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Materials and Structures (2017)50:55

DOI 10.1617/s11527-016-0914-5

ORIGINAL ARTICLE

Fiber orientation distribution and tensile mechanical


response in UHPFRC
Luis Felipe Maya Duque . Benjamin Graybeal

Received: 18 September 2015 / Accepted: 8 June 2016


Ó RILEM 2016

Abstract In this study, the crucial effect of the fiber to implement robust and reliable safety factors
orientation distribution on the tensile mechanical accounting for the fiber orientation distribution impact
response of ultra high performance fiber reinforced on the design methodologies for UHPFRC. Finally,
concretes (UHPFRC) is discussed. A direct tension the need of a comprehensive design framework for
test method was used to characterize the tensile UHPFRC structures was highlighted in order to allow
response of a UHPFRC material as well as to assess for fully exploitation of the material properties.
the actual tensile response along the principal direc-
tions in a real-scale UHPFRC structural element. Keywords Fiber orientation  Orientation factor 
Moreover, the actual fiber orientation distribution was Tensile response  Direct tension test  Image analysis 
evaluated in representative sections through an image UHPFRC
analysis technique. The experimental results validated
the anisotropy in the fiber orientation distribution and,
consequently, in the tensile mechanical properties as a 1 Introduction
consequence of the casting process and the flow
pattern. The concept of the fiber orientation factor was Ultra-high performance fiber reinforced concrete
discussed as well as the approaches currently adopted (UHPFRC) is a class of cementitious composite
material that exhibits exceptional mechanical and
durability properties. These materials are usually
characterized by compressive strength greater than
150 MPa and the use of fibers as reinforcement, which
Luis Felipe Maya Duque is formerly affiliated with the Turner
Fairbank Highway Research Center. U.S Federal Highway
allows for sustained postcracking tensile strength and
Administration, USA. toughness increase [1–3]. Those exceptional tensile
mechanical properties have been of interest for the
L. F. Maya Duque (&) civil infrastructure community as they might lead to
Exergy Ltd., The Technocentre, Coventry University
new design and construction concepts.
Technology Park, Puma Way, Coventry CV1 2TT, UK
e-mail: femayadu@gmail.com The unique tensile response of UHPFRC is affected
not only by the material formulation but also by the
B. Graybeal casting method and element production process. These
Turner Fairbank Highway Research Center, U.S Federal
factors affect the actual fiber distribution and orienta-
Highway Administration, 6300 Georgetown Pike,
McLean, VA 22101, USA tion, and thus the mechanical tensile response. More-
e-mail: benjamin.graybeal@dot.gov over, fiber properties (e.g., strength, stiffness,
55 Page 2 of 17 Materials and Structures (2017)50:55

Poisson’s ratio, geometry, shape, and volume), matrix Therefore, the impact of these factors and the conse-
properties (e.g., strength, stiffness, Poisson’s ratio, quent anisotropy and non-homogeneity of the mechan-
compactness), as well as interface properties need to be ical properties must be properly accounted for in order
carefully considered during the material formulation. to enable safe, economic and sustainable UHPFRC
Despite the exceptional properties, the industrial designs.
uptake and engagement of UHPFRC within the civil The influence of the material formulation on the
infrastructure has been limited. Among the different mechanical and physical properties of UHPFRC has
factors that need to be addressed to promote the been the subject of a number of research initiatives.
widespread use of UHPFRC, the development of Analytic models as well as experimental validations
specific design standards is regarded as crucial. In have enabled mix formulation optimization to ensure
doing so, reliable tests and methodologies for quan- the achievement of exceptional mechanical and dura-
tifying the mechanical properties, in particular the bility properties while controlling the rheology and
tensile response, are required. Those methodologies workability of the material for a proper fiber distribu-
must account for the material anisotropy and facilitate tion [5–8]. Likewise, the impact of the casting method
the quality control and the performance assessment of and the production process on the final orientation and
UHPFRC structural elements. distribution of the fibers have been experimentally
studied, among others, by Ferrara et al. [9], Martinie
and Roussel [10], Oesterlee et al. [11], and Wille et al.
2 Tensile response [12]. Several techniques have been employed to assess
the fiber distribution, including image analysis
An efficient use of UHPFRC for infrastructure appli- [12–14] and non destructive methods based on elec-
cations requires a throughout understanding and trical resistivity measurements [15, 16] and alternating
quantification of the singularities of its tensile current-impedance spectroscopy (AC-IS) [17, 18].
mechanical behavior. Figure 1 presents the idealized Furthermore, probabilistic approaches have been
tensile response of UHPFRC, which is characterized employed to account for the fiber distribution and
by an initial elastic response until the first cracking of the fiber orientation [13, 14, 19, 20], as well as
the composite, the subsequent multi-cracking and numerical models to simulate the distribution of the
crack straining domains and the final strain localiza- fibers and their orientation during the flow [16, 21, 22].
tion at a discrete crack [4].
The fiber volume fraction for UHPFRC is usually 2.1 Orientation factor
relatively high, over 2.0 %, and the fiber dispersion
and orientation distribution are usually assumed to be In order to account for the effect of the fiber
uniform, which enable the material to be often orientation distribution on the tensile mechanical
considered as homogeneous and isotropic. However, response of fiber reinforced concretes, fiber orienta-
the actual dispersion and orientation distribution of the tion factor concepts are usually considered. Several
fibers are definitely affected by the material formula- analytical and empirical approaches for the fiber
tion, the casting method and the production process. orientation factor have been discussed in the literature.
Soroushian and Lee [23] presented a formulation for
the average fiber orientation factor using a uniform
probability function for the distribution of the incli-
nation angle of the fibers with respect to two perpen-
dicular axes that are parallel to the crack surface. As
suggested by Aveston and Kelly [24], other
approaches have considered variable probability den-
sities for the inclination angle between the fiber axis
and the cut plane [14, 19, 20, 25, 26]. Based on that
latter approach, and assuming a sine function for the
probability density function of the angle of the fiber to
Fig. 1 Idealized tensile response for UHPFRC [4] the normal vector to the cut plane, the orientation
Materials and Structures (2017)50:55 Page 3 of 17 55

factor has been derived for two- and three-dimensional different design guidelines for quantifying the tensile
(2D and 3D) uniform cases, and it is equal to 2/p and mechanical response of fiber reinforced concretes and
0.5, respectively [20]. defining their constitutive models [32]. As for
Following the Soroushian and Lee approach [23], a UHPFRC in particular, there are limited specific
first expression for the calculation of the fiber orien- design guidelines available [1, 33], from which the
tation factor a was defined as the ratio between the recommendations developed by the Association Fran-
actual number of fibers counted in a cross section to caise de Gènie Civil (AFGC) [1] might represent the
the average theoretical number estimated in the main reference document. Unlike most of the design
section, Eq. (1). recommendations for fiber reinforced concrete, the
N Af AFGC recommendations for UHPFRC explicitly
aeq:1 ¼ ð1Þ accounts for the impact of the fiber orientation
Ap Vf
distribution on the tensile material constitutive model
where N is the total number of fibers crossing an area and, thus, on the structural design through the
Ap , Vf is the fiber volume fraction, and Af is the fiber definition of specific reduction factors. In order to
cross sectional area. However, two main drawbacks determine the reduction factors, denominated K factors
have been pointed out for this definition of the fiber in the AFGC recommendations, a series of suitability
orientation factor. First, the actual theoretical number tests must be completed under conditions that repre-
of fibers in a cross section is usually overestimated by sent the stress states of the element in the real
the approximate method adopted, and, second, the fact structure. The AFGC recommendations distinguishes
that counting the number of fibers does not directly between global and local K factors, Kglobal and Klocal , in
reflect the actual inclination of the fibers with respect order to take into account possible local effects and the
to the cross section and thus their effectiveness [6, 22]. potential inability of stress redistribution. The mini-
Therefore, an alternative definition of the fiber orien- mum value for the K factor is 1.0 and higher values
tation factor has been adopted by other researchers reflect negative fiber orientation effects. In an initial
[12, 22, 27], Eq. (2). design stage and only for pre-dimensioning purposes
the AFGC recommendations suggests values of 1.25
1X n
1X n
bi and 1.75 for Kglobal and Klocal , respectively. The
aeq:2 ¼ cos hi ¼ ð2Þ
N i¼1 N i¼1 ai reduction factor affects only the non-linear part of
the tensile constitutive law in the form of 1/K. More
where N is again the total number of fibers in the cut
recently, the fib Model Code 2010 [30] has adopted a
section, hi is the angle between the fiber axis and the
more comprehensive approach for fiber reinforced
vector normal to the cut plane, a1 is the major axis of
concrete materials which also covers UHPFRC mate-
the elliptical footprint of the fiber on the cut plane, and
rials. The innovative approach also accounts explicitly
bi is the minor axis of the elliptical footprint of the
for the influence of fiber orientation distribution in a
fiber on the cut plane, which is equal to the diameter of
the fiber, see Fig. 2. The fiber footprint for a fiber
perpendicular to the cut plane is a circle and the
footprint is an ellipse which major axis is larger as the
angle of inclination between the fiber longitudinal axis
and the vector normal to the cut plane increases.

2.2 Codes and recommendations

There are currently a number of standards and


recommendations that provide methods to character-
ize the material properties of fiber reinforced concrete
materials as well as specific design guidelines for these
materials [28–31]. However, there are substantial
differences among the approaches adopted in the Fig. 2 Parameters defining fiber orientation in a section
55 Page 4 of 17 Materials and Structures (2017)50:55

similar fashion that the AFGC recommendations, i.e, smooth surfaces and facilitate the releasing of the cast
the determination of reduction factors. However, the elements. The UHPFRC was poured at one end of the
fib Model Code 2010 does not provide specific formwork using a wide wooden chute and the material
guidelines on the quantification of those factors. was let flow freely to fill completely the formwork,
which was placed slightly inclined. Along with the
slab elements, cylinders and prismatic specimens were
cast for material characterization. A total of twelve
3 Experimental validation
cylinders (72 mm diameter and 152 mm height) were
cast for each slab using plastic molds. Likewise,
A comprehensive approach for designing and manu-
twelve prismatic elements (50.8 mm wide, 50.8 mm
facturing UHPFRC structural elements must consider
thick and 431.8 mm long) were cast for each slab
the effect of the fiber orientation distribution on the
element using metallic molds.
mechanical performance through suitable and repre-
The slabs and the companion elements were
sentative experimental validation. In this paper that
covered with a tarp for one day after cast and then
design approach has been pursued in the framework of
left curing at ambient conditions for over six months.
a large ongoing research project on structural effi-
Prismatic elements (50.8 mm wide, 50.8 mm thick
ciency of fiber reinforcement which comprises tests at
and 431.8 mm long) were then cut from one of the slab
both material and semi-structural levels. The experi-
elements using a table saw. The prismatic elements
mental validation and results presented in this paper
were cut at three different inclinations with respect to
aim at studying and discussing the current approach to
the direction of the flow during the casting; parallel,
account for the fiber orientation distribution effect on
perpendicular and at 45 with respect to the flow
the tensile mechanical properties at the material level.
direction as it is shown in the layout in Fig. 4.
For that purpose, the actual tensile properties were
quantified and the fiber orientation distribution was
assessed using specimens representative of the actual 3.2 Uniaxial direct tension test
conditions in structural elements. The correlation
between the performance at structural level and the Uniaxial direct tension tests were carried out on
design methodologies integrating the study at material prismatic specimens. The tests were performed fol-
level is going to be addressed through ongoing semi- lowing the test method developed by Graybeal and
structural tests, which are out of the scope of this Baby [4], which allows for testing both mold cast and
paper. extracted specimens. The specimens were tested under
actuator displacement control at a constant
3.1 Specimen preparation

A total of five slabs were cat using a proprietary


UHPFRC material, which basic formulation has been
detailed elsewhere [4]. The steel fibers used were non-
deformed, cylindrical, high tensile strength steel with
a diameter of 0.2 mm, a length of 12.7 mm, and a
minimum tensile strength of 2.4 GPa. A fiber rein-
forcement volume fraction of 2.0 % was used in this
study. The slabs were 3048 mm long, 914 mm wide
and 50.8 mm thick. The casting process aimed at
mimicking usual manufacturing processes for similar
structural elements. The formwork consisted of an
open wooden bottom part and a top acrylic plate kept
in place by using clamps in order to have a confined
flow, Fig. 3. A thin polyurethane layer was applied on
the internal faces of the wooden formwork to ensure Fig. 3 Slab elements formwork ready for casting
Materials and Structures (2017)50:55 Page 5 of 17 55

Fig. 4 Layout of prismatic elements cut from UHPFRC slab

large mapping capability. The final composed images


derived from the ESEM scanning were then processed
and analyzed using an open source image processing
software to identify the footprints of the fibers inter-
cepted at the cut plane [34]. In general, the procedure for
the fiber detection and analysis started by cropping the
composed images and then converting the gray-scale
image to a binary image using a thresholding algorithm.
In a subsequent step, the image was filtered to disregard
the small particles detected, using in this case a threshold
based on the area of the particles. Finally, ellipses were
fitted to the oval-shaped fiber footprints on the cut plane
and the dimensions and local position of each fiber were
Fig. 5 Uniaxial direct tension test, Graybeal and Baby [4] registered.

displacement rate of 0.00254 mm/s. Figure 5 shows a 4 Results and discussion


general detail of the test configuration, further details
can be obtained from Graybeal and Baby [4] 4.1 Tensile response

3.3 Image analysis The direct tension test method allowed for quantifying
the tensile response of both cast and extracted
After completion of the direct tension tests, a series of specimens. The stress versus average axial strain
image analysis were carried out on sections cut out from results for the four sets of specimens are shown in
the prismatic elements. The cross sections analyzed Fig. 6. Specimen sets F0, F45 and F90 correspond,
were cut perpendicular to the larger axis of the prismatic respectively, to prismatic specimens extracted from
elements, which also corresponded to the main loading the slab element at 0, 45 and 90 degrees with respect to
direction during the direct tension tests. The sections the direction of the flow during the casting. Specimen
were cut at a distance of 1.5 times the fiber length from set FEC corresponds to the companion prismatic
the main crack so that fiber orientation and distribution specimens cast in molds. The thin lines in Fig. 6
were representative of those at the crack location while correspond to individual specimens, while the thick
avoiding missing fibers that were actually pulled out lines are the averages for each specimen set. Table 1
during the tests [12]. The section were then polished summarizes the main average results for each speci-
under wet conditions. All samples were analyzed in a men set, i.e., compressive strength, elastic modulus,
FEI Quanta 650 ESEM using backscattered electron first cracking stress, average multi-cracking strength,
detector at 15 kV of voltage and MAPS software for and strain at localization.
55 Page 6 of 17 Materials and Structures (2017)50:55

related to the tensile strength of the unreinforced


matrix. The average strain at crack localization for sets
F45 and F90 was also around 50 % of the strain
observed for set F0. In general, the small differences
between the first cracking stress and the average multi-
cracking stress is directly related to the low strain-
hardening response, which is however observed as
indicated by the strain domain registered prior the
crack localization. In fact, the AFGC recommenda-
tions for UHPFRC defines three different types of
tensile constitutive laws, i.e., strain softening, low
strain-hardening, and high strain-hardening, which not
only depend on the material but also on the production
and placing methods [1]. Most of the UHPFRCs
currently available on the market correspond to low
strain-hardening fiber reinforced concrete, whose
average constitutive laws exhibit strain-hardening
Fig. 6 Tensile response of prismatic specimens
behavior but might be strain softening in terms of
the characteristic law. For those materials and from a
For the specimens tested a clear discontinuity was structural design standpoint, a maximum value of
observed at the moment of the first crack and thus the 0.0025 is usually adopted for the ultimate tensile strain
stress value at that local maximum was registered as in the tensile constitutive law, which is of the order of
the first cracking stress. Likewise, the ultimate strain the maximum value observed for sets F45 and F90.
and the corresponding stress were registered at the The reduction in the elastic modulus was less signif-
local maximum point where the softening tensile icant and not conclusive, it was, respectively, 5 and
response started. The specimen set F0, which corre- 10 % for specimen sets F45 and F90 in comparison to
sponded to specimens extracted parallel to the material specimen set F0. In general, the results confirm the
flow direction, overperformed the rest of the specimen anisotropy in the tensile mechanical properties, which
sets in terms of average cracking stress, average multi- is mostly due to fiber orientation effects induced by the
cracking stress, strain at localization and elastic casting conditions and the material flow. Moreover,
modulus. A significant reduction in the average first the results reinforce the need to explicitly account for
cracking stress and the average multi-cracking stress the fiber orientation distribution and thus the aniso-
was observed for specimen sets F45 and F90 in tropy of the tensile properties in the design guidelines.
comparison to specimen set F0. Those reductions,
over 50 % for set F90 and 40 % for set F45, suggest a 4.2 Fiber orientation
strong influence of the fiber orientation distribution
not only on the post-cracking response, usually The actual fiber orientation distribution was studied
determined by the fiber bridging mechanisms, but through an image analysis method. Twelve cross
also on the first cracking stress, which is sometimes sections from prismatic specimens previously tested

Table 1 Tensile response of prismatic specimens


Set Compressive strength Elastic modulus First cracking stress Average multi-cracking Strain at localization eu
(MPa) (GPa) (MPa) stress (MPa) (m/m)

F0 176.5 63.5 9.9 11.4 0.0060


F45 60.3 7.0 7.1 0.0027
F90 57.1 5.1 5.6 0.0029
FEC 59.3 8.5 10.1 0.0035
Materials and Structures (2017)50:55 Page 7 of 17 55

specimen sets, i.e, specimens extracted from the slab


element at 0, 45 and 90 degrees with respect to the
direction of the material flow, as well as mold cast
specimens.
Table 2 summarizes the main results from the
image analysis completed. The average number of
fibers detected on the cross sections for each specimen
are reported along with the calculated orientation
factors. The average orientation factors were calcu-
lated first based on the number of fibers detected in the
cross sections, Eq. 1, and second based on the
estimated inclination of the fibers with respect to the
normal vector to the cross section, Eq. 2.
The average number of fibers detected on the cross
sections decreased for specimen sets F45 and F90 in
comparison to specimen sets F0 and FEC. Therefore,
the orientation factor calculated as defined by Eq. 1
decreased as well. An orientation factor value of 0.72
Fig. 7 Image analysis, representative cross sections; FEC (S- was obtained for specimen set F0, for which the
41M), F0 (S-9), F45 (S-18), F90 (S-23)
average amount of fibers detected was around twice of
the average amount of fibers detected for the specimen
under the direct tension test method were analyzed. set F90, whose fiber orientation factor was calculated
The studied sections were perpendicular to the loading as 0.37. In turn, the orientation factor calculated as
direction during the tension tests. Figure 7 shows defined by Eq. 2, which considers not only the number
representative cross sections for the different of fibers but also their inclination with respect to the

Table 2 Fiber orientation factor values for specimen sets F0, F45, F90, and FEC
Casting method Vf df lf Specimen N fibres Orientation fct;max eu
(%) (mm) (mm) factor (MPa)
Eq. 1 Eq. 2

Extracted specimens Extracted at 90 2.0 0.20 13 S5-0 629 0.43 0.71 6.4 0.0041
(3000 9 1000 9 50 mm (perpendicular to S23-0 492 0.33 0.60 6.1 0.0028
horizontally cast slab) flow direction)
S46-0 543 0.36 0.65 7.3 0.0031
F90
Average 555 0.37 0.65 6.6 0.0033
Extracted at 45 S18-45 775 0.52 0.70 7.3 0.0031
(with respect to S39-45 843 0.57 0.75 6.7 0.0023
flow direction)
S59-45 937 0.63 0.77 9.7 0.0054
F45
Average 852 0.57 0.74 7.9 0.0036
Extracted at 0 S9-90 1112 0.75 0.86 12.3 0.0039
(parallel to flow S28-90 1160 0.71 0.83 13.9 0.0065
direction)
S52-90 1036 0.70 0.80 12.8 0.0078
F0
Average 1103 0.72 0.83 13.0 0.0061
Mold cast specimens Pour from one end S41M 1079 0.72 0.85 9.0 0.0037
(50.8 9 50.8 9 431.8mm) FEC S42M 1001 0.67 0.85 10.8 0.0043
S46M 1061 0.71 0.86 9.4 0.0023
Average 1047 0.70 0.85 9.73 0.0034
55 Page 8 of 17 Materials and Structures (2017)50:55

main longitudinal axis of the prismatic specimen, calculated according to Eq. 1 in two or three orthog-
decreased from 0.83 for specimen set F0 to 0.65 for onal directions. As for the data reported in Table 3, the
specimen set F90. orientation factor aeq:1;1 refers to the factor calculated
Table 3 compiles results from previous studies in the cross section perpendicular to the direction of
completed on UHPFRC components and where the the principal tensile stress applied, aeq:1;2 refers to the
orientation factor was directly evaluated. Some factor calculated in the cross section perpendicular to
authors reported values of the orientation factor the main transverse axis of the element and thus

Table 3 Fiber orientation factors on UHPFRC specimens—review


Reference Casting method Vf (%) df (mm) lf (mm) Specimen Orientation factor ftu (MPa) eu
set
aeq:1;1 aeq:1;2 aeq:1;3 aeq:2;1

Osterlee [11] Extracted specimens 3.00 0.16 13 T2H 0.19 0.79 – – 2.9a –
Vertically cast T6H-1 0.67 0.49 – – 9.7a c
panel a c
3000 9 1500 mm T6H-2 0.74 0.39 – – 14.9
T7H-1 0.79 0.36 – – 12.8a c

T2V 0.63 0.53 – – 7.4a c

T4V 0.75 0.55 – – 14.1a c

T6V 0.53 0.50 – – 12.2a c

Ferrara et al. Horizontally cast 1.27 0.16 13 A 0.85 0.44 – – – –


[9] slabs 1000 9 500 B 0.76 0.54 – – – –
mm poured from
center of: A. long
edge, B. short edge
Wuest [35] Horizontally cast 6.00 0.20 10 CM0-98-T4 0.66 0.57 0.25 – 10.7a 0.0010
dog-bones 100 mm CM22-94-T5 0.53 0.67 0.35 – 10.4a d
central width
CM23-P-T1 0.77 0.57 0.33 – 14a 0.0011
4.00 0.16 13 HIFCOM-14- 0.70 0.38 0.24 – 13a 0.0024
T2
Horizontally cast 6.00 0.20 10 CM0-05-TE1 0.37 0.72 0.61 – 5.2a –
rectangular plates CM22-3-e 0.65 0.53 0.34 – 14a 0.0029
200 mm central
width
UHPFRC overlay 6.00 0.20 10 SAMD2 0.58 0.68 – – – –
Wille [12] Beam specimens 1.50 0.18 6 S1 0.67 – – 0.66 16.5b –
150 9 150 9 500 1.25/0.75 0.18/0.18 6/18 S2 0.65 – – 0.65 27.2b –
mm cast from one
end S3 0.69 – – 0.66 17.0b –
S4 0.66 – – 0.64 15.5b –
1.50 0.15 13 S5 0.78 – – 0.78 24.9b –
S6 0.74 – – 0.78 24.4b –
S7 0.71 – – 0.79 20.8b –
4.85 0.18 9 S8 0.65 – – 0.65 27.9b –
S9 0.65 – – 0.67 31.7b –
S10 0.59 – – 0.63 26.7b –
1.0/2.0 0.18/0.15 9/13 S11 0.81 – – 0.73 27.7b –
S12 0.65 – – 0.69 27.5b –
S13 0.86 – – 0.74 32.4b –
1.0/2.65 0.18/0.30 9/17.5 S14 0.65 – – 0.67 24.3b –
S15 0.69 – – 0.70 25.1b –
1.0/3.5 0.18/0.30 9/17.5 S16 0.62 – – 0.70 29.8b –
S17 0.63 – – 0.70 30.0b –
1.25/2.68 0.18/0.30 6/17.5 S18 0.64 – – 0.69 26.9b –
S19 0.71 – – 0.69 27.0b –
1.0/1.5 0.18/0.38 9/30 S20 0.69 – – 0.66 24.3b –
Materials and Structures (2017)50:55 Page 9 of 17 55

Table 3 Fiber orientation factors on UHPFRC specimens—review


Reference Casting method Vf (%) df (mm) lf (mm) Specimen Orientation factor ftu (MPa) eu
set
aeq:1;1 aeq:1;2 aeq:1;3 aeq:2;1

S21 0.75 – – 0.69 30.4b –


1.0/1.78 0.18/0.15 6/13 S22 0.78 – – 0.76 26.5b –
S23 0.83 – – 0.78 35.3b –
c
Xia and Mackie [14] Prisms 50.8 9 50.8 2.0 0.20 13 FL1 0.69 – 0.41 – –
g c
9 431.8 mm cast FL2 0.91 – 0.31 – –
from one end
Kang and Kim [36] Dog-bones cast 2.0 0.20 0.13 PL1 0.64f – – 0.64 16.04a c

parallel to tensile PL2 0.71f – – 0.66 16.03a c


direction
PL3 0.72f – – 0.65 16.08a c

f a c
Dog-bones cast TL1 0.63 – – 0.41 12.67
perpendicular to TL2 0.68 f
– – 0.46 10.67 a c
tensile direction f a c
Tl3 0.64 – – 0.42 12.06
Kang et al. [13]e Beams 2.0 0.20 13 PL-TC 0.66f – – 0.70 – –
100 9 100 9 400 PL-HC – – 0.57f 0.49 – –
mm poured
parallel (PL) and PL-VC – 0.61f – 0.53 – –
f
perpendicular (TL) TL-TC 0.62 – – 0.56 – –
to tensile direction. TL-HC – – 0.62f 0.59 – –
Sections cut in
transverse (TC), TL-VC – 0.69f – 0.62 – –
Horizontal (HC)
and Vertical (VC)
direction
Yoo et al. [37] Beam specimens 2.0 0.20 13 S1-E 0.68 – – 0.75 – –
100 9 100 9 400 S2-C 0.70 – – 0.74 – –
mm cast from one
end (E) and center 16.3 S3-E 0.67 – – 0.75 – –
(C) S4-C 0.69 – – 0.75 – –
19.5 S5-E 0.68 – – 0.73 – –
S6-C 0.68 – – 0.75 – –
30 S7-E 0.65 – – 0.75 – –
S8-C 0.67 – – 0.73 – –
a
ftu obtained through direct tension test
b
Equivalent bending strength obtained on notched specimens under three-point loading
c
Specimens exhibited strain hardening but specific data was not reported
d
Atypical specimen from the set, did not exhibit strain hardening
e
Average values
f
Estimated from data reported
g
Electromagnetic field imposed on the specimen during casting

parallel to the direction of the principal tensile stress et al. [13] where the analysis were completed at
applied, and aeq:1;3 refers to the factor calculated in the longitudinal, transverse and vertical sections. The
cross section perpendicular to the transverse axis term ft;u corresponds to either the maximum tensile
defining the element height and thus parallel to the stress obtained through direct tension tests or the
direction of the principal tensile stress applied. The ultimate equivalent flexural stress obtained in bending
orientation factor values reported according to Eq. 2, tests. Finally, eu corresponds to the ultimate tensile
denominated aeq:2;1 , correspond to the factor calcu- strain before the single crack localization for those
lated for the cross section perpendicular to the elements tested under direct tension test configura-
direction of the principal tensile stress applied, with tions and which exhibited some degree of strain
the only exception of the results reported by Kang hardening behavior.
55 Page 10 of 17 Materials and Structures (2017)50:55

In general, the calculated orientation factor values orientation following the material flow field, which,
are higher for mold cast specimens and for specimens defined by the closed formwork and the material being
extracted parallel to the casting direction, i.e., spec- poured at one end of the slab element, might have been
imens along the main direction of predominantly shear predominantly shear governed. As noted by Martinie
governed material flows. The orientation factor values and Roussel [10], the shear induced orientation might
calculated for specimen sets F0 and FEC using Eq. 1, be almost instantaneous in the conditions of industrial
0.72 and 0.70 respectively, agree well with the values casting, which was the case for the conditions intended
reported in Table 3 for specimen sets PL1-3 [36], PL-T in this research. Recent numerical analysis completed
[13], S1 and S2 [37], and FL1 [14]. Those specimens by Karihaloo and Kulasegaram [22] showed that fibers
were cast in molds using a similar type and volume of in shear governed flows tend to reorient themselves
fiber reinforcement as the ones used in this study and with the direction of the flow, irrespective of the fiber
their casting processes might have led to the develop- volume fraction, which in their case of study led to
ment of favorable material flows in terms of expected orientation factor values around 0.90.
fiber orientation. Likewise, the orientation factor Graphical evidence of the fiber orientation distri-
values for sets F0 and FEC agree well with the values bution can also be observed in Fig. 8, which shows the
calculated for some of the specimens extracted from histograms for the roundness distribution of the fibers
structural components at areas were well defined shear detected in some representative cross sections. The
material flow patterns were expected and along the roundness is defined as the ratio between the minor
expected preferential fiber orientation direction, e.g., and the major axis of the fitted ellipses, so that the
specimens CM0-98-T4, CM23-P-T1, HIFCOM-14- roundness is 1.0 for a circular element and it
T2 and CM22-3-e [35], as well as specimens T6-H,T2- approaches to zero for very elongated elements. The
V, T4-V [11]. Furthermore, the orientation factor roundness distribution for specimen sets F0 and FEC
calculated for specimen set F90 through Eq. 1, which is skewed to the right, i.e, the detected fibers tended to
led to a value of 0.37, agrees well with the factor value be oriented perpendicular to the cut section and
calculated for specimen CM0-05-TE1 [35], for which parallel to the direction of the flow. That preferential
the fibers were also expected to be predominantly fiber alignment is not evident for specimens corre-
oriented perpendicular to the principal tensile stressed sponding to sets F45 and F90 which were extracted at
direction. Even lower orientation factor values have 45 and 90 with respect to the direction of the
been reported for specimens extracted from areas with material flow during the casting and for which the
complex and more unfavorable material flow patterns, detected fibers tended to be less perpendicular to the
e.g, specimen T2H in Table 3 [11]. vector normal to the cut section analyzed.
The calculation of the orientation factor through Although it is not possible to establish a direct
Eq. 2 is more time consuming and labor intensive than comparison for the tensile response of specimens from
the fiber counting required for calculation through different studies, the values reported in Tables 2 and 3
Eq. 1. The former approach does provide a better evidence the correlation between the orientation factors
representation of the actual fiber orientation distribu- and the tensile response in terms of strength and strain
tion, however, it is also more sensitive to image quality capacity for individual studies. In particular and for the
as well as to the capabilities and limitations of the specimen sets in this study, the fiber orientation distri-
image analysis methodology implemented. An aver- bution observed in Fig. 8 as well as the orientation factor
age orientation factor value of 0.83 was calculated for values shown in Table 2 correlate well with the tensile
specimen set F0 using Eq. 2, which evidences again response results discussed in Sect. 4.1, which demon-
the preferential alignment of the fibers in the direction strate the strong influence of the fiber orientation
of the material flow. Similar values were reported by distribution on the tensile strength and the effectiveness
Wille [12] for mold cast specimens where the material of the fiber bridging mechanisms. As the fibers deviate
was let flow along an inclined 1.0 m long chute before from the orientation perpendicular to the cross section,
being poured at one end of the beam elements. and thus the fiber orientation factor decreases, the tensile
Specimen sets F0 and FEC exhibited similar evidence response is affected, as observed for specimen sets F45
of preferential alignment. In particular for specimen and F90. This unfavorable fiber orientation distribution
set F0, fibers might have adopted a preferential might lead to the reduction or loss of the strain capacity,
Materials and Structures (2017)50:55 Page 11 of 17 55

Fig. 8 Histograms of roundness distribution

due to the low effectiveness of the fiber bridging load capacity in a similar range [40]. From a structural
mechanisms, as well as to the reduction of the tensile point of view Martinie and Roussel [10] proposed that
capacity. Lower cracking stress and no evidence of strain fibers can be considered as fully oriented when they
hardening were observed for specimens exhibiting are oriented at less than 20 with respect to the main
unfavorable fiber orientation distribution in previous tensile stress field. Therefore, the induced fiber
studies, e.g., specimen T2H [11] and specimen CM0-05- orientation might account for the differences in the
TE1 [35]). Oesterlee referred to fibers as local defects that tensile response of the specimen sets where the fibers
might have a weakening effect on the tensile capacity and were not preferentially aligned to the main loading
estimated, through a simplified linear elastic fracture direction. However, further specific research is
mechanics approach, that the stress concentration at the required to quantify the combined and total effect of
edges of the fiber cross section, considered as a local the hypothesized mechanisms, as well as other fiber
defect, increases by a factor of at least 3 and it increases and matrix related mechanisms (e.g., snubbing, fiber
steeply for elliptic defects [11]. The more inclined the bending, matrix spalling) on the cracking strength and
fibers are with respect to the main tensile stressed post-cracking behavior in sections with non-preferen-
direction, the larger the weakening effect might be. tial fiber alignment.
Furthermore, many authors agree with the existence of an
optimal fiber orientation which improves the ultimate 4.3 Fiber orientation considerations for design
load capacity and the material toughness in terms of
energy absorption capacity. The maximum pullout load The general concept of a material reduction factor
for a single straight steel fiber has been shown to slightly accounting for the non-uniform fiber orientation dis-
decrease for angles up to 30 with respect to load tribution and the subsequent anisotropic tensile
direction, which corresponds to an orientation factor response have been widely discussed [20, 24]. The
of 0.87, while it decreases more sharply for larger direct translation of the fiber orientation assessments
angles [38, 39]. Moreover, specific pullout studies on into meso-mechanical models have been suggested as a
UHPFRC also suggested the existence of a maximum reliable way to account for the material anisotropy in
55 Page 12 of 17 Materials and Structures (2017)50:55

UHPFRC [11, 14, 22, 35]. Wille et al. [12] developed a cast specimens used to determine the intrinsic post-
shape function concept coupling the spatial and cracking tensile material law and the actual orientation
orientation distribution of the fibers, estimated through of the fibers in the structural element. The term
the use of Eqs. 1 and 2 in discrete sections, which were intrinsic in such an approach refers to the material
then incorporated in a backward analysis. However, properties measured through standard or common test
this model, as well as other similar models in the methodologies, as it could be debatable whether there
literature, suffers from lack of generality. Some other is an intrinsic tensile response when the properties
proposed models rely only on fiber counting and, thus, depend on factors like the geometry of the specimen,
on the fiber orientation factor defined by Eq. 1, which is the casting process and the test method. The method-
then coupled with fiber efficiency factors in order to ology in the AFGC recommendations relies on the
establish the tensile response of UHPFRC. A meso- completion of suitability tests, which might sometimes
mechanical model following that approach was imple- be costly and resource demanding. The K factors are
mented by Wuest [35] and Oesterlee [11]. However, determined considering the tensile strength of the
the calculation of the fiber efficiency factor depends on material in the principal directions of tension in the
the orientation angle of the fibers crossing the section structure. Either direct tension test methods or four
or the estimation of its average value, which leads point bending test methods can be used to assess the
again to the need of explicitly analyzing the fiber tensile response and determine the K factor value, both
orientation distribution. For that purpose, the use of for local and global or overall conditions. The global
stereological principles might provide an alternative to factor, Kglobal , is the ratio of the mean of the peak of the
estimate the required average values [41]. In a different tensile response registered for the mold cast specimens
approach, Xia and Mackie [14] implemented a prob- to the mean peak of the tensile response registered for
abilistic model of the axisymmetric fiber distribution to the extracted specimens. In turn, the local factor,
quantify the global preference of fiber alignment, Klocal , is the ratio of the mean of the peak of the tensile
which only requires counting the total number of fiber response registered for the mold cast specimens to the
footprints in the cross section. Moreover, non-destruc- lowest value of the peak of the tensile response
tive techniques for monitoring fiber dispersion and registered for the extracted specimens [1].
orientation are also available [15, 17, 18], with those The importance of properly addressing the assess-
techniques constituting a feasible alternative to assess ment of the fiber orientation distribution and the
the fiber dispersion and the orientation distribution. determination of reliable orientation factors for the
Therefore, it is clear that despite the availability of a structural design of UHPFRC components has been
wide range of techniques to assess or estimate the highlighted in several deployed application. However,
dispersion and orientation distribution of the fibers in specific studies on the topic are scarce or the results are
structural elements, there is still a need for reliable and not always made available; therefore, the data is
general protocols to translate the fiber orientation limited to a number of specific projects [1, 42], some
distribution assessments and the corresponding fiber of them summarized in Table 4. The specimen
orientation factors into material reduction factors that extraction location needs to be carefully planned in
can be fully integrated into specific design codes and order to properly assess and reflect the influence of the
recommendations for UHPFRC and that reflect the fiber orientation distribution on the main stress
actual mechanical properties of the material at struc- transfer mechanisms engaged in a specific targeted
tural level. application, as it might be the case in prestress
Currently, the reduction factor concept proposed in transferring zones, shear governed regions or flexural
the AFGC recommendations for UHPFRC [1] is the elements. Moreover, the suitability tests allow for
most widely accepted approach to account for the better capturing the impact of complex flow conditions
anisotropic tensile response of UHPFRC in structural as well as other constructability issues that otherwise
elements. The recommendations provide specific might be underestimated. For instance, a planned
guidelines for the calculation of material reduction break during concreting or the intersection of different
factors (K factors) to take into account the difference flow fronts might lead to higher reduction factors or
between the fiber orientation distribution in the mold the adoption of additional reinforcement strategies, as
Materials and Structures (2017)50:55 Page 13 of 17 55

Table 4 K factors—review
Project Element Sample K Factor
Kglobal Klocal

Bourg-Lès-Valence p beam Web 45° 1.03 1.46


(2001-02) Web vertical 0.83 ? 1.00 1.22
Web horizontal [K factors adopted] 1.25 1.72
Upper flange (transverse) 1.09 1.34
Upper flange (longitudinal) 0.88 ? 1.00 1.14
Saint-Pierre-la-Cour (2005) I beam Web 45°, zone B2/B7 0.73 ? 1.00 0.86 ? 1.00
Web 45°, zone B3/B6 0.68 ? 1.00 1.36
PS34 Overpass (2005) Box beam Web (vert.), upper slab (transv.), lower 1.50 –
slab (transver.) samples. [Single
K factor adopted]
Pinel bridge (2007) Inv. T beam Variable web thickness. Web (horz., vert., 1.33 1.75
60°) samples. [K factor maximum of the
3 zones]
Pont du Diable (2009) Footbridge (Shear design) Web 45°, zone 1 0.79 ? 1.00 0.85 ? 1.00
Web 45°, zone 2 1.24 1.37
Web vertical, zone 1 0.93 ? 1.00 1.04
Web vertical, zone 2. [K factors adopted] 1.26 2.12
Achères plant (2010) Shell Bearing zone where prestressed force was 1.35 1.55
introduced. Longitudinal samples
Midspan zone for bending validation. 1.20 1.65
Longitudinal samples

reported for the PS34 Overpass and the Pont the direction, the value of the K factors would be higher;
Diable projects. [43, 44]. 1.39 and 1.68 for local and global conditions,
The K factors for each specimen set in this study respectively.
were calculated based on the results from the direct As mentioned before, the translation of the fiber
tension tests carried out. The values were corrected to orientation factors calculated based on image analysis
account for the effect of the forms and the sawn or other non-destructive techniques into robust design
surfaces on the fiber orientation distribution [1, 19]. factors for the tensile response of UHPFRC is not
The global and local K factors obtained for each completely straightforward. There is not currently a
specimen set are reported in Table 5. In general, the K general and reliable approach to determine the K factor
values obtained for the specimen sets in this study values from the results of non-mechanical assess-
agree well with values reported for similar structural ments. The lack of such approach as well as the
components, see Table 4. The preferential alignment misinterpretation of those non-mechanical assess-
of the fibers is once more evident in the results of ments might lead in some cases to excessively
specimen set F0, for which the average values penalizing the mechanical properties and, therefore,
calculated for the K factor were below 1.0. As an limiting or completely eliminating the comparative
illustrative example, the factors to be used in the case advantages that the use of UHPFRC offers for
of a similar structural element where the stress field structural design.
were mainly oriented at 45 with respect to material Figure 9 shows the values of the K factors
flow direction would be 1.07 and 1.37 for global and calculated for the specimen sets tested in this study
local conditions, respectively. In the hypothetical along with the global and local K factor values
unfavorable condition of an element subjected to a recommended for preliminary analysis in the AFGC
stress field perpendicular to the material flow recommendations for UHPFRC [1]. In the same
55 Page 14 of 17 Materials and Structures (2017)50:55

Table 5 Material reduction factors; K factors and Ka


Set Peak stress K factor Ka
Average (MPa) Min (MPa) Kglobal Klocal Ka;Eq:1 Ka;Eq:2

Maya and Graybeal FEC 10.9 9.6


FE0 12.4 10.7 0.69 ? 1.00 0.80 ? 1.00 0.98 1.08
FE45 8.1 6.3 1.07 1.36 1.23 1.34
FE90 6.1 5.1 1.39 1.68 1.88 1.57
Oesterlee [11]a T-Mold 10.8
T-4/7H 10.5 9.1 0.95 ? 1.00 1.09 0.94 –
T-1/3H 3.2 2.6 3.06 3.80 3.61 –
a
Values estimated from limited data

of UHPFRC materials. Although there are a number of


fiber orientation assessments reported in the literature,
some of them already summarized in Table 3, the data
is limited and similar comparisons can not be estab-
lished for all sets. Oesteerle [11] studied a vertical cast
panel and identified five different sections according
to the estimated flow pattern. Although the number of
tests is limited for a reliable calculation of the
K factors, a rough estimation led to the values reported
in Table 5 for two orthogonal directions. A high
K factor value was estimated for specimens where the
fibers were expected to be aligned perpendicular to the
principal tensile direction, which agrees well with the
Fig. 9 Material reduction factors; K factor and Ka low value of the fiber orientation factor calculated
figure the results from the image analysis completed in through Eq. 1 and reported in Table 3 (Specimen
this study are represented. In order to follow a similar T2H). In that study the assessment of the fiber
approach as the one adopted in the AFGC recommen- orientation distribution for sections of specimens cast
dations for the K factors, the fiber orientation factors in molds was not reported. However, the value of the
obtained from the image analysis for the extracted factor Ka was estimated assuming a value of 0.69 for
specimens were normalized to the average value the fiber orientation factor, which represents the
obtained for the mold cast specimens. The values Ka average of the factor calculated using Eq. 1 for
shown in Fig. 9 were derived from Eqs. 1 to 2 and were specimens in Table 3 which were also cast in moulds
calculated as aFEC =aFðiÞ and acosðaFðiÞ Þ=acosðaFEC Þ, and with cross sections similar to the used by Oesterlee
respectively [11]. Likewise, the assumed value agrees well with the
Figure 9, although only illustrative, establishes a value of 0.70 obtained for the mould cast specimens in
visual comparison of different fiber orientation assess- the present study. The Ka values for those two
ments; those derived from the image analysis and orthogonal specimen sets are also reported in Table 5.
those based on the measured mechanical response. A The assessment of the fiber dispersion and orien-
correlation between the tensile mechanical response tation distribution, which can be completed using
and the fiber orientation distribution is observed. either destructive and non-destructive techniques,
Moreover, the figure illustrates the difficulty in certainly offers opportunities to control and predict
developing a unified approach to determine robust the material performance through the optimization of
and reliable design factors to take into account the the material flow, the formwork and the casting
fiber orientation distribution effect on the tensile law process for specific applications. Moreover, such
Materials and Structures (2017)50:55 Page 15 of 17 55

optimization might eventually lead to a lowering of overdue. The direct tension test method has proven to
the material reduction factors and, thus, allow for fully be a reliable test method to characterize the mechanical
exploiting the properties of the UHPFRC materials. tensile response of UHPFRC. The test method allows
Therefore, the implementation of fiber dispersion and for testing both cast and extracted specimens and thus
orientation distribution assessments along with stan- directly assessing the actual material properties within
dardized tensile test methods to fully quantify the structural elements along different directions.
intrinsic tensile response of UHPFRC might allow for The experimental results suggest a strong influence
establishing a robust and reliable methodology to of the fiber orientation distribution not only on the post-
determine design factors accounting for the fiber cracking response of UHPFRC materials (average
orientation. Those factors could be then implemented multi-cracking stress, strain domains, strain at local-
in meso-mechanical models to predict the tensile ization), but also on the first cracking stress. Further
mechanical response of UHPFRC materials and research is needed to better understand and quantify the
engaged in macro-mechanical models for designing impact that preferential fiber alignments might have on
structural components. the first cracking stress of UHPFRC, which are
The experimental evidence presented in this paper, characterized by a relatively high fiber volume.
as well as a large part of the references available, deal Image analysis techniques provide sound evidence
with elements cast under predominant shear flow of the impact of the flow pattern and the casting
patterns, while other flow patterns (e.g extensional, process on the actual fiber orientation distribution
converging, diverging) have been less studied [9, 45]. within a structural element. However, they are time
A better understanding and estimation of the different consuming and labor intensive, which might limit their
flow patterns might be crucial to establish methodolo- implementation in quality control procedures. Alter-
gies for the assessment of the fiber orientation distri- natively, non-destructive techniques are also available
bution and the determination of reliable constitutive and might constitute a feasible option for quality
models for design methodologies and simulation tools. control.
Finally, the exceptional properties of UHPFRC The assessment of the fiber orientation distribution
materials demand comprehensive design approaches in structural elements, or its estimation through
enabling the material properties and the casting simulation tools, might be useful for further optimiza-
processes to be tailored in order to achieve a specific tion of the material flow, the formwork and the casting
structural performance [9]. The reduction factor process for each specific application. However, the
approach is one of the key concepts to be integrated translation of those fiber orientation assessments into
in that comprehensive design framework. The robust design safety factors might not be completely
approach has proven so far to be a reliable method to straightforward.
account for the inherent variability of the fiber The reduction factor concept adopted in the AFGC
orientation and distribution and, thus, the tensile recommendations for UHPFRC [1], and more recently
properties of UHPFRC in large scale applications integrated in the fib Model Code 2010 [30], has proven
[42]. However, further research is required to develop to be a robust approach to account for the fiber
reliable, cost-effective and quality control oriented orientation distribution impact on the tensile mechan-
methodologies for the determination of the reduction ical response of UHPFRC. In particular, the reduction
factors. factor values obtained in this experimental validation
were consistent with those previously reported for
similar elements and of the order of the preliminary
5 Conclusions values suggested in the AFGC recommendations for
UHPFRC.
The present study emphasizes the importance of The reduction factor approach is a key concept in a
accounting for the fiber orientation distribution and comprehensive design framework for UHPFRC struc-
the anisotropy of the tensile properties in design tures. The implementation of fiber dispersion and
guidelines for UHPFRC. orientation distribution assessments along with stan-
The development of standard test methods to dardized tensile test methods to fully quantify the
quantify the mechanical response of UHPFRC is intrinsic tensile response of UHPFRC are necessary
55 Page 16 of 17 Materials and Structures (2017)50:55

for the development of a robust and reliable method- 11. Oesterlee C (2010) Structural response of reinforced
ology to determine material design factors accounting UHPFRC and RC composite members, Doctoral Disserta-
tion. EPFL, Lausanne
for the fiber orientation. 12. Wille K, Tue NV, Parra-Montesinos GJ (2014) Fiber distri-
Further research is required to better understand the bution and orientation in UHP-FRC beams and their effect on
main parameters affecting the tensile response at backward analysis. Mater Struct 47(11):1825–1838
structural level, thus eventually leading to refine the 13. Kang ST, Lee BY, Kim J, Kim YY (2011) The effect of fiber
distribution characteristics on the flexural strength of steel
material reduction factors and fuller exploitation of the fibre-reinforced ultra high strength concrete. Constr Build
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well as structural element typologies are among the 14. Xia J, Mackie K (2014) Axisymmetric fiber orientation
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Acknowledgments The research discussed herein could have fibres distribution in a steel fibre reinforced concrete with
been not possible without the dedicated effort and support of the electrical resistivity measurements. NDT E Int 41(8):638–647
federal and contract staff associated with the FHWA Structural 16. Martinie L, Lataste JF (2015) Fiber orientation during
Concrete Research Program. Special recognition goes to Corey casting of UHPFRC: electrical resistivity measurements,
Hollmann, Brian Nakashoji and Jose Muñoz for their valuable image analysis and numerical simulation. Mater Struct
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support of the U.S National Research Council through its 17. Ozyurt N, Mason TN, Shah SP (2006) Non-destructive
Postdoctoral Research Associateship Program. monitoring of fiber orientation using AC-IS: an industrial
scale application. Cem Concr Res 36(9):1653–1660
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