Postweld heat treatment (PWHT) of the vessel is decided
based on the material of construction, fabrication methods, thickness of shell sections, etc., as contained in clause UW 40 (see Chapter 21, Section 17). Usually, vessels of 11/2 in. (38 mm) and over in thickness have to undergo PWHT. Those in the range of 11/4 to 11/2 in. (32 to 38 mm) need not go for PWHT, provided preheat at a minimum temperature of 200°F (93.3°C) is given during welding. Further, vessels that are subjected to low temperatures shall also undergo PWHT irrespective of thickness. As this is a design criterion, it is not elaborated here. However, as this requirement is indicated in the draw- ings, we try to carry out the PWHT according to the provisions of the code.
In any procedure for PWHT, the following aspects shall be ad-
dressed.
2.1 Method of PWHT
Depending on the size of the vessel and capacity of the furnace (size and maximum temperature), a full or partial PWHT is performed. In full PWHT, there are two types of firing meth- ods. The most common one is the furnace PWHT wherein the vessel is loaded inside the furnace and heated to the required level in a single firing as per the previously laid down proce- dure. This is the most desirable type of PWHT because all pa- rameters in the heating, soaking, and cooling cycle can be con- trolled well. However, the availability of such furnaces are the only constraint. Both oil firing as well as electrical heating could be used for this. If PWHT in one go is not possible due to the size of the vessel, UW 40 permits the use of part-by- part PWHT with sufficient overlap of the heated zones. In the second method, the vessel itself is made the fur- nace by providing burners at appropriate points and by giving insulation all around the vessel. The method is called internal firing and is very much dependent on the skill of those that perform this feat. The method of heating adopted is generally oil firing with an additional electrical- or oil-fired heating sys- tem at anticipated cold spots. The third method is to do the PWHT of welds alone when the design permits, using electrical resistance heating. Here again proper overlap between two PWHT zones shall be given as envisaged in UW 40.
2.2 Heating Rate
The heating rates to be followed are given in UCS 56 for car- bon steel vessels and UHT 56 for steels whose properties en- hanced by heat treatment. The rate specified in UCS 56 is above 800°F (427°C), which is the maximum permitted fur-
nace temperature at the time of loading the vessel. The heat-
ing rates recommended are based on the thickness of the shells. As thickness increases, the rate falls. As per UCS 56, the rate suggested is 400°F/hr per inch (204.4°C/hr per 25 mm) thickness of the vessel, but in no case more than 400°F/ hr (204.4°C/hr). The manufacturer can always go for a lower heating rate. However, too low a heating rate may be too ex- pensive.
2.3 Soaking Temperature and Time
For carbon steel vessels, the soaking time and temperature are specified in UCS 56. Soaking temperature is related to the material specification, whereas the time is based on the thick- ness of the shell of the vessel. For P. No. 1 materials, the soak- ing time specified is 1 hr per inch (1 hr per 25 mm) of vessel thickness with a minimum of 15 min. Similarly the soaking temperature specified is 1100°F (593.3°C). Soaking at temper- atures lower than that specified calls for extended soaking time, as specified in UCS 56.1. However, it is recommended to carry out the PWHT at the specified temperature and time frame so that detrimental effects due to spheroidization can be avoided.
2.4 Cooling Rate
After soaking, the cooling starts. As per UCS 56, the recom- mended maximum cooling rate is 500°F/hr per inch (260°C/ hr per 25 mm) thickness of the vessel but in no case greater than 500°F/hr (260°C/hr). Slower cooling rates are always preferred, the only consideration being cost. The cooling rate specified is only up to 800°F (427°C), below which it may be cooled in still air.
3 HEAT TREATMENT CYCLE
The chart indicating the heating rate, soaking temperature/
time, and cooling rate is the heat treatment cycle and shall
form a part of the procedure previously approved as per the
provisions of the code. All the other details elaborated are the ones that are normally followed by the operator of the furnace.
4 PLACEMENT OF THERMOCOUPLES
The number of thermocouples to be used for monitoring the
temperature is calculated based on the diameter, length, and position of other welded attachments on the vessel as per the code. Once the number of thermocouples is finalized based on the code and client specification, the location of the same is fixed based on the configuration of the vessel as well as the heating method proposed and the location of the heat source. By looking at the position of the heat source and the configu- ration of the vessel, one can easily locate the probable cold and hot spots. Even though the very purpose of the thermocouple is to monitor the temperature, it should also indicate the dif- ference in temperature at the hot and cold spots. Because of this reason, thermocouples shall be randomly provided at the hot and cold spots evenly as far as possible. In case the differ- ence in temperature between thermocouples is found to be in excess of that stipulated in the codes [i.e., 250°F (121°C) while heating and 150°F (65.6°C) during soaking], the same shall be brought within the acceptable limits by either bringing down the heating rate or by providing additional heat sources at the cold spots.
5 CALIBRATION OF RECORDERS AND THERMOCOUPLES
The recorders to be used shall have valid calibration certifi-
cates on the date of performance of the PWHT. Further the thermocouples shall also have valid certification as to the chemical composition of the element as this is the only possible calibration for the same.
A certificate indicating the loading temperature, heating rate,
soaking temperature, soaking time, cooling rate, unloading temperature, etc., is prepared as in Figure 7.1 for every heat treatment. In addition to this information, the actual heat treatment chart will have the speed of the chart and will ac- company this certificate. A sample procedure for PWHT is en- closed in Chapter 15 in which a PWHT cycle is proposed. The actual time/temperature chart obtained from the multipoint recorder connected to thermocouples will reveal the deviation from the proposed cycle. The following aspects shall be verified from the chart:
1. The loading temperature shall be below 800°F
(427°C). 2. The heating and cooling rates shall be either equal to or lesser than that specified in the procedure drawn out as per code. For calculating this the chart speed has also to be noted down. 3. Soaking temperature and time shall be marginally above that specified. 4. The unloading temperature shall be less than 900°F (482°C), that specified in the code. 5. All recorders and thermocouples shall have a valid calibration certificate.