.01 -2 7820 3.89320675306 3.870402 7419.961138 0.0005200736
20 1.30102999566398 9217 3.96458958749 4.295949 19767.35407 0.1097987564
10 1 8307 3.91944421047 4.269143 18584.17025 0.1222893661
1 0 4877 3.68815275559 4.165099 14625.09236 0.2274773551
0.1 -1 2977 3.47377883465 4.034059 10815.82061 0.3139143963
0.7743690395
35000

30000

25000

20000
 35000

30000

25000

20000

15000

10000

5000

0
-3 -2 -1 0 1 2 3 4 5
1 10 100
 a= -3.570977
b= 8.210183
c= -2.792214
d= 0.26112

Chart Title
35000

30000

25000

20000

15000

10000

5000

0
1E-05 0.0001 0.001 0.01 0.1 1 10 100 1000 10000

Log at & T
3000
2500
2000
log at

1500
1000
500
0
0 5 10 15 20 25 30 35 40 45
Temperature
500
0
0 5 10 15 20 25 30 35 40 45
Temperature
3 4 5 6
fr Temp phase angle Freq time at log at reduced time tr log Red t
50237.73 5 6.4 20 0.05 2511.886 3.4 1.990535853E-05 -4.70103
25118.86 5 7.4 10 0.1 2511.886 3.4 3.981071706E-05 -4.4
2511.886 5 8.2 1 1 2511.886 3.4 0.000398107171 -3.4
251.1886 5 9.5 0.1 10 2511.886 3.4 0.003981071706 -2.4
25.11886 5 11.5 0.01 100 2511.886 3.4 0.039810717055 -1.4
20 20 11 20 0.05 1 0 0.05 -1.30103
10 20 11 10 0.1 1 0 0.1 -1
1 20 13.7 1 1 1 0 1 0
0.1 20 17.2 0.1 10 1 0 10 1
0.01 20 20.1 0.01 100 1 0 100 2
0.028251 40 18.3 20 0.05 0.001413 -2.85 35.39728921921 1.54897
0.014125 40 18.3 10 0.1 0.001413 -2.85 70.79457843841 1.85
0.001413 40 23.1 1 1 0.001413 -2.85 707.9457843841 2.85
0.000141 40 26.6 0.1 10 0.001413 -2.85 7079.457843841 3.85

Chart Title
35000

30000

25000

20000

15000

10000

5000

0
1E-05 0.0001 0.001 0.01 0.1 1 10 100 1000 10000
 E* from actual data log E* Log E* Pred Pred E* Error=e²
31581 4.4994258777
31086 4.4925648427
27394 4.4376554514
23426 4.3696981389
19886 4.2985474351
19504 4.2901236883
18197 4.2599997951
14526 4.1621460398
10771 4.0322560259
7820 3.8932067531
9217 3.9645895875
8307 3.9194442105
4877 3.6881527556
2977 3.4737788346
0 1 20.244833229
0 1 20.183138866
0 1 19.692785906
0 1 19.094261826
0 1 18.477510052
0 1 18.405161261
0 1 18.147598254
0 1 17.323459657
0 1 16.259088658
0 1 15.157058822
0 1 15.717970597
0 1 15.362042919
0 1 13.602470749
0 1 12.067139392
239.73452019
35000

30000

25000

5
20000
20
40
15000 five to 20
40 to 20
10000

5000

0
1E-05 0.0001 0.001 0.01 0.1 1 10 100 1000 10000
100 1000 10000
 Temp phase angle phase in rad Freq log at at log fr reduced frequency
0.05 5 6.4 0.1117010721 20 0 1 1.30103 20
0.1 5 7.4 0.1291543646 10 0 1 1 10
1 5 8.2 0.1431169987 1 0 1 0 1
10 5 9.5 0.1658062789 0.1 0 1 -1 0.1
100 5 11.5 0.200712864 0.01 0 1 -2 0.01
106.8981 20 11 0.1919862177 20 -3.33 0 1.30103 0.009354702825744
213.7962 20 11 0.1919862177 10 -3.33 0 1 0.004677351412872
2137.962 20 13.7 0.2391101075 1 -3.33 0 0 0.000467735141287
21379.62 20 17.2 0.3001966313 0.1 -3.33 0 -1 4.677351412872E-05
213796.2 20 20.1 0.3508111797 0.01 -3.33 0 -2 4.677351412872E-06
62946.27 40 18.3 0.3193952531 20 -6.100 8E-07 1.30103 1.5886564694486E-05
125892.5 40 18.3 0.3193952531 10 -6.100 8E-07 1 7.9432823472428E-06
1258925 40 23.1 0.4031710572 1 -6.100 8E-07 0 7.9432823472428E-07
12589254 40 26.6 0.464257581 0.1 -6.100 8E-07 -1 7.9432823472428E-08

35000
f(x) = 28671.7313035254 x^0.117971083161648
R² = 0.928501748757776
30000

25000

20000
Column K
15000 Power (Column K)

10000

5000

0
1E-08 1E-07 1E-06 1E-05 0.0001 0.001 0.01 0.1 1 10 100

E'(loss modulus)
E 31376 1 31384.13
E1 2.0078 t1 0.02 0.863 4003.73991521012
E2 2.009 t2 0.2 0.998 3907.17700992879
E3 2.0091 t3 2 1 3866.40521489223
E4 2.0091 t4 20 1 3964.63074382038
E5 0 t5 200 1 3721.53864582413
E6 0 t6 2000 1 3472.15128886699
E7 0 t7 20000 1 3440.31090974918
E8 0 t8 200000 1 3185.07140702443
E9 0 t9 2000000 1 2687.41881165952
E10 0 t10 20000000 1 2894.06846665157
E11 0 t11 200000000 1 2608.33533172123
E12 0 t12 2000000000 1 1913.42811767557
E13 0 t13 20000000000 1 1332.97880449602
E14 0 t14 2E+11 1
E15 0 t15 2E+12 1
E16 0 t16 2E+13 1
E17 0 t17 2E+14 1
E* from actual data E'(lstorage modulus) E''( loss modulus)
31581 31384.1846550108 3520.300348008
31086 30827.0897538407 4003.7399152101
27394 27113.930069488 3907.1770099288
23426 23104.7265016112 3866.4052148922
19886 19486.7826760898 3964.6307438204
19504 19145.6565859632 3721.5386458241
18197 17862.6698571971 3472.151288867
14526 14112.7225170858 3440.3109097492
10771 10289.3032384198 3185.0714070244
7820 7343.71705138063 2687.4188116595
9217 8750.85462742543 2894.0684666516
8307 7886.8774427713 2608.3353317212
4877 4485.96944243812 1913.4281176756
2977 2661.8971630708 1332.978804496

reduced frequency angular reduced frequency E' predicted error SSE

20 125.663706143592 31384.13 0
10 31384.13 749685761.2
1 31384.13 754982945.62
0.1 31384.13 757225177.35
 0.01 31384.13 751828939.46
0.009354702825744 31384.13 765218960.43
0.004677351412872 31384.13 779078555.57
0.000467735141287 31384.13 780857025.35
4.677351412872E-05 31384.13 795186905.53
4.677351412872E-06 31384.13 823501233
1.588656469449E-05 31384.13 811683606.17
7.943282347243E-06 31384.13 828046358.79
7.943282347243E-07 31384.13 868522269.44
7.943282347243E-08 31384.13 903071688.18

0.985520362 10368889426

0.010000;
0.071969; 0.517947; 3.727594; 26.82696; 193.069773; 1389.495494; 10000.000000
0

0
Temp phase angle Freq log Freq at log at Red Freq log Red Freq

-7.3 0 10 1 398107.170553 5.6 3981071.71 6.6

-7.3 0 5 0.698970004336 398107.170553 5.6 1990535.85 6.29897000434
-7.3 0 1 0 398107.170553 5.6 398107.171 5.6
-7.3 0 0.5 -0.30102999566 398107.170553 5.6 199053.585 5.29897000434
-7.3 0.1 -1 398107.170553 5.6 39810.7171 4.6
-7.3 0 0.01 -2 398107.170553 5.6 3981.07171 3.6
10.5 0 10 1 120.226443462 2.08 1202.26443 3.08
10.5 0 5 0.698970004336 120.226443462 2.08 601.132217 2.77897000434
10.5 0 1 0 120.226443462 2.08 120.226443 2.08
10.5 0 0.5 -0.30102999566 120.226443462 2.08 60.1132217 1.77897000434
10.5 0.1 -1 120.226443462 2.08 12.0226443 1.08
10.5 0 0.01 -2 120.226443462 2.08 1.20226443 0.08
24.6 0 20 1.301029995664 1 0 20 1.30102999566
24.6 0 10 1 1 0 10 1
24.6 5 0.698970004336 1 0 5 0.69897000434
24.6 0 1 0 1 0 1 0
24.6 0 0.5 -0.30102999566 1 0 0.5 -0.3010299957
24.6 0 0.1 -1 1 0 0.1 -1
41.1 0 20 1.301029995664 0.01584893192 -1.8 0.31697864 -0.4989700043
41.1 0 10 1 0.01584893192 -1.8 0.15848932 -0.8
41.1 0 5 0.698970004336 0.01584893192 -1.8 0.07924466 -1.1010299957
41.1 0 1 0 0.01584893192 -1.8 0.01584893 -1.8
41.1 0 0.5 -0.30102999566 0.01584893192 -1.8 0.00792447 -2.1010299957
41.1 0 0.1 -1 0.01584893192 -1.8 0.00158489 -2.8

40000
35000
30000
25000
20000
15000
E*

x y
-7.3 5.6 10000
10.5 2.08 5000
24.6 0 0
1 01 1 1 10 0 00 0 00 00
41.1 -1.8 00 0. 0. 10 00
0. 10 10 000 000 0
1 10 000
1

Frequency HZ
 00 0.
0 0. 1 10 0 00 0 00
0. 10 10 00 00 0
10 10 00
10

Frequency HZ
 E* from
actual log E* Log E* Pred Pred E* Error=e²
data
35628.9 4.5518 4.5501814007 35496.16 2.627685E-06
34802.1 4.54161 4.5380011376 34514.46 1.299107E-05
Chart Title
31978.9 4.50486 4.5033762395 31869.57 2.212006E-06 40000
30553.9 4.48507 4.4852697122 30568.19 4.123309E-08 a= 1.600088
35000
27195.5 4.4345 4.4342143152 27177.8 7.993777E-08 b= 2.284056
22307.1 4.34844 4.3340397102 21579.42 0.000207458 30000c= 0.751037
17858.2 4.25184 4.2664424268 18468.96 0.0002132986 d= 1.251974
16072.1 4.20607 4.221725002 16661.92 0.0002449969 25000e 0.43056
12252.7 4.08823 4.1005916207 12606.42 0.0001527652 f= 1.390769
20000
10693.2 4.02911 4.0405468475 10978.6 0.0001308543
7590.73 3.88028 3.8822502153 7625.182 3.867796E-06 15000
4342.67 3.63776 3.6120321321 4092.909 0.00066176
8820.7 3.9455 3.9351560494 8613.032 0.0001070605 10000
7506.3 3.87543 3.8624618669 7285.542 0.0001680666
5000
6227.5 3.79431 3.7850283021 6095.766 8.621929E-05
3915.5 3.59279 3.5884490962 3876.583 1.881939E-05 0
3125 3.49485 3.4975452149 3144.454 7.264067E-06 0.001 0.01 0.1 1 10 100

1792.7 3.25351 3.2762011235 1888.866 0.0005149952

2725.1 3.43538 3.4361168262 2729.712 5.393177E-07
2245.4 3.35129 3.3406637483 2191.108 0.0001129963
1689.3 3.22771 3.2434065493 1751.486 0.0002464827
1013.8 3.00595 3.0150329907 1035.221 8.245918E-05
834.2 2.92127 2.91754044 827.0665 1.3911E-05
510 2.70757 2.698857082 499.87 7.591801E-05
0.0030676842

at vs temp
7
6
5 f(x) = 0.00142215177401 x² − 0.200685051044914 x + 4.0529
-7.3 R² = 0.999962360614284
10.5 4
41.1 3
24.6 2
41.1 to 24.6
10.5 to 24.6 1
-7.3 to 24.6 0
00 0 00 00 00
10 00 00 00 00 -1
10 10 0 00
10 10 -2

Z -3
-10 0 10 20 30
 0 00 0 00 00
10 10 00 00 00
-1
10 10 0
10 -2

Z -3
-10 0 10 20 30
 Chart Title

wrong
40000

35000

30000

25000

20000
1 1 10 100 1000 10000 100000 1000000 10000000
15000

10000

5000

0
-4 -2 0 2 4

at vs temp

7401 x² − 0.200685051044914 x + 4.05291973753468

4284

10 20 30 40 50
10 20 30 40 50
wrong

2 4 6 8
 Temp phase angle phase in rad Freq W log at at
5.000 6.400 0.112 20.000 125.664 0 1
5.000 7.400 0.129 10.000 62.832 0 1
5.000 8.200 0.143 1.000 6.283 0 1
5.000 9.500 0.166 0.100 0.628 0 1
5.000 11.500 0.201 0.010 0.063 0 1
20.000 11.000 0.192 20.000 125.664 -3.4 0.0003981072
20.000 11.000 0.192 10.000 62.832 -3.4 0.0003981072
20.000 13.700 0.239 1.000 6.283 -3.4 0.0003981072
20.000 17.200 0.300 0.100 0.628 -3.4 0.0003981072
20.000 20.100 0.351 0.010 0.063 -3.4 0.0003981072
40.000 18.300 0.319 20.000 125.664 -6.2 6.309573E-07
40.000 18.300 0.319 10.000 62.832 -6.2 6.309573E-07
40.000 23.100 0.403 1.000 6.283 -6.2 6.309573E-07
40.000 26.600 0.464 0.100 0.628 -6.2 6.309573E-07

35000

30000 f(x) = 1533.47790888988 ln(x) + 26589.9434874124

R² = 0.99544234589425

25000

20000

15000

10000

5000

0
1E-08 1E-07 1E-06 1E-05 0.0001 0.001 0.01 0.1 1 10 100
 log fr reduced frequency Wr E* from actual data E'(lstorage modulus)
1.3010299957 20 125.663706143592 31581.000 31384.1846550108
1 10 62.8318530717959 31086.000 30827.0897538407
0 1 6.28318530717959 27394.000 27113.930069488
-1 0.1 0.628318530717959 23426.000 23104.7265016112
-2 0.01 0.062831853071796 19886.000 19486.7826760898
-2.098970004 0.00796214341107 0.050027622494092 19504.000 19145.6565859632
-2.4 0.003981071705535 0.025013811247046 18197.000 17862.6698571971
-3.4 0.000398107170553 0.002501381124705 14526.000 14112.7225170858
-4.4 3.981071705535E-05 0.00025013811247 10771.000 10289.3032384198
-5.4 3.981071705535E-06 2.5013811247046E-05 7820.000 7343.71705138063
-4.898970004 1.2619146889604E-05 7.92884383259E-05 9217.000 8750.85462742543
-5.2 6.3095734448019E-06 3.964421916295E-05 8307.000 7886.8774427713
-6.2 6.3095734448019E-07 3.964421916295E-06 4877.000 4485.96944243812
-7.2 6.3095734448019E-08 3.964421916295E-07 2977.000 2661.8971630708
 log E' Predicted logE' Predicted E' Error^2 n λ E(t/) tr
4.4967108504 4.4878637804154 30751.321262 7.827E-05 0 1 30751.32 0.05
4.4889325269 4.4768522628315 29981.424452 0.000146 0.036579 1.020796 29370.62 0.1
4.4331924716 4.4328182761981 27090.578314 1.4E-07 0.044034 1.024959 26430.88 1
4.363700832 4.3747825806141 23701.868299 0.000123 0.058036 1.032713 22951.06 10
4.2897401418 4.2988405439217 19899.425752 8.282E-05 0.075942 1.04251 19087.99 100
4.2820702647 4.2901812844967 19506.586796 6.579E-05 0.087494 1.048762 18599.64 125.5943
4.2519463716 4.2624411793776 18299.582409 0.00011 0.092151 1.051267 17407.16 251.1886
4.1496108026 4.1535801770712 14242.30156 1.576E-05 0.108861 1.060191 13433.71 2511.886
4.0123859666 4.0149704489339 10350.71734 6.68E-06 0.13861 1.075834 9621.111 25118.86
3.8659159354 3.8414702697826 6941.7707925 0.000598 0.1735 1.093819 6346.364 251188.6
3.9420504692 3.9330569528357 8571.5024347 8.088E-05 0.182797 1.098551 7802.553 79244.66
3.8969050922 3.8791852404088 7571.5577718 0.000314 0.178958 1.0966 6904.578 158489.3
3.6518563109 3.6746666288243 4727.8820008 0.00052 0.204519 1.10952 4261.194 1584893
3.4251912734 3.4291439911157 2686.234924 1.562E-05 0.245523 1.129929 2377.347 15848932
0.002157

δ 4.608499
α -4.866673
β 3.284729
γ -0.297889
 E(t)
35000

30000

25000

20000

15000

10000

5000

0
01 0.
1 1 10 10
0 00 00
0 00 00 00 00
0. 10 00 00 00 00
10 10 0 0 0
10 10
0 00
10

log fr log E'

1.30103 4.496711 4.981315
1 4.488933 4.980411 SUMMARY OUTPUT
0 4.433192 4.973931
-1 4.363701 4.965853 Regression Statistics
-2 4.28974 4.957256 Multiple R 0.963242
-2.09897 4.28207 4.956364 R Square 0.927836
-2.4 4.251946 4.952863 Adjusted R 0.921822
-3.4 4.149611 4.940967 Standard E 0.090673
-4.4 4.012386 4.925015 Observatio 14
-5.4 3.865916 4.907989
-4.89897 3.94205 4.916839 ANOVA
-5.2 3.896905 4.911592 df SS MS F
-6.2 3.651856 4.883106 Regression 1 1.268498 1.268498 154.2869
-7.2 3.425191 4.856758 Residual 12 0.09866 0.008222
Total 13 1.367158

Coefficients
Standard Error t Stat P-value
Intercept 4.458603 0.037035 120.3876 7.235E-20
X Variable 0.116243 0.009358 12.42123 3.29E-08
Significance F
3.29E-08

Lower 95%Upper 95%Lower 95.0%

Upper 95.0%
4.37791 4.539296 4.37791 4.539296
0.095853 0.136633 0.095853 0.136633