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ETCH TESTS alcohol, and then drying them. The etched surface may
then be preserved by coating it with a thin clear lacquer.
K-1
(c) Aluminum Alloy. The following etching solution
(a) Carbon and Low Alloy Steels. Etching solutions is suggested for revealing the macrostructure of welded
suitable for carbon and low alloy steels, together with aluminum alloy specimens:
directions for their use, are suggested as follows.
Hydrochloric Acid (conc.) 15 ml
(1) Hydrochloric Acid. Hydrochloric (muriatic) Hydrofluoric Acid (48%) 10 ml
acid and water equal parts by volume. The solution Water 85 ml
should be kept at or near the boiling temperature during
the etching process. The specimens are to be immersed This solution is used at room temperature and etching
in the solution for a sufficient period of time to reveal is accomplished by either swabbing or immersion of
all lack of soundness that might exist at their cross- the specimen. The surface to be etched should be
sectional surfaces. smoothed by filing or machining or by grinding on
No. 180 Aloxite paper. With different alloys and tempers
(2) Ammonium Persulfate. One part of ammonium
the etching period will vary from 15 sec to several
persulfate to nine parts of water by weight. The solution
minutes and should be continued until the desired
should be used at room temperature and should be
contrast is obtained.
applied by vigorously rubbing the surface to be etched
with a piece of cotton saturated with the solution. The
etching process should be continued until there is a
clear definition of the structure in the weld. CLOSURE OF OPENINGS
(3) Iodine and Potassium Iodide. One part of RESULTING FROM SECTIONING
powdered iodine (solid form), two parts of powdered K-2
potassium iodide, and ten parts of water, all by weight.
The solution should be used at room temperature and (a) Holes in welded joints left by the removal of
brushed on the surface to be etched until there is a trepanned plug specimens may be closed by any welding
clear definition of outline of the weld. method approved by the authorized inspector. Some
(4) Nitric Acid. One part of nitric acid and three suggested methods for closing round plug openings by
parts of water by volume. welding are as follows.
(1) Insert and weld in special plugs of which some
CAUTION: Always pour the acid into the water. Nitric acid causes acceptable types are shown in Fig. K-2. Type (a) is
bad stains and severe burns.
adapted to welding from both sides and should be used
The solution may be used at room temperature and wherever that method is practicable, and Types (b) and
applied to the surface to be etched with a glass stirring (c) when access is possible only from one side. The
rod. The specimens may also be placed in a boiling diameter of the filler plug shall be such as to make a
solution of the acid but the work should be done in snug fit in the hole to be filled. Each layer of weld
a well-ventilated room. The etching process should be metal as deposited shall be thoroughly peened to reduce
continued for a sufficient period of time to reveal all residual stresses. The 1⁄4 in. (6 mm) hole in the center
lack of soundness that might exist at the cross-sectional of the plugs shown in Fig. K-2 may afterwards be
surfaces of the weld. closed by any reasonable method. Plain plugs without
(b) The appearance of the etched specimens may be a hole may be used.
preserved by washing them in clear water after etching, (2) For joints where the thickness of the thinner
removing the excess water, immersing them in ethyl plate at the joint is not greater than one-third of the
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