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Portland Cement Concrete Material Characterization for Pavement ME Design Implementation in Idaho View project
All content following this page was uploaded by Somayeh Nassiri on 17 March 2018.
Authors:
Affiliation Statements:
Harry Rodin III: MS student, Civil and Environmental Engineering Department, Washington State
University
Milena Rangelov: PhD Candidate, Civil and Environmental Engineering Department, Washington State
University
Somayeh Nassiri: PhD, Associate Research Professor, Civil and Environmental Engineering Department,
Karl Englund: PhD, Associate Research Professor, Civil and Environmental Engineering Department,
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Abstract
Cured Carbon Fiber Composite Material (CCFCM) is available from manufacturing lines; however, excess
CCFCM has no reuse applications at present. Post-industrial CCFCM was mechanically refined and used
as reinforcement to improve the mechanical properties of pervious concrete (PC). Four PC mixtures were
included in the study, which contained zero (control), three, four, and five percent CCFCM by volume.
Infiltration rate of all CCFCM-mixtures were above the acceptable level of 1,200 cm/h. Paired t-tests
showed that all CCFCM mixtures significantly outperformed the control mixture in terms of split tensile
strength by 57-84% and flexural strength by 36-65% in 28-day testing. Load-displacement curves of
CCFCM-mixtures indicated increases of 41-54% in toughness indices. Mass loss due to Los Angeles
Machine abrasion (Cantabro) ranged 16-31% for CCFCM mixtures, while the control lost 50% of its
original mass. Overall, within the tested range, up to four percent CCFCM addition to PC presented the
optimal result across the entire experimental scope higher CCFCM contents may be possible if used as a
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Introduction
Pervious concrete pavements allow free draindown of rain and snowmelt through the slab, facilitating
stormwater management, especially in areas with high rain volume. Free draindown of runoff is made
possible by designing pervious concrete (PC) slabs to withhold 15-35 percent porosity. permeable pore
system is created by using narrow-graded coarse aggregate sized 9-19 mm, and by eliminating (minimizing)
the fine aggregate content (ACI, 2010). Pore volume fraction (porosity), pore size, and pore tortuosity
influence the hydraulic and mechanical properties of PC, causing decreases in strength compared to
conventional portland cement concrete (PCC) (Rehder et al. 2014, ACI, 2010). PC strength is also reduced
by the weak contact links between the coarse aggregate, cement, and fibers (if used) (Hesami et al. 2014),
which can result in excess abrasion and raveling under traffic loading (Dong et al. 2013). The combination
of these factors creates a popcorn-like mixture with reduced paste surface area to bind the aggregate, leaving
weak areas in the PC and lower compressive strengths (around 2,500 psi) compared to PCC (Tennis et al.
2004). The addition of reinforcing elements to PC can improve the mechanical properties, such as flexural
and tensile strength, by bridging the voids and holding the matrix together, while keeping the free drainage
ability of PC (Rangelov et al. 2016). Fibers also increase abrasion and raveling resistance in PC via the
“bird-nest” effect that helps mitigate over-compaction and clogging (Eisenberg et al. 2015).
Polypropylene fibers commonly used in PCC have been the most used in PC, as well. However, researchers
cautioned that polypropylene fibers may not bond well in PC due to the low paste content, and are therefore
likely to decrease strength (Wang et al. 2006 & Joung and Grasley 2008). Increasing the cement content
seems to alleviate this problem, as modified PC mixtures with polypropylene fiber reinforcement showed
improvement in split tensile strength and freeze-thaw durability (Wang et al. 2006 & Yang 2011). In
addition to improved strength and durability, the use of polypropylene fibers in PC may enhance resistance
to impact loading, and decrease brittle failure in PC that is caused by the porous matrix (Huang et al. 2010
and Wu et al. 2011). Researchers also alerted against poor dispersion of polypropylene fibers throughout
the mixture, which can lead to reduced strength (Wu et al. 2011). Negligible improvements in mechanical
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properties of PC with latex and polypropylene fibers was attributed to a poor fiber dispersion (Huang et al.
2010). When incorporating fibers in PC, attention should be paid to maintaining the hydraulic performance,
as the infiltration rate (I) may decline with increased volume of fibers (Kevern et al. 2014).
In the present study, fiber-like reinforcing elements produced by mechanical refining of aerospace
industry’s cured carbon fiber composite materials (CCFCM) was used to improve PC’s mechanical
properties. Composite materials, such as CCFCM, have become economically competitive for
manufacturing of high-performance products (Das et al. 2016). Therefore, the global demand for composite
materials has accelerated, yielding an increased amount of excess high-valued materials from manufacturers
in aerospace, automotive, and sports industry that urgently need a viable reuse application (Ribeiro et al.
2016). This study examines a reuse option for the excess CCFCM from aerospace industry. The fiber-
shaped CCFCM reinforcing elements used in the present study are composite materials that include carbon
fibers embedded in the epoxy matrix, rather than individual strands of carbon, metal, synthetic, and natural
fibers commonly used in PCC or PC. However, due to their high modulus and flexibility, CCFCM
reinforcement is expected to behave closer to steel fibers than the other fiber types. The review of literature
on the performance of PC reinforced with steel fibers revealed that steel fibers incorporated in PC at 0.5
percent by volume resulted in increases in compressive, split tensile and flexural strengths for three different
water-to-cement ratios (Hesami et. al 2014). Hooked steel fibers are typically implemented in PCC slabs,
beams and columns (Sujivorakul 2012). The 2012-study showed that hooked steel fibers increase ductility
and tensile strength of PCC for fiber volume contents 0.25-1.5 percent. In all mixtures, the first-peak and
post-cracking tensile strength increased as the fiber content increased (Sujivorakul 2012). Concrete
reinforced with hooked steel fibers at one and two percent by volume was tested for tensile stress-strain
comparisons (Kim et al. 2012). The two-percent fiber content outperformed the one-percent by bearing
higher tensile stresses at the same strain values, as well as greater post-cracking strength. Steel fibers were
implemented in PCC mixtures designed for two different 𝑓𝑓′𝑐𝑐 containing 0.5-1.5 percent volume fiber
content. The addition of fibers introduced improvements in 28-day strengths for all fiber-reinforced
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mixtures compared to the control except for 𝑓𝑓′𝑡𝑡 of 0.5 percent. The increase of fiber content introduced
enhanced post-peak behavior; however, reduced the workability of the fresh mixture (van Zijl and Zeranka
2012). An optimized content of fibers is beneficial for improving ductility and strength properties to a
desired extent, while not compromising the mixtures’ workability (Mihashi and Ishikawa 2012). Post-peak
performance of 0.5-3.0 percent by volume waste-metallic fibers in PCC was evaluated by comparing the
toughness indices estimated according to the American Society for Testing and Materials (ASTM) C1018
(Meddah and Bencheikh 2009). Smaller fibers at higher contents yielded higher toughness indices,
indicating a more ductile response; however prior to the first peak, the fibers had minor effect on the
performance.
Scope of Work
Based on the above literature review, it is hypothesized that the addition of a proper amount of CCFCM to
PC will result in improved split tensile and flexural strengths, with negligible improvements or even
possible reductions in compressive strengths and hydraulic performance compared to the plain PC. Post-
peak loading performance is also expected to increase along with improved ductility of the reinforced
specimens. To test this hypothesis, four CCFCM-reinforced PC (CrPC) were evaluated against a control
- Mechanical performance: 7- and 28-day indirect split tensile, modulus of rupture, compressive
The control mixture was designed to withhold a target porosity (Φ) of 25 percent, using crushed basalt
coarse aggregate with a 9.5-mm nominal maximum grain size (Fig. 2). CCFCM was mechanically ground
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and screened to produce fiber-shaped particles that passed Screen 10 (2 mm) and retained on Screen 20
(0.841 mm) (Fig. 1). The particle size distribution for the refined CCFCM is presented in Fig. 2.
Mechanically refined CCFCM was incorporated in three CrPC mixtures at three, four, and five percent
During mixing, CCFCM was added into the mixer in a dry state, simultaneously with the cement and water.
CCFCM particles uniformly distributed in the fresh mixture, especially when mixing CrPC3. At higher
CCFCM contents, CCFCM formed spherical clusters around the aggregate grains, which were
mechanically disintegrated during mixing. Upon discharge, the fresh density of PC (D) was experimentally
determined (ASTM C1688). The experimentally determined D was used to determine the exact mass of the
fresh PC needed to cast each specimen type. Three specimen types were cast: small cylinders (100 by 200
mm), large cylinders (150 by 300 mm) and 100 by 100 by 350-mm beams. Currently no standardized test
procedures are approved for casting and compaction of PC cylinders and beams; because of this, methods
were adopted to receive uniform compaction throughout the specimen, while reproducing experimental
fresh density. The pre-determined amount of fresh PC was divided into two equal lifts for the 100-mm
cylinders and prisms, and three lifts for the 150-mm cylinders. Each lift was compacted using the standard
Proctor Hammer, while the number of blows was adjusted so that the pre-determined amount of the fresh
PC fits in the mold. Moreover, a sufficient number of strikes of the mallet to the sides of the molds were
applied to prevent the formation of undesired air pockets in the interior of the specimens and to ease the
compaction and placement of the total pre-weighed material in the molds. Small cylinders were compacted
using solely strokes of the mallet on the sides of the molds to prevent the over compaction. The specimens
were finished by applying a float on the surface and were cured in the laboratory conditions while covered
by lids or plastic wrap. Fig. 3 shows a 100-mm cylinder from each mixture type for comparison after the
curing period.
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Specimens were demolded at 7-day age and tested to obtain Φ, hardened density (ρ) and infiltration rate.
Porosity and ρ were determined on all specimens, by taking the specimens’ dimensions, as the average of
a minimum of two caliper measurements, to calculate the volume (V). The mass of dry specimens (Md),
and the mass of the submerged specimen (Mw) are then used to determine Φ per Eq. 1 (ASTM C1754):
(Md - Mw )
ϕ = [1- ] ( 1)
ρw * V
where, ρw is the density of water. Hardened density was estimated as the ratio of the specimen’s dry mass
to its volume. Infiltration tests were performed on cylindrical specimens per the modified respective ASTM
procedure (ASTM C1701). The specimens were enclosed on the sides by shrink wrap to prevent the lateral
loss of water. Infiltration tests were run with 1 and 2 liters of water for the 100- and 150-mm cylinders,
respectively. The time during which the designated volume of water (Vw) permeates through the specimen
(t) was recorded and used to calculate the infiltration per Eq. 2:
4Vw
I= ( 2)
R 2π t
where, R stands for the diameter of each specimen, determined as a part of the Φ characterization procedure
described previously.
Mechanical tests were performed on specimens on two test ages: 7- and 28-day age in accordance with the
respective ASTM procedure for conventional PCC. It is noteworthy that currently a standardized test
procedure for mechanical testing of PC is lacking. Hence, the loading rates recommended for PCC were
adjusted for PC to allow for a no-shock and gradual loading during a test period of about 4-5 minutes per
specimen. Split tensile strength tests were performed on 150-mm cylinders at a loading rate of 890-980
N/sec (ASTM C496). Flexural strengths were determined for simple beams in center loading test setup and
at loading rate 0.15 mm/min (ASTM C293). Compressive strength test was performed on 100-mm
cylinders, using loading rate 0.10-0.14 MPa/sec (ASTM C39). Abrasion resistance using a Los Angeles
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Machine (Cantabro test) was conducted on the two halves of 100-mm cylinders on 30-day age (ASTM
C1747). The specimens were placed in the steel drum of the abrasion machine without the steel ball charges
and subjected to a total of 500 rotation cycles. The drum was discharged after every 50 cycles and the mass
Overall, the average Φ ranged from 23.6 to 27.1 percent for all specimens from all mixtures, which agrees
well with the target Φ at 25 percent. As seen in Fig. 4, the prisms are the specimen type with the highest Φ
for all mixtures, except CrPC3, which may be due to the difficulty of placing the PC in the corners of the
beam molds. The 150-mm cylinders demonstrated the lowest Φ for every mixture, except CrPC0, most
likely due to the three-lift, as opposed to the two-lift compaction used for 100-mm cylinders and beams.
Fig. 5 presents the Φ-ρ relationship for all cast specimens. Strong negative linear Φ-ρ relations are evident
for all four mixtures (R2 values ranging 0.92-0.99). Fig. 5 also indicates that for the same value of Φ, the
control mixture has the highest ρ (the heaviest mixture), followed by CrPC3, CrPC4 and CrPC5,
respectively. The trends in Fig. 5 indicate that the addition of CCFCM to PC has a weight lightening effect
on the mixture. As seen in Fig. 5, CrPC mixtures display a wider range of Φ among the specimens compared
to the control. Further, CrPC3 and CrPC5 resulted in several prisms and 100-mm cylinders with Φ beyond
28 percent implying that higher contents of CCFCM may hinder proper compaction. This problem may be
Infiltration Rate
Kevern et al. (2014) found that I decrease as higher volumes of fibers are implemented in PC. In the present
study too, CrPC mixtures generally demonstrate lower I comparing to the control mixture. Fig. 6 shows
that I for all specimens range 1,270-3,556 cm/h, which is within the typical range for PC reported in the
literature: 508-7,620 cm/h (Eisenberg et al. 2015). The addition of CCFCM decreases I of 150-mm
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cylinders, with CrPC4 exhibiting the lowest infiltration rate. In terms of 100-mm cylinders, an increase in
I is seen for CrPC3, while CrPC4 and CrPC5 show decreases in infiltration. As seen earlier in Fig. 4, 100-
mm cylinders from CrPC3 had the highest Φ of all cylinders, which is likely the reason for the high I relative
to CrPC4 and CrPC5. Therefore, the effect of CCFCM addition on I can be best investigated in comparison
to porosity.
Fig. 7 presents the Φ-I relations for all the tested specimens. A distinct direct linear Φ-I relationship with
comparable slopes are established for CrPC0 and CrPC3. However, at higher CCFCM contents (CrPC4 and
CrPC5), the slope of the Φ-I line is more gradual, which indicates almost constant levels of I over the range
of porosity. This behavior points to the effect of the CCFCM additions in perhaps disturbing the
connectivity of the voids. Mixtures with lower values of I are typically more prone to clogging, which
results in reduced serviceability. To mitigate this problem, for PC mixture designs that yield low I rates, it
is suggested to use CCFCM as a replacement of coarse aggregate rather than an additive to achieve higher
Indirect split tensile strength (f’t) was determined for five 150-mm cylinders per mixture, both on 7- and
28-days (Fig. 8). The addition of CCFCM to PC increased f’t of all CrPCs. Comparing to control, CrPC3,
4, and 5 increased in 7-day f’t by 65, 57 and 44 percent and 57, 84 and 57 percent on 28-day test. CrPC3
has the highest f’t among the CrPC mixtures at 7-day age. On 28-day test, CrPC4 outperforms all the
mixtures, which is most likely due to the CrPC4’s lower average porosity than the other mixtures. Limited
studies established f’t for PC; a 0.57-1.72 MPa range was found in the literature for plain PC on 28-day age
(Hesami et al. 2014, Ibrahim et al. 2014), depending on the mixture design and targeted porosity. Near-2.1
MPa 28-day average f’t obtained for CrPC in this study exceeds the upper bound reported in the literature.
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Flexural Strength
Flexural strength indicated by the modulus of rupture (MR) is a critical property for pavement applications
because bending is the primary mode of loading in pavement structures. Any improvements to MR are
expected to directly result in an extended fatigue life for an in-service concrete pavement. MR was
characterized for three beams from each mixture at both 7 and 28-day age (Fig. 9). The addition of CCFCM
in 3, 4 and 5 percent volumetric contents increased the 7-day MR compared to the control by 84, 69, and
57 percent, respectively. For 28-day tests, MR increased by 36, 65 and 41 percent for CrPC3, 4 and 5,
respectively. CrPC3 and CrPC4 show the greatest increase in MR among all CrPC mixtures for 7- and 28-
day ages, respectively. CrPC mixtures also demonstrate lower variations in MR comparing to the CRPC0
(smaller error bars in Fig. 9). Flexural test results for PC are scarce in the literature; two studies reported
28-day MR of 0.95 and 2.21 MPa (Hesami et al. 2014, Ibrahim et al. 2014), which are outperformed by the
The addition of fibers is generally expected to have the most positive influence on the toughness and post-
peak loading behavior of the PCC (Meddah and Bencheikh 2009). Post-cracking behavior of PCC has been
shown to increase due to the implementation of steel fibers (Kim et al. 2012). Load-displacement curves
were recorded during MR testing for all specimens. Fig. 10 (a) displays the curves for one representative
beam from each mixture during 28-day testing to compare their behavior to that of the control. Fig. 10 (a)
shows the control presents a brittle failure at the peak load, indicated by an abrupt drop in the load followed
by a slight residual load bearing. On the contrary, CrPC mixtures demonstrate a ductile behavior with a
more gradual decline past the post peak-load, presenting higher post-peak residual strength.
According to ASTM C1018, four incremental areas under the load-deflection curve bound between 1, 3,
5.5 and 10.5 times the first-crack deflection are calculated. These areas under the curve are used to calculate
toughness indices I5, I10 and I20, which provide indications of the post peak-load behavior, with higher
toughness index values corresponding to more residual loading capacity. The outlined procedure for PCC
needs to be modified to account for the PC’s less ductile failure comparing to PCC, typically occurring well
10
before 3δp is reached. Fig. 10 (b) illustrates the modified procedure for PC toughness index (I2) calculation
adopted in this study. In this procedure, the total area under the load-deflection curve (A+B) is defined as
the area up to two times the peak-load (2δp), instead of three times, as recommended for PCC. A respective
toughness index, I2 is then estimated as the ratio of the total area to the area under the curve limited to the
peak load (A). The specimens with more desirable residual loading capacity present more gradual drop of
post-peak loading, which manifests in higher values of I2.Note that for the control the curve was extended
with the dotted line to continue the data trend that would have brought the specimen to the zero-load point.
The average I2 values for each CrPC mixture is listed in Table 2. CrPC mixtures demonstrate higher values
of I2 comparing to CrPC0 at both test ages, which indicates their enhanced toughness and residual loading
capacity. The addition of steel fibers increased ductility of conventional PCC (Sujivorakul 2012), which
can be related to the post-peak behavior analyzed by comparing toughness index values in the current study.
Based on the obtained results, the addition of CCFCM yields improvement in post-peak loading, resulting
in greater areas under the curve and higher toughness. Experiments performed by van Zijl and Zeranka
(2012) also showed enhanced post-peak behavior when introducing steel fibers to PCC. Mixture CrPC5
shows the highest I2 on both test days. On 7-day test CrPC3 and CrPC4 demonstrate comparable values of
I2, while 28-day results suggest that higher CCFCM content results in higher toughness.
Compressive Strength
Addition of fibers is most influential on tensile and flexural strengths and is not expected to influence the
compressive strengths (f’c) of the PC (Rehder et al. 2014, Meddah and Bencheikh 2009). Five specimens
from each mixture were tested on 7- and 28-day f’c (Fig. 11). The f’c of CrPC3 and CrPC4 can be
characterized as comparable to that of CrPC0. CrPC5 demonstrates a decrease in f’c by 22.5 and 14.5 percent
comparing to CrPC0 on 7- and 28-day tests, respectively. Based on the literature, the average 28-day f’c of
plain PC was reported to range 3.45-12.4 MPa (Hesami et al. 2014, Ibrahim et al. 2014). The results from
Fig. 11 indicate that f’c of all the tested mixtures resides within this range, indicating that the addition of
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In order to evaluate the significance of the CCFCM additions on all mechanical properties, Pearson’s two-
sample t-test at 95 percent confidence interval was performed, aiming to compare the mechanical properties
of CrPC mixtures to that of the control mixture (Table 3). For 7- and 28-day f’t, p-values are lower than
0.05, which indicates that the improvements introduced by CCFCM are significant. Similarly, CrPCs show
a statistically significant enhancement in MR on both tests dates. The only exception is the 28-day MR of
CrPC5, however, the p-value of 0.078 indicates a significance at a lower confidence interval of 10 percent.
Conversely, relatively high p-values for f’c in Table 3 suggest that CrPC mixtures had comparable values
of f’c comparing to the control, with CrPC5 as an exception, which showed a significant drop in compressive
strength.
Cantabro Test
Cantabro tests were performed for a total of 500 cycles, while the specimens were weighed for the mass
loss after every 50 cycles. The tests were performed on four halves (two tops and two bottoms) of 100-mm
cylinders from each mixture. The average percent mass loss was calculated and is presented in Fig. 12 for
the tops (a) and bottoms (b) of 100-mm cylinders from each mixture. The bottom control specimens both
failed at 350 cycles. As seen in Fig. 12, CrPCs outperformed the control on Cantabro test. CrPC4
demonstrates a substantial improvement comparing to CrPC0, with the final mass loss of 16 and 25 percent
for the tops and bottoms, respectively. CrPC4 specimens had comparable Φ but showed substantially higher
resistance against impact loading compared to the control. The specimens from CrPC3 and CrPC5
Conclusions
The objective of this experimental study was to improve the physical, hydraulic and mechanical properties
of pervious concrete (PC) using Cured Carbon Fiber Composite Material (CCFCM) as a reinforcement
(CrPC). CCFCM fiber-like elements were implemented at zero, three, four, and five percent by volume
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content in the PC (CrPC0, CrPC3, CrPC4, and CrPC5) to assess the impact of different CCFCM contents
on PC properties. Based on the experimental results, the following conclusions can be drawn:
• Dispersion of CCFCM particles was uniform in CrPC3. However, at higher CCFCM contents,
namely four and five percent, the CCFCM elements clustered into spheres around the aggregate
grains, which had to be deliberately disintegrated during the mixing process. Future work will look
into alternative mixing methods other than the rotary drum mixer, and the use of admixtures that
can help mitigate the formation of spherical clusters and maintain the workability and uniformity
of fresh PC mixture.
• CrPC mixtures presented comparable porosity to that of the control mixture, as well as the target
porosity. The combination of Proctor hammer and mallet strikes delivered relatively uniform
compaction for CrPC mixtures, resulting in consistent porosity values. At the same porosity level,
CrPC0 showed the highest density followed by CrPC3, 4 and 5, respectively. The results suggest
• The addition of CCFCM generally reduced the infiltration rate (I), with the exception of 100-mm
cylinders from CrPC3, which may be due to the relatively high porosity of this specimen group.
CrPC4 and 5 showed lower I compared to the control, while also showing less correlation between
porosity and infiltration than CrPC3. For mixtures with low porosity and I, CCFCM added as a
replacement of coarse aggregate rather than an additional constituent can help maintain the
• CrPC mixtures outperformed the control in terms of split tensile strength (f’t) on both 7- and 28-
day test dates and the enhancements were statistically significant. At 7-day age CrPC mixtures
demonstrated improvements ranged 44-65 percent and on 28-day test f’t increased by 57-84 percent.
CrPC3 and CrPC4 showed the highest f’t at 7-day and 28-day age, respectively.
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• The addition of CCFCM resulted in statistically significant improvements in modulus of rupture
(MR) on both 7- and 28-day tests, ranging 57-84 and 36-65 percent in comparison to the control.
CrPC3 and CrPC4 had the highest MR for 7- and 28-day, respectively.
• In addition to the improvements in MR, CCFCM enhanced the toughness of the PC and the post-
peak load bearing indicated by all CrPC mixtures’ higher toughness index values.
• The compressive strength (f’c) of CrPC mixtures were comparable to that of the control, except for
CrPC5, which demonstrated significantly lower f’c than the control. Based on literature, this type
• In Cantabro testing, the mass loss for CrPCs’ cylinder tops ranged 16-31 percent compared to the
50-percent of the control; with CrPC4 having the lowest mass loss of 16 percent. The CrPC bottom
specimens ranged 25-63 percent compared to the 66-percent mass loss of the control; and the
control specimens completely failed after 350 cycles. The results of Cantabro test suggests that all
CrPC mixtures showed higher resistance to impact and abrasion with lower mass losses than the
Based on the above test results and observations, CCFCM addition generally improves the mechanical
properties of pervious concrete. CrPC3 and CrPC4 yield the optimal results across the experimental scope,
with improved f’t and MR while maintaining comparable compressive strength. CrPC3 and CrPC4 also
show negligible changes in porosity and infiltration. CrPC5 showed lower I and compressive strength,
however did result in increased f’t, MR, and toughness compared to the control.
Acknowledgements
The Boeing Company is gratefully acknowledged for their financial and in-kind support of the project.
Donations of aggregate from Pre-Mix Inc. and portland cement from Ash Grove Cement Company is also
acknowledged.
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Fig. 1: Fiber particles that passed Screen 10 (2 mm) and retained on Screen 20 (0.841 mm).
Fig. 2. Particle size distribution for the CCFCM and coarse aggregate used in the experiment.
Fig. 3. Specimens from each mixture, from left to right: CrPC0, CrPC3, CrPC4 and CrPC5.
Fig. 4. Hardened porosity per specimen type and mixture design. Number of specimens per
compared to control. Specimens include 18 100-mm cylinders, 10 150-mm cylinders and 6 prisms
Fig. 6. Infiltration rates of CCFCM reinforced PC. Infiltration generally drops with the addition of
CCFCM.
Fig. 7. Porosity-infiltration relations: CrPC3 demonstrates a similar slope as the control, while
CrPC4 and CrPC5 show gradually sloped trend lines: I remains constant at higher Φ levels.
Fig. 8. Average 7- and 28-day split tensile strength for each mixture. CrPC mixtures demonstrate
notably higher f’t than the control on both test dates. For CrPC0, 3, 4 and 5, respectively, the avg.
Φ of specimens tested at 7-day age were 26, 25, 23 and 24 percent. The respective coefficients of
variation (COV) of Φ were 0.03, 0.04, 0.03 and 0.03. For specimens tested on 28-day age, avg. Φ
were 25, 25, 21 and 26 with respective COV of Φ of 0.03, 0.02, 0.05 and 0.03.
Fig. 9. Avg. 7- and 28-day MR for each mixture. CrPC mixtures outperform CrPC0 on both test
dates and supersede those reported in the literature for plain PC. For CrPC0, 3, 4 and 5,
respectively, avg. Φ of specimens tested on 7-day age were: 28, 28, 26 and 27 percent with the
19
corresponding COV of 0.01, 0.02, 0.08 and 0.03. For specimens tested on 28-day, the avg. Φ were
28, 28, 26 and 29 with the corresponding COV of 0.02, 0.03, 0.04 and 0.02.
Fig. 10. (a) Twenty-eight day load-deflection curves during MR testing for toughness evaluation;
(b) Representation of the areas and equation used to calculate the toughness-index, shown for a
beam from CrPC5 as an example based on a modified procedure for PC (ASTM C1018).
Fig. 11. Avg. 7-day f’c for each mixture. All CrPC mixtures present comparable values of f’c to
that of the control, except CrPC5, however f’c for all mixtures fall in the range reported in the
literature. For CrPC0, 3, 4 and 5, respectively. Avg. Φ of tested specimens at 7-day were 26, 25,
23 and 24 percent. Respective COV of Φ were 0.04, 0.04, 0.05 and 0.05. For specimens tested on
28-day, avg. Φ were 25, 25, 21 and 26 with respective COV of Φ of 0.03, 0.02, 0.02 and 0.04.
Fig. 12. Percent mass loss during Cantabro test for all four mixtures: (a) tops of 100-mm cylinders,
and (b) bottoms of 100-mm cylinders. Both bottom specimens from the control failed at 350 cycles.
Average Φ of tested specimens: 0.24, 0.28, 0.23, 0.26 for CrPC0, CrPC3, CrPC4, and CrPC5,
respectively.
20
Table 1. PC and CrPC mixture designs used in the study.
Portland Admixtures CCFCM
Coarse CCFCM
Cement Water weight
Mixture ID Aggregate VMAR Recover volume
Type I/II (kg/m3) (kg/m3)
(kg/m3) (g/m3) (g/m3) fraction (%)
(kg/m3)
CrPC0 (Control) 1,376 413 112 1,450 1,409 0 0
CrPC3 1,376 413 112 1,450 1,409 3 46.8
CrPC4 1,376 413 112 1,450 1,409 4 62.4
CrPC5 1,376 413 112 1,450 1,409 5 78.0
21
1
2 Table 2. Toughness index estimated at deflection corresponding to two-time the peak deflection.
22
4
5 Table 3. Statistical comparison of mechanical properties of CrPC mixtures to the control mixture.
p-value
Mechanical property Seven-day testing 28-day testing
CrPC3 CrPC4 CrPC5 CrPC3 CrPC4 CrPC5
f’t 0.000 0.003 0.010 0.001 0.000 0.000
MR 0.011 0.035 0.050 0.016 0.050 0.078
f’c 0.604 0.653 0.012 0.389 0.802 0.036
6
23
7
24
8
25
9
26
10
27
11
28
12
29
13
30
14
31
15
32
16
33
17
34
18
35
19
20
21
36
22
37