Certificate of Analysis

Product Name: Caffeine Natural Coffee Bean

(Caffeine Anhydrous Natural)
CAS# 58-08-2
Extraction Solvent(s): methylene chloride
Country of Origin: India
Batch Number: 031018
Manufacture Date: October 1, 2018
Test Date: March 22, 2019
Retest Date: September 1, 2023
Test Results Obtained by PureBulk
ITEMS SPECIFICATIONS RESULTS
Caffeine (HPLC) ≥98.5% & ≤101% on anhydrous basis 100.62%
Aerobic Plate Count <100 cfu/g Not Detected
Yeast & Mold <10 cfu/g Not Detected
Coliforms Report Only Not Detected
E. Coli Negative Absent
Salmonella Negative Absent
Staph aureus Negative Absent
Pseudo. aeruginosa Negative Absent
Conclusion (PureBulk): This product conforms to standards

The following information is an indirect translation of information provided from the Manufacturer's Certificate of Analysis, and
should not be used solely as an instrument for strict quality control.
ITEMS SPECIFICATIONS RESULTS
Description A white crystalline powder; sublimes readily White crystalline powder; sublimes readily
Odor No odor Conforms
Solubility Sparingly soluble in water, freely soluble in Passes test
boiling water, slightly soluble in ethanol and
in ether. It dissolves in concentrated
solutions of alkali benzoates or salicylates.
Identification A By IR absorption identical with Std. Passes test
Identification B To Comply Passes test
Water Losses ≤0.5% 0.35%
Melting Range Bet. 235°-237.5°C after drying at 80°C for 4 Passes test
hours
Residue on Ignition ≤0.1% Passes test
Arsenic ≤3 ppm NIL
Heavy Metals ≤0.001% Passes test
Readily Carbonizable Substances The solution has no more color than Passes test
matching Fluid D.
Residual Solvents To Comply Passes test
Other Alkaloids No PPT is formed. Passes test
Chromatographic Purity: ≤0.1% Complies
Any individual impurity
Total Impurity ≤0.1% Complies
Conclusion (Manufacturer): This product conforms to enterprise standards
GMO Statement Non-GMO
Storage Conditions: Keep in sealed container under 25°C.
Keep away from strong light, heat and moisture.

Purebulk.Inc verifies that the information contained herein is true and correct to the best of our knowledge.
Verified By: Candace Gibson / Brenda Bristow
( This document was produced electronically and is valid without signature. )

Purebulk Inc., store@purebulk.com Ph: 1-541-679-1500 • Toll Free: 1-888-280-0050

1640 Austin Rd, Roseburg, OR, USA 97471 Fax: 1-541-393-9005