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Composite Structures 75 (2006) 192–198

www.elsevier.com/locate/compstruct

Failure of carbon composite-to-aluminum joints


with combined mechanical fastening and adhesive bonding
Jin-Hwe Kweon *, Jae-Woo Jung, Tae-Hwan Kim, Jin-Ho Choi, Dong-Hyun Kim
School of Mechanical and Aerospace Engineering, Research Center for Aircraft Parts Technology, Gyeongsang National University,
Jinju, Gyeongnam 660-701, Republic of Korea

Available online 19 May 2006

Abstract

Composite-to-aluminum double lap joints were tested to obtain the failure loads and modes for three types of joints: adhesive bond-
ing, bolt fastening and adhesive-bolt hybrid joining. A film type adhesive FM73 and a paste type adhesive EA9394S were used for alu-
minum and composite bonding. A digital microscope camcorder was used to monitor the failure of the joints. It was found that hybrid
joining improves joint strength when the mechanical fastening is stronger than the bonding, as when the paste type adhesive is used. On
the other hand, when the strength of the bolted joint is lower than that of the bonded joint, as when the film type adhesive is used, bolt
joining contributes little to the strength of the hybrid joint.
 2006 Elsevier Ltd. All rights reserved.

Keywords: Composite joint strength; Hybrid joint; Adhesive bonding; Mechanical fastening

1. Introduction well-proven joining method compared to bonding meth-


ods. Any number of papers can easily be found about
Application fields for composite materials are continu- mechanical joints that use bolts, rivets, or pins. These
ously expanding, from traditional application areas such papers consider various approaches, including the charac-
as military aircraft to various engineering fields including teristic length method [1,2] and the 3-dimensional finite ele-
commercial aircrafts, automobiles, robotic arms and even ment method [3,4] and/or test [5,6].
architecture. Unless all the parts are co-cured (for compo- In mechanical fastening, ironically, the fasteners them-
sites) or integrally machined (for metals), it is inevitable that selves are an important source of weight increase. Particu-
joints will be used to connect the parts. Accordingly, joint larly in weight-sensitive structures like aircraft, reducing
design technology became a critical and common technol- the number of fasteners is a research priority. Adhesive
ogy for the design of composite parts. The structural integ- bonding can be considered as an alternative joining method
rity of the composite parts actually depends on the joint. [7–12]. In adhesive bonding, the fastener and fastening
When mechanical joints such as bolting or riveting are holes are unnecessary. The stress distributions in the joint
used in composite structures, reinforcing fibers must be are relatively uniform compared with those in the mechan-
cut to fabricate the fastener hole, around which the stress ical joint. However, it is problematic that the bonded joint
concentration occurs. The use of fastener holes inherently cannot be disassembled without damage. Also, these joints
results in micro and local damages to the composite are very sensitive to environmental factors like humidity
laminate during their fabrication. Consequently, strength and temperature. The most serious problem for adhesive
degradation of the structures is induced. Although bonding, however, is that design engineers are uncertain
mechanical fastening has many weak points, it is still a regarding long-term structural integrity and, further,
bonded joints tend to fail instantaneously, not progres-
*
Corresponding author. Tel.: +82 55 751 6104; fax: +82 55 757 5622. sively. Even if a bonded joint meets strength requirements
E-mail address: jhkweon@gsnu.ac.kr (J.-H. Kweon). in laboratory testing, some designers worry about whether

0263-8223/$ - see front matter  2006 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compstruct.2006.04.013
J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198 193

the bonding will work with the designed target perfor- were tested for the bonded and hybrid joints, respectively.
mance throughout the whole life span of the joint. For the joint with paste type adhesive EA9394S, four and
In the hybrid joint, mechanical fastening is added to the six specimens were tested for the bonded and hybrid joints,
bonded joint. The hybrid joint uses mechanical fastening in respectively. Another four bolted joint specimens were
addition to bonding in an effort to overcome the potential tested to obtain the bearing strength.
weaknesses of adhesive bonding. Optimally designed A schematic configuration showing the dimensions of
mechanical fastening might induce more progressive failure the hybrid joint is illustrated in Fig. 1. The bonded area
propagation and increase joint strength. Although some is a square measuring 25.4 mm · 25.4 mm. The fastener
studies [13,14] on hybrid joints have been reported, still hole diameter is 4.763 mm. A NAS6203-05 steel bolt was
failure and strength data for the hybrid joint are lacking. used for the mechanical fastening and an aluminum
In this paper, the effect of bolting on the joint strength is washer, NAS1149D0463K, was used on both the top and
studied by testing the effect of adding a bolt joint to a the bottom sides of the joint. The bolt was tightened man-
bonded joint, which makes a hybrid joint. Tests were con- ually just for contact.
ducted for the three types of joints: simple bonding, simple The stacking sequence of the composite laminate is
bolting and combined bonding and bolting (hybrid joints). [±45/0/90]2S. The material properties of the USN125
A film type adhesive FM73 and a paste type adhesive carbon/epoxy unidirectional laminate are as follows: E1=
EA9394S were used for bonding. Specimens were made 131 GPa, E2 = 8.2 GPa, G12 = 4.5 GPa, m12 = 0.281, XT =
to be composite-to-aluminum double lap joints. SK Chem- 2000 MPa, XC = 1400 MPa, YT = 61 MPa, YC = 130 MPa
ical USN125 carbon/epoxy prepreg tapes were used for the and S = 70 MPa. Aluminum 7075-T62 with a thickness of
composite laminate. Aluminum alloy 7075-T62 was the 3.224 mm was used for the joints. The material properties
other adherend. of the aluminum 7075-T6 are as follows: E = 71.0 GPa,
m = 0.33, X = 551.6 MPa and S = 275.8 MPa.
2. Test The material properties of the film type adhesive FM73
are as follows: E = 2.9 GPa, m = 0.40 and 46.1 MPa. Shear
2.1. Specimen preparation strength S denotes the tensile shear strength for a metal-to-
metal bonded single lap joint. Specimens using the FM73
A total of 24 carbon-to-aluminum double lap joint spec- adhesive were cured in an autoclave. The material proper-
imens were tested using the three types of joining methods. ties of the paste type adhesive EA9394S are as follows:
For the joint with film type adhesive FM73, five specimens E = 4.2 GPa, m = 0.45 and S = 29 MPa. EA9394S was

Fig. 1. Configuration and dimensions of the hybrid joint.

Fig. 2. A typical hybrid joint specimen.


194 J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198

Fig. 3. Microscopic view of bonded specimen after water-jet cutting.

Fig. 4. Test set-up.

cured at room temperature. No other material, such as might behave differently than single lap joints. Further-
glass fabric, was added to the paste type adhesive layer. more, adherend materials can also affect the joints. Com-
All specimens were cut by water jet. A typical hybrid posite materials are unlike aluminum and steel.
specimen is shown in Fig. 2. Sections of the bonded speci- Therefore, it is common to determine the bonding strength
men fabricated by water jet are shown in Fig. 3. of the adhesive for a joint with a test for given conditions.
Conventionally, the bonding strength of an adhesive is
2.2. Test defined as the maximum carried load divided by the
bonded area. On the other hand, the bearing strength of
A material testing machine, Instron model 5582, was a bolted or riveted joint is defined as the maximum load
used for the joint test as shown in Fig. 4. The load was divided by the compressed area (the thickness of the joint
applied at 1.27 mm/min, as per ASTM specification times the diameter of the fastener hole). The method of
D3528-96. A digital microscope camcorder was installed defining the strength of the joint depends on the type of
to monitor and record the damage propagation in the joints. joint. Certainly, in this type of research, the method of
defining the joint strength should be consistent for compar-
3. Results and discussion ison purposes. Herein, therefore, for convenience and con-
sistency, the strength of the joint, regardless of the joining
3.1. Bonded joints method, is defined as the maximum load divided by the
cross sectional area of the composite laminates. The cross
3.1.1. Joints with film type adhesive FM73 sectional area of the aluminum, which is the other adher-
To investigate the reinforcing effect of bolting on the end, is not used because all failures occurred in the com-
strength of bonded joints, a test for bonded joints with film posite laminates in these tests. This definition of joint
type adhesive FM73 was conducted first. The baseline strength is different from the method to define the shear
material properties of the adhesive are generally provided strength of an adhesive or to define the bearing strength
by the manufacturer. These properties, however, can be of the mechanically fastened joints.
affected by test conditions such as the temperature, humid- Table 1 shows the test results for a bonded joint with the
ity and even the surface treatment. Also, double lap joints film type adhesive FM73. In the Table, Pmax denotes the
J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198 195

Table 1 500
Test results for bonded joints with film type adhesive FA-1
FA-1
FA-2

Applied stress (MPa)


Resultnspecimen FA-1 FA-2 FA-3 FA-4 Average 400 FA-2
FA-3
FA-3
Joint strength, 464 441 477 428 453
Pmax/2A (MPa) FA-4
FA-4
300
Adhesive strength, 32.7 31.1 33.7 30.2 31.9
Pmax/2AB (MPa)
200

maximum load carried by the joint. 2A and 2AB represent 100 P P


the cross sectional area and the bonded area of the lami-
nates of the double-lap joint, respectively. The average 0
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5
shear strength of the adhesive itself is 31.9 MPa. The Displacement (mm)
strength is the maximum load divided by the bonded area
2AB. It is 31% lower than the shear strength 46.1 MPa Fig. 5. Load–displacement curves for bonded joints with film type
adhesive.
based on an aluminum-to-aluminum single-lap joint [15].
It is, however, higher than the shear strength 23.6 MPa
for the composite-to-composite single lap bonded joint ried loads. However, the displacements corresponding to
[7]. In the reference, all the specimens failed in the delami- the loads differ greatly depending on the specimens. The
nation of the laminate while the adhesive sustained the joints also have various failure patterns, as shown in
bonding. The strength of the joint in this case was lower Fig. 6. The failure patterns can be categorized in terms of
than the shear strength of the adhesive itself. Present results the definition given in Fig. 7. The specimen FA-1 shows
for the joints with composite-to-aluminum double joints delamination, which is a kind of adherend failure, in the
are placed between the strengths of the aluminum-to-alu- composite laminate over about half the bonded area. The
minum and composite-to-composite joints. FA-1 specimen failed at a relatively short elongation.
The joint strength, which is the maximum load divided FA-2, -3 and -4 show a typical mixed mode failure. Adhe-
by the cross sectional area of the composite laminate, is sives are found in both the composite and aluminum sur-
453 MPa, on average. This will be compared with the other faces, which indicates a failure of the bonded surface.
two types of joints. The results show that the failure modes and maximum
Fig. 5 shows the load–displacement curves for the joints elongations are greatly influenced by the characteristics of
that were used to define the maximum carried load. In the the specimens, while the maximum carried loads are less
figure a large difference is not found in the maximum car- sensitive to the specimen conditions.

Fig. 6. Failure modes of bonded joints with film type adhesive: (a) FA-1, (b) FA-2, (c) FA-3 and (d) FA-4.
196 J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198

Adherend

Adhesive

Failure
Location

Adherend

(a) (b) (c) (d)

Fig. 7. Schematic diagram for the failure mode definition of an adhesive bonded joint: (a) cohesive failure, (b) adhesive failure, (c) mixed failure and
(d) adherend failure.

Table 2 joint strength with the film type adhesive FM73 and is
Test results of bonded joints with paste type adhesive 2.4 times the average joint strength with the paste type
Resultnspecimen PA-1 PA-2 PA-3 PA-4 PA-5 Average adhesive EA9394S. All specimens failed in bearing mode.
Joint strength, 69.1 59.8 81.7 59.6 65.5 67.1 In the table, d and t represent the hole diameter and lami-
Pmax/2A (MPa) nate thickness, respectively.
Adhesive strength, 4.87 4.22 5.76 4.21 4.62 4.74 The load–displacement curves are shown in Fig. 8. The
Pmax/2AB (MPa)
stiffness degradation by local failure is observed from the
curves. The curves show the typical pattern of the load–dis-
3.1.2. Joints with paste type adhesive placement curve for the bolted joint. Typical deformed
The test results for composite-to-aluminum bonded shapes that form around the fastener hole after the bearing
joints with paste type adhesive EA9394S are given in Table of the laminate are shown in Fig. 9.
2. The meanings of Pmax, 2A and 2AB are the same as in
Table 1. EA9394S is an adhesive that can be cured at room 200
temperature. The average shear strength of the adhesive
itself is found to be 4.74 MPa, but the manufacturer states BT- 1
BT- 2
Applied stress (MPa)

a shear strength value of 29 MPa; the present test result is 150 BT- 3
BT- 4
just 16% of the value given by the manufacturer. There are
many factors that may have contributed to the degraded 100
shear strength of the adhesive. One possible factor is the
fabric layer. This layer is usually added to an adhesive
before curing to enhance the bonding force and to control 50
the thickness of the bonding layer. In the present test, how- P P
ever, the fabric layer was not used because the purpose of
the present study is not to evaluate the shear strength of 0
0 1 2 3 4 5 6
the adhesive EA9394S, but to investigate the effect of the Displacement (mm)
relative difference of the strengths of the bonded and bolted
Fig. 8. Load–displacement curves for bolted joints.
joints on the hybrid joint. This means that two types of
adhesives – relatively strong and relatively weak – are
needed and there should be a distinct difference between
the shear strength of each.

3.2. Bolted joints

Table 3 shows the test results for simple bolted joints


without adhesive bonding. The average joint strength of
the simple bolted joints is 162 MPa, which is 36% of the

Table 3
Test results of bolted joints
Resultnspecimen BT-1 BT-2 BT-3 BT-4 Average
Joint strength, Pmax/2A (MPa) 167 172 156 154 162
Bearing strength, Pmax/2dt (MPa) 891 917 832 821 865
Fig. 9. Laminates after bearing failure.
J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198 197

3.3. Hybrid joints in the hybrid joint, then the bearing failure of the laminate
by bolting would start when the displacement u reached
Summaries of the test results and of the load–displace- about 1.0 mm and would result in final failure when u
ment curves of hybrid joints with the film type adhesive equaled about 2.0 mm. Fig. 8 shows, however, that the
are given in Table 4 and Fig. 10, respectively. The average bonded joint using FM73 sustains its structural integrity
joint strength, defined as the maximum carried load Pmax even when the displacement is about 2.0 mm. This means
divided by the cross sectional area 2A, is 440 MPa, which that the composite laminate fails first in bearing mode
is 3% lower than the strength of the simple bonded joint before the adhesive failure occurs. Once the bearing failure
(453 MPa). It is important to remember, however, that occurs, the joint load should be sustained by the adhesive
hybrid joints have a fastening hole with an area that is alone. It becomes the same as the simple bonded joint,
about 3% of the bonded area. Accordingly, the actual which has a bonded area that is 3% smaller than in the sim-
strength of the hybrid joint is the same as that of the simple ple joint, which explains why the hybrid joints have 3% less
bonded joint when the film adhesive FM73 was used. The strength than the simple bonded joint with FM73.
load–displacement curves shown in Fig. 10 also show pat- Typical failure modes are shown in Fig. 11. The figure
terns similar to those of the curves for the simple bonded shows that the composite laminates partially fail by delam-
joints (Fig. 5). ination and that the delaminated parts remain bonded to
Test results for the hybrid joints can be interpreted in the aluminum surface over about 30% of the original
terms of the load–displacement curves shown in Figs. 5, 8 bonded area after the final failure. More than half the
and 10. As shown in Fig. 8, local failures in the simple bonded area fails in mixed modes. In the mixed mode fail-
bolted joint are observed even before the displacement u ure, adhesives are observed in both the aluminum and com-
reaches 1.0 mm. If this situation is assumed to be the same posite sides. Bearing failures of laminates are easily
observed in Fig. 11(c) and (d). The white rings are due to
Table 4 the washers.
Test results of hybrid joints with film type adhesive
The results for the hybrid joints with a paste type adhe-
Resultnspecimen FH-1 FH-2 FH-3 FH-4 FH-5 FH-6 Average sive are given in Table 5. The average strength of the
Joint strength, 449 451 453 446 414 428 440 hybrid joints is 192 MPa, which is higher than the strength
Pmax/2A (MPa) of the simple bonded or bolted joints and is almost 84% of
the sum of each of the strengths (219 MPa). This is very
500 different from the results for the joints with film type adhe-
FH-1 sive. In the joints with film type adhesive, the bolting did
400 FH-2
not affect the strength of the bonded joints. On the con-
Applied stress (MPa)

FH-3
FH-4 trary, in hybrid joints with paste type adhesive that was
FH-5
300 FH-6 cured at room temperature with low bonded shear
strength, the bolt joint greatly increased the strength of
200 the hybrid joints. It should also be noted that the strength
of the hybrid joints is even greater than the strength of the
simple bolted joint, which means that the adhesive works
100
P P
Table 5
0 Test results of hybrid joints with paste type adhesive
0 0.5 1 1.5 2 2.5 3 3.5
Displacement (mm) Resultnspecimen FH-1 FH-2 FH-3 FH-4 FH-5 Average
Joint strength, 202 164 206 187 200 192
Fig. 10. Load–displacement curves for hybrid joints with film type
Pmax/2A (MPa)
adhesive.

Fig. 11. Typical failure modes of hybrid joints with film type adhesive: (a) Al (top), (b) Al (bottom), (c) Laminate (top) and (d) Laminate (bottom).
198 J.-H. Kweon et al. / Composite Structures 75 (2006) 192–198

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