Exp Cd Cu Fe Ni× Pb Zn Sulfate COD Cd Cu Fe Ni Pb Zn

run removal removal

(%) (%)

1 100 500 1500 50 100 100 62.67 61.4 90 93.6 60.4 45 97 84

2 100 250 1500 100 50 100 68.54 64.7 92 97.6 81.6 48 94 80

3 50 500 1500 100 50 100 66.2 63.4 98 99.4 84.5 44 97 92

4 100 500 500 100 100 50 65.65 65 100 99.6 64.5 46 97 88

5 50 250 500 100 100 100 71.42 72.6 100 99.6 77 48 97 96

6 50 500 1500 50 100 50 69.89 69.3 100 99.8 86.2 52 97 92

7 50 250 1500 100 100 50 66.45 66 100 99.6 72.6 53 98 88

8 50 500 500 50 50 100 78.56 76.3 100 100 80 55.4 96 95

9 100 500 500 100 50 50 73.84 70.3 100 100 64 49 94 90

10 50 250 500 50 50 50 81.32 80.2 100 100 88.2 64 99 98

11 100 250 1500 50 50 50 76.42 74.3 100 100 85.5 61 98 96

12 100 250 500 50 100 100 72.32 73.6 100 100 68.2 58 97 85

Table:Plackett–Burman statistical design presenting the removal of different heavy metals,

sulfate and COD in different combination levels

From the analysis; it is found that sulfate and COD removal are significant or effected by Fe and
Ni as apparent from analysis of variance (ANOVA) and Pareto charts
 Pareto Chart of the Standardized Effects
(response is C11, Alpha = 0.05)
2.571

D
Term

0 1 2 3 4 5 6 7
Standardized Effect

Pareto Chart of the Standardized Effects

(response is C12, Alpha = 0.05)
2.571

B
Term

0 1 2 3 4 5 6 7
Standardized Effect
 Pareto Chart of the Standardized Effects
(response is C15, Alpha = 0.05)
2.571

B
Term

0.0 0.5 1.0 1.5 2.0 2.5 3.0

Standardized Effect

Pareto Chart of the Standardized Effects

(response is C16, Alpha = 0.05)
2.571

F
Term

0 1 2 3 4 5 6 7 8
Standardized Effect
Factors: 6 Replicates: 1
Base runs: 12 Total runs: 12
Base blocks: 1 Total blocks: 1

Design Table (randomized)

Run Blk A B C D E F
1 1 + - - - + +
2 1 + + - + + -
3 1 + - + + - +
4 1 - - + + + -
5 1 - + + + - +
6 1 + - + - - -
7 1 - - - - - -
8 1 + + + - + +
9 1 - - - + + +
10 1 - + + - + -
11 1 + + - + - -
12 1 - + - - - +

Factorial Fit: C11, C12, C13, C14, C15, C16, C17, C18

Factorial Fit: C11 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C11 (coded units) This is t test
Term Effect Coef SE Coef T P
Constant 71.107 0.4938 144.00 0.000
A -2.400 -1.200 0.4938 -2.43 0.059
B -3.277 -1.638 0.4938 -3.32 0.021
C -5.490 -2.745 0.4938 -5.56 0.003
D -4.847 -2.423 0.4938 -4.91 0.004
E -6.080 -3.040 0.4938 -6.16 0.002
F -2.310 -1.155 0.4938 -2.34 0.066

S = 1.71055 PRESS = 84.2682

R-Sq = 95.84% R-Sq(pred) = 76.05% R-Sq(adj) = 90.85%

Analysis of Variance for C11 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 337.29 337.29 56.215 19.21 0.003
A 1 17.28 17.28 17.280 5.91 0.059
B 1 32.21 32.21 32.210 11.01 0.021
C 1 90.42 90.42 90.420 30.90 0.003
D 1 70.47 70.47 70.471 24.08 0.004
E 1 110.90 110.90 110.899 37.90 0.002
F 1 16.01 16.01 16.008 5.47 0.066
Residual Error 5 14.63 14.63 2.926
Total 11 351.92

Estimated Coefficients for C11 using data in uncoded units

Term Coef
Constant 104.967
A -0.480000
B -0.131067
C -0.0549000
D -0.969333
E -1.21600
F -0.462000

Least Squares Means for C11

Mean SE Mean
A
5 72.31 0.6983
10 69.91 0.6983
B
25 72.75 0.6983
50 69.47 0.6983
C
50 73.85 0.6983
150 68.36 0.6983
D
5 73.53 0.6983
10 68.68 0.6983
E
5 74.15 0.6983
10 68.07 0.6983
F
5 72.26 0.6983
10 69.95 0.6983

Predicted Response for New Design Points Using Model for C11

Point Fit SE Fit 95% CI 95% PI

1 72.5183 1.3065 (69.1600, 75.8767) (66.9854, 78.0512)
2 66.7050 1.3065 (63.3467, 70.0633) (61.1721, 72.2379)
3 68.2617 1.3065 (64.9033, 71.6200) (62.7288, 73.7946)
4 66.8917 1.3065 (63.5333, 70.2500) (61.3588, 72.4246)
5 67.3850 1.3065 (64.0267, 70.7433) (61.8521, 72.9179)
6 75.4183 1.3065 (72.0600, 78.7767) (69.8854, 80.9512)
7 83.3083 1.3065 (79.9500, 86.6667) (77.7754, 88.8412)
8 63.7517 1.3065 (60.3933, 67.1100) (58.2188, 69.2846)
9 70.0717 1.3065 (66.7133, 73.4300) (64.5388, 75.6046)
10 68.4617 1.3065 (65.1033, 71.8200) (62.9288, 73.9946)
11 72.7850 1.3065 (69.4267, 76.1433) (67.2521, 78.3179)
12 77.7217 1.3065 (74.3633, 81.0800) (72.1888, 83.2546)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
 12 5 50 50 5 5 10

Effects Plot for C11

Effects Pareto for C11

Factorial Fit: C12 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C12 (coded units)

Term Effect Coef SE Coef T P

Constant 69.758 0.5059 137.88 0.000
A -3.083 -1.542 0.5059 -3.05 0.029
B -4.283 -2.142 0.5059 -4.23 0.008
C -6.483 -3.242 0.5059 -6.41 0.001
D -5.517 -2.758 0.5059 -5.45 0.003
E -3.550 -1.775 0.5059 -3.51 0.017
F -2.183 -1.092 0.5059 -2.16 0.083

S = 1.75257 PRESS = 88.4592

R-Sq = 95.83% R-Sq(pred) = 75.99% R-Sq(adj) = 90.83%

Analysis of Variance for C12 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 353.07 353.07 58.845 19.16 0.003
A 1 28.52 28.52 28.521 9.29 0.029
B 1 55.04 55.04 55.041 17.92 0.008
C 1 126.10 126.10 126.101 41.06 0.001
D 1 91.30 91.30 91.301 29.73 0.003
E 1 37.81 37.81 37.808 12.31 0.017
F 1 14.30 14.30 14.301 4.66 0.083
Residual Error 5 15.36 15.36 3.071
Total 11 368.43

Estimated Coefficients for C12 using data in uncoded units

Term Coef
Constant 104.167
A -0.616667
B -0.171333
C -0.0648333
D -1.10333
E -0.710000
F -0.436667

Least Squares Means for C12

Mean SE Mean
A
5 71.30 0.7155
10 68.22 0.7155
B
25 71.90 0.7155
 50 67.62 0.7155
C
50 73.00 0.7155
150 66.52 0.7155
D
5 72.52 0.7155
10 67.00 0.7155
E
5 71.53 0.7155
10 67.98 0.7155
F
5 70.85 0.7155
10 68.67 0.7155

Predicted Response for New Design Points Using Model for C12

Point Fit SE Fit 95% CI 95% PI

1 73.4917 1.3385 (70.0508, 76.9325) (67.8228, 79.1605)
2 65.8750 1.3385 (62.4342, 69.3158) (60.2062, 71.5438)
3 65.0417 1.3385 (61.6008, 68.4825) (59.3728, 70.7105)
4 66.7583 1.3385 (63.3175, 70.1992) (61.0895, 72.4272)
5 63.8417 1.3385 (60.4008, 67.2825) (58.1728, 69.5105)
6 72.7417 1.3385 (69.3008, 76.1825) (67.0728, 78.4105)
7 82.3083 1.3385 (78.8675, 85.7492) (76.6395, 87.9772)
8 62.7250 1.3385 (59.2842, 66.1658) (57.0562, 68.3938)
9 71.0583 1.3385 (67.6175, 74.4992) (65.3895, 76.7272)
10 67.9917 1.3385 (64.5508, 71.4325) (62.3228, 73.6605)
11 69.4250 1.3385 (65.9842, 72.8658) (63.7562, 75.0938)
12 75.8417 1.3385 (72.4008, 79.2825) (70.1728, 81.5105)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C12

Effects Pareto for C12

Factorial Fit: C13 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C13 (coded units)

Term Effect Coef SE Coef T P

Constant 98.333 0.8692 113.13 0.000
A -2.667 -1.333 0.8692 -1.53 0.186
B -0.667 -0.333 0.8692 -0.38 0.717
C -3.333 -1.667 0.8692 -1.92 0.113
D 0.000 0.000 0.8692 0.00 1.000
E -0.000 -0.000 0.8692 -0.00 1.000
F -3.333 -1.667 0.8692 -1.92 0.113

S = 3.01109 PRESS = 261.12

R-Sq = 66.34% R-Sq(pred) = 0.00% R-Sq(adj) = 25.94%

Analysis of Variance for C13 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 89.333 89.3333 14.8889 1.64 0.301
A 1 21.333 21.3333 21.3333 2.35 0.186
B 1 1.333 1.3333 1.3333 0.15 0.717
C 1 33.333 33.3333 33.3333 3.68 0.113
D 1 0.000 0.0000 0.0000 * *
E 1 0.000 0.0000 0.0000 * *
F 1 33.333 33.3333 33.3333 3.68 0.113
Residual Error 5 45.333 45.3333 9.0667
Total 11 134.667

Estimated Coefficients for C13 using data in uncoded units

Term Coef
Constant 111.667
A -0.533333
B -0.0266667
C -0.0333333
D 0.000000
E -0.000000
F -0.666667

Least Squares Means for C13

Mean SE Mean
A
5 99.67 1.229
10 97.00 1.229
B
25 98.67 1.229
50 98.00 1.229
C
50 100.00 1.229
150 96.67 1.229
D
5 98.33 1.229
10 98.33 1.229
E
5 98.33 1.229
10 98.33 1.229
F
5 100.00 1.229
10 96.67 1.229

Predicted Response for New Design Points Using Model for C13
Point Fit SE Fit 95% CI 95% PI
1 97.333 2.300 (91.422, 103.245) (87.594, 107.073)
2 100.000 2.300 (94.088, 105.912) (90.260, 109.740)
3 94.000 2.300 (88.088, 99.912) (84.260, 103.740)
4 100.000 2.300 (94.088, 105.912) (90.260, 109.740)
5 96.000 2.300 (90.088, 101.912) (86.260, 105.740)
6 97.333 2.300 (91.422, 103.245) (87.594, 107.073)
7 103.333 2.300 (97.422, 109.245) (93.594, 113.073)
8 93.333 2.300 (87.422, 99.245) (83.594, 103.073)
9 100.000 2.300 (94.088, 105.912) (90.260, 109.740)
10 99.333 2.300 (93.422, 105.245) (89.594, 109.073)
11 100.000 2.300 (94.088, 105.912) (90.260, 109.740)
12 99.333 2.300 (93.422, 105.245) (89.594, 109.073)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C13

Effects Pareto for C13

Factorial Fit: C14 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C14 (coded units)

Term Effect Coef SE Coef T P

Constant 99.1000 0.5090 194.68 0.000
A -1.2667 -0.6333 0.5090 -1.24 0.269
B -0.7333 -0.3667 0.5090 -0.72 0.504
C -1.5333 -0.7667 0.5090 -1.51 0.192
D 0.4000 0.2000 0.5090 0.39 0.711
E -0.8000 -0.4000 0.5090 -0.79 0.468
F -1.4667 -0.7333 0.5090 -1.44 0.209

S = 1.76333 PRESS = 89.5488

R-Sq = 58.96% R-Sq(pred) = 0.00% R-Sq(adj) = 9.71%

Analysis of Variance for C14 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 22.3333 22.3333 3.7222 1.20 0.431
A 1 4.8133 4.8133 4.8133 1.55 0.269
 B 1 1.6133 1.6133 1.6133 0.52 0.504
C 1 7.0533 7.0533 7.0533 2.27 0.192
D 1 0.4800 0.4800 0.4800 0.15 0.711
E 1 1.9200 1.9200 1.9200 0.62 0.468
F 1 6.4533 6.4533 6.4533 2.08 0.209
Residual Error 5 15.5467 15.5467 3.1093
Total 11 37.8800

Unusual Observations for C14

Obs StdOrder C14 Fit SE Fit Residual St Resid

8 6 93.600 96.000 1.347 -2.400 -2.11R

R denotes an observation with a large standardized residual.

Estimated Coefficients for C14 using data in uncoded units

Term Coef
Constant 106.433
A -0.253333
B -0.0293333
C -0.0153333
D 0.080000
E -0.160000
F -0.293333

Least Squares Means for C14

Mean SE Mean
A
5 99.73 0.7199
10 98.47 0.7199
B
25 99.47 0.7199
50 98.73 0.7199
C
50 99.87 0.7199
150 98.33 0.7199
D
5 98.90 0.7199
10 99.30 0.7199
E
5 99.50 0.7199
10 98.70 0.7199
F
5 99.83 0.7199
10 98.37 0.7199

Predicted Response for New Design Points Using Model for C14

Point Fit SE Fit 95% CI 95% PI

1 98.267 1.347 (94.805, 101.729) (92.563, 103.970)
2 99.400 1.347 (95.938, 102.862) (93.696, 105.104)
3 97.933 1.347 (94.471, 101.395) (92.230, 103.637)
4 99.867 1.347 (96.405, 103.329) (94.163, 105.570)
5 98.467 1.347 (95.005, 101.929) (92.763, 104.170)
6 99.000 1.347 (95.538, 102.462) (93.296, 104.704)
7 101.800 1.347 (98.338, 105.262) (96.096, 107.504)
8 96.000 1.347 (92.538, 99.462) (90.296, 101.704)
 9 99.933 1.347 (96.471, 103.395) (94.230, 105.637)
10 98.733 1.347 (95.271, 102.195) (93.030, 104.437)
11 100.200 1.347 (96.738, 103.662) (94.496, 105.904)
12 99.600 1.347 (96.138, 103.062) (93.896, 105.304)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C14

Effects Pareto for C14

Factorial Fit: C15 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C15 (coded units)

Term Effect Coef SE Coef T P

Constant 76.058 2.002 37.99 0.000
A -10.717 -5.358 2.002 -2.68 0.044
B -5.583 -2.792 2.002 -1.39 0.222
C 4.817 2.408 2.002 1.20 0.283
D -4.050 -2.025 2.002 -1.01 0.358
E -9.150 -4.575 2.002 -2.29 0.071
F -1.550 -0.775 2.002 -0.39 0.715

S = 6.93490 PRESS = 1385.07

R-Sq = 77.22% R-Sq(pred) = 0.00% R-Sq(adj) = 49.89%

Analysis of Variance for C15 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 815.24 815.245 135.874 2.83 0.137
A 1 344.54 344.541 344.541 7.16 0.044
B 1 93.52 93.521 93.521 1.94 0.222
C 1 69.60 69.601 69.601 1.45 0.283
D 1 49.21 49.208 49.208 1.02 0.358
E 1 251.17 251.167 251.167 5.22 0.071
F 1 7.21 7.208 7.208 0.15 0.715
Residual Error 5 240.46 240.464 48.093
Total 11 1055.71
Estimated Coefficients for C15 using data in uncoded units

Term Coef
Constant 117.817
A -2.14333
B -0.223333
C 0.0481667
D -0.810000
E -1.83000
F -0.310000

Least Squares Means for C15

Mean SE Mean
A
5 81.42 2.831
10 70.70 2.831
B
25 78.85 2.831
50 73.27 2.831
C
50 73.65 2.831
150 78.47 2.831
D
5 78.08 2.831
10 74.03 2.831
E
5 80.63 2.831
10 71.48 2.831
F
5 76.83 2.831
10 75.28 2.831

Predicted Response for New Design Points Using Model for C15

Point Fit SE Fit 95% CI 95% PI

1 67.7583 5.2966 (54.1429, 81.3737) (45.3269, 90.1898)
2 59.6750 5.2966 (46.0596, 73.2904) (37.2435, 82.1065)
3 77.6750 5.2966 (64.0596, 91.2904) (55.2435, 100.1065)
4 80.7917 5.2966 (67.1763, 94.4071) (58.3602, 103.2231)
5 82.8083 5.2966 (69.1929, 96.4237) (60.3769, 105.2398)
6 83.2750 5.2966 (69.6596, 96.8904) (60.8435, 105.7065)
7 89.1750 5.2966 (75.5596, 102.7904) (66.7435, 111.6065)
8 66.9917 5.2966 (53.3763, 80.6071) (44.5602, 89.4231)
9 74.4250 5.2966 (60.8096, 88.0404) (51.9935, 96.8565)
10 79.2583 5.2966 (65.6429, 92.8737) (56.8269, 101.6898)
11 68.8250 5.2966 (55.2096, 82.4404) (46.3935, 91.2565)
12 82.0417 5.2966 (68.4263, 95.6571) (59.6102, 104.4731)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
 9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C15

Effects Pareto for C15

Factorial Fit: C16 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C16 (coded units)

Term Effect Coef SE Coef T P

Constant 51.950 0.5167 100.55 0.000
A -1.567 -0.783 0.5167 -1.52 0.190
B -6.767 -3.383 0.5167 -6.55 0.001
C -2.900 -1.450 0.5167 -2.81 0.038
D -7.900 -3.950 0.5167 -7.65 0.001
E -3.233 -1.617 0.5167 -3.13 0.026
F -4.433 -2.217 0.5167 -4.29 0.008

S = 1.78979 PRESS = 92.256

R-Sq = 96.54% R-Sq(pred) = 80.10% R-Sq(adj) = 92.40%

Analysis of Variance for C16 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 447.513 447.513 74.586 23.28 0.002
A 1 7.363 7.363 7.363 2.30 0.190
B 1 137.363 137.363 137.363 42.88 0.001
C 1 25.230 25.230 25.230 7.88 0.038
D 1 187.230 187.230 187.230 58.45 0.001
E 1 31.363 31.363 31.363 9.79 0.026
F 1 58.963 58.963 58.963 18.41 0.008
Residual Error 5 16.017 16.017 3.203
Total 11 463.530

Estimated Coefficients for C16 using data in uncoded units

Term Coef
Constant 90.7000
A -0.313333
B -0.270667
C -0.0290000
D -1.58000
E -0.646667
F -0.886667

Least Squares Means for C16

Mean SE Mean
A
5 52.73 0.7307
 10 51.17 0.7307
B
25 55.33 0.7307
50 48.57 0.7307
C
50 53.40 0.7307
150 50.50 0.7307
D
5 55.90 0.7307
10 48.00 0.7307
E
5 53.57 0.7307
10 50.33 0.7307
F
5 54.17 0.7307
10 49.73 0.7307

Predicted Response for New Design Points Using Model for C16

Point Fit SE Fit 95% CI 95% PI

1 56.1167 1.3670 (52.6028, 59.6306) (50.3275, 61.9059)
2 45.8833 1.3670 (42.3694, 49.3972) (40.0941, 51.6725)
3 48.5500 1.3670 (45.0361, 52.0639) (42.7608, 54.3392)
4 51.3167 1.3670 (47.8028, 54.8306) (45.5275, 57.1059)
5 43.3500 1.3670 (39.8361, 46.8639) (37.5608, 49.1392)
6 60.8833 1.3670 (57.3694, 64.3972) (55.0941, 66.6725)
7 65.3500 1.3670 (61.8361, 68.8639) (59.5608, 71.1392)
8 46.4500 1.3670 (42.9361, 49.9639) (40.6608, 52.2392)
9 49.7833 1.3670 (46.2694, 53.2972) (43.9941, 55.5725)
10 52.4500 1.3670 (48.9361, 55.9639) (46.6608, 58.2392)
11 49.1167 1.3670 (45.6028, 52.6306) (43.3275, 54.9059)
12 54.1500 1.3670 (50.6361, 57.6639) (48.3608, 59.9392)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C16

Effects Pareto for C16

Factorial Fit: C17 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C17 (coded units)

Term Effect Coef SE Coef T P
Constant 96.7500 0.4031 240.01 0.000
A -1.1667 -0.5833 0.4031 -1.45 0.208
B -0.8333 -0.4167 0.4031 -1.03 0.349
C 0.1667 0.0833 0.4031 0.21 0.844
D -1.1667 -0.5833 0.4031 -1.45 0.208
E 0.8333 0.4167 0.4031 1.03 0.349
F -0.8333 -0.4167 0.4031 -1.03 0.349

S = 1.39642 PRESS = 56.16

R-Sq = 59.79% R-Sq(pred) = 0.00% R-Sq(adj) = 11.55%

Analysis of Variance for C17 (coded units)

Source DF Seq SS Adj SS Adj MS F P

Main Effects 6 14.5000 14.5000 2.41667 1.24 0.416
A 1 4.0833 4.0833 4.08333 2.09 0.208
B 1 2.0833 2.0833 2.08333 1.07 0.349
C 1 0.0833 0.0833 0.08333 0.04 0.844
D 1 4.0833 4.0833 4.08333 2.09 0.208
E 1 2.0833 2.0833 2.08333 1.07 0.349
F 1 2.0833 2.0833 2.08333 1.07 0.349
Residual Error 5 9.7500 9.7500 1.95000
Total 11 24.2500

Estimated Coefficients for C17 using data in uncoded units

Term Coef
Constant 101.333
A -0.233333
B -0.0333333
C 0.00166667
D -0.233333
E 0.166667
F -0.166667

Least Squares Means for C17

Mean SE Mean
A
5 97.33 0.5701
10 96.17 0.5701
B
25 97.17 0.5701
50 96.33 0.5701
C
50 96.67 0.5701
150 96.83 0.5701
D
5 97.33 0.5701
10 96.17 0.5701
E
5 96.33 0.5701
10 97.17 0.5701
F
5 97.17 0.5701
10 96.33 0.5701
Predicted Response for New Design Points Using Model for C17

Point Fit SE Fit 95% CI 95% PI

1 97.0833 1.0665 (94.3417, 99.8250) (92.5665, 101.6002)
2 95.9167 1.0665 (93.1750, 98.6583) (91.3998, 100.4335)
3 95.2500 1.0665 (92.5084, 97.9916) (90.7332, 99.7668)
4 98.0833 1.0665 (95.3417, 100.8250) (93.5665, 102.6002)
5 95.5833 1.0665 (92.8417, 98.3250) (91.0665, 100.1002)
6 97.2500 1.0665 (94.5084, 99.9916) (92.7332, 101.7668)
7 98.2500 1.0665 (95.5084, 100.9916) (93.7332, 102.7668)
8 96.4167 1.0665 (93.6750, 99.1583) (91.8998, 100.9335)
9 97.0833 1.0665 (94.3417, 99.8250) (92.5665, 101.6002)
10 98.4167 1.0665 (95.6750, 101.1583) (93.8998, 102.9335)
11 95.0833 1.0665 (92.3417, 97.8250) (90.5665, 99.6002)
12 96.5833 1.0665 (93.8417, 99.3250) (92.0665, 101.1002)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10

Effects Plot for C17

Effects Pareto for C17

Factorial Fit: C18 versus A, B, C, D, E, F

Estimated Effects and Coefficients for C18 (coded units)

Term Effect Coef SE Coef T P

Constant 90.333 1.297 69.62 0.000
A -6.333 -3.167 1.297 -2.44 0.059
B -0.333 -0.167 1.297 -0.13 0.903
C -3.333 -1.667 1.297 -1.28 0.255
D -2.667 -1.333 1.297 -1.03 0.351
E -3.000 -1.500 1.297 -1.16 0.300
F -3.333 -1.667 1.297 -1.28 0.255

S = 4.49444 PRESS = 581.76

R-Sq = 70.00% R-Sq(pred) = 0.00% R-Sq(adj) = 34.00%

Analysis of Variance for C18 (coded units)

Source DF Seq SS Adj SS Adj MS F P
Main Effects 6 235.667 235.667 39.278 1.94 0.241
A 1 120.333 120.333 120.333 5.96 0.059
B 1 0.333 0.333 0.333 0.02 0.903
C 1 33.333 33.333 33.333 1.65 0.255
D 1 21.333 21.333 21.333 1.06 0.351
E 1 27.000 27.000 27.000 1.34 0.300
F 1 33.333 33.333 33.333 1.65 0.255
Residual Error 5 101.000 101.000 20.200
Total 11 336.667

Unusual Observations for C18

Obs StdOrder C18 Fit SE Fit Residual St Resid

6 1 96.0000 90.1667 3.4327 5.8333 2.01R

R denotes an observation with a large standardized residual.

Estimated Coefficients for C18 using data in uncoded units

Term Coef
Constant 117.167
A -1.26667
B -0.013333
C -0.0333333
D -0.533333
E -0.600000
F -0.666667

Least Squares Means for C18

Mean SE Mean
A
5 93.50 1.835
10 87.17 1.835
B
25 90.50 1.835
50 90.17 1.835
C
50 92.00 1.835
150 88.67 1.835
D
5 91.67 1.835
10 89.00 1.835
E
5 91.83 1.835
10 88.83 1.835
F
5 92.00 1.835
10 88.67 1.835

Predicted Response for New Design Points Using Model for C18

Point Fit SE Fit 95% CI 95% PI

1 87.1667 3.4327 (78.3427, 95.9907) (72.6290, 101.7043)
2 87.5000 3.4327 (78.6760, 96.3240) (72.9624, 102.0376)
3 84.1667 3.4327 (75.3427, 92.9907) (69.6290, 98.7043)
4 90.8333 3.4327 (82.0093, 99.6573) (76.2957, 105.3710)
5 90.1667 3.4327 (81.3427, 98.9907) (75.6290, 104.7043)
 6 90.1667 3.4327 (81.3427, 98.9907) (75.6290, 104.7043)
7 99.8333 3.4327 (91.0093, 108.6573) (85.2957, 114.3710)
8 83.5000 3.4327 (74.6760, 92.3240) (68.9624, 98.0376)
9 90.8333 3.4327 (82.0093, 99.6573) (76.2957, 105.3710)
10 93.1667 3.4327 (84.3427, 101.9907) (78.6290, 107.7043)
11 90.5000 3.4327 (81.6760, 99.3240) (75.9624, 105.0376)
12 96.1667 3.4327 (87.3427, 104.9907) (81.6290, 110.7043)

Values of Predictors for New Observations

New Obs A B C D E F
1 10 25 50 5 10 10
2 10 50 50 10 10 5
3 10 25 150 10 5 10
4 5 25 150 10 10 5
5 5 50 150 10 5 10
6 10 25 150 5 5 5
7 5 25 50 5 5 5
8 10 50 150 5 10 10
9 5 25 50 10 10 10
10 5 50 150 5 10 5
11 10 50 50 10 5 5
12 5 50 50 5 5 10