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04-09-2018

Fiber Materials
• Materials that satisfy these requirementsare
glasses and plastic
Fiber Material • Majority of fibers are made ofglass consisting
of either silica orsilicate.
• Plastic fibers are less widely used becauseof
their higher attenuation
• Plastic fibers are used for short distance
applications (several hundred meters) and
abusiveenvironments
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Fiber Materials
• Requirements for optical fibermaterial
– It must be possible to make long thin,flexible
fibers from the material
– Material must be transparent at a particular
optical wave length in order for fiber to guide light
efficiently
– Physically compatible materials that haveslightly
different refractive indices for core and cladding
must be available

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GlassFiber
• Glass is made by fusing mixture of metal • Since the fiber cladding must have a lower index • silica (SiO2) n=1.458

oxides, sulfides, or selenides. The resulting than the core, examples of glass fiber compositions
material is a randomly connected molecular are
Germanium oxide
network rather a well defined structure as GeO2-SiO2 core; SiO2 cladding
found in crystallinematerials P2O5-SiO2core; SiO2 cladding
Phosphorus pentoxide
SiO2 core; B2O3-SiO2 cladding
• A consequence of this random order isglass
GeO2 – B2O3-SiO2 core; B2O3-SiO2 cladding
does not have a well defined melting point Fluorine Boron trioxide
• Sand is the principle raw material for silica
• When glass is heated , it gradually beginsto • Glass composed of pure silica is referred to as either silica
soften until it becomes a viscous liquid glass, fused glass, or vitreous silica. (transparent )

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GlassFiber Active Glass Fibers

• Optical fiber are made from oxide glasses and


most popular is silica (SiO2) which has •Incorporating rare-earth elements (atomic number 57-71) into a normally passive
glass gives the resulting material new optical and magnetic properties allow the
refractive index of 1.458 at 850nm. material to perform amplification, attenuation, and phase retardation on the light
passing through it .
• To produce two similar materials with slightly
different refraction indices for core and •Doping can be carried out using silica, tellurite and halide glasses.

cladding, either fluorine or other oxides •Two commonly used materials for fiber lasers are erbium and neodyium
(dopants) are added to silica

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Fiber materials
Glass fiber features:
Plastic Optical Fibers (POF)
– Advantages: low attenuation, cheap and abundant raw material • Growing demand for delivering high-speed services to workstations has
(mostly sand) led the developers to create high bandwidth graded index
– Disadvantages: high installation cost, complexity, requires skilled polymer(plastic) optical fibers (POF)
technicians, inflexible, easy-to-break • The core of this fibers are Poly(ethyl methacrylate) or a perfluorinated
polymer these fibers are referred as PMMA POF and PF POF
• Have greater optical signal attenuations than glass fiber, they tough and
durable
• Core diameter is 10-20 times larger

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Plastic Optical Fiber


• Advantages:
– Simpler and less expensive components
– Lighter weight
– greater flexibility and ease in handling and
– Lower installation cost
• Disadvantages:
– High attenuation
– Limited production

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04-09-2018

Fiber Fabrication
• Two basic techniques
– Vapor-phase oxidation process
• Outside vapor phase oxidation
• Vapor phase axial deposition
• Modified chemical vapor deposition
– Direct-melt methods

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Fiber Materials (Requirement)


• Requirements for optical fiber material
– It must be possible to make long thin, flexible fibers from the
material
FIBER FABRICATION
– Material must be transparent at a particular optical wave
length in order for fiber to guide light efficiently

– Physically compatible materials that have slightly different


refractive indices for core and cladding must be available

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Preform Generation Techniques


FIBER FABRICATION STEPS:
• The soot (layer of SiO2 particles is called soot) for the core material is
made by mixing three gases: SiCl4, GeCl4 and O2 through flame
 Thefiber fabrication process is a two-step process hydrolysis or chemical vapor deposition (CVD).
which involves:
SiCl4  2 H2O  SiO2  4 HCl
1. Making the preform GeCl4  2H2O GeO2  4 HCl
2. Drawing process SiCl4  O2  SiO2  2 Cl2
GeCl4 +O2  GeO2  2 Cl2
 ‘Preform’ is a rod of glass made by vapor deposition
process. It consists of both the core and cladding • The doping level is controlled by changing the amount of GeCl4 gas
added to the mixture.
materials. • Manufacturers deposit the soot on the surface of a glass substrate
(mandrel) or inside a hollow tube by one of the following methods:
 Thepreform is drawn into fibers using the fiber – Modified chemical vapor deposition (MCVD)
drawing process. – Plasma enhanced MCVD(PMCVD)

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Chemical vapor deposition (CVD)


Fabrication Steps • Chemicals are mixed in
vapour phase and react
inside a rotating glass tube
• Producing a pure glass. • Fine particles of solid
germano or phosphoro
• Converting it into the required glass silicate glass deposit on
composition for the core-cladding the inside of the tube.
structure, that is, the preform. • A travelling burner
• Preform is a rod of glass made by moving along the tube
deposition process. stimulates a chemical
reaction and also fuses the
• The preform has the same structure particles into glass on the
as the final optical fiber. inner wall of the tube.
• The fiber is drawn from preform at • Next the tube is heated to
the correct diameter (125 µm) 2000 C and collapses into
a “preform”
maintaining the same refractive
index profile. • The preform is then put
into a furnace and is
drawn into fibre.
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O utsi de Vapor -Phase O xi dati on (OVPO):  The fiber that is subsequently drawn from
( Exte r nal CVD) this preform rod will have a core that consists
of the vapor-deposited material and a
cladding that consists of the original silica
tube.

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M odi fie d C h e mic a l Vapor D e p ositio n


(MCVD) : (Inte r nal CVD) Plasma enhanced MCVD (PMCVD)
 The process shown in figure is widely adopted
to produce ve r y l ow-l oss gr ade d-i n de x • It is nearly identical to MCVD.
fibers. • The main difference is the stimulation of oxide
 The gl a ss va p or par ti cl e s, ar i si ng from the formation by isothermal plasma in a
re ac ti on of t h e c on s ti t ue nt me tal hal i de microwave cavity (3-5 MHz) at low pressure,
g a s e s a n d oxyge n, fl ow t h r oug h t h e i n si de which surrounds the silica tube.
of a re vol vi ng si l i c a tube . • Volatile reactants supplied to the tube react within
 As the SiO 2 particles are deposited, they are the microwave cavity. By controlling the
sintered to a clear glass layer by an microwave cavity, the reaction zone is moved
Oxyhydrogen torch which travels back and backward and forward.
forth along the tube.
 Whe n th e d e s i r e d t h i c k n e s s of gl a s s has
• With this technique, very thin-layer deposition is
b e e n d e p osi te d, t h e vapor flow is s h ut off possible. Hence in a single preform we can have
a n d t h e t ub e i s h e a t e d strongl y to c a us e up to 2,000 layers, and a good graded-index
to c ol l apse i nto a sol i d rod pre for m. profile can be obtained.
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FIBER CABLES

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Fiber Drawing and Coating


• The preform obtained by any
one method is placed
Fiber Cables
vertically on a drawing tower. There are two basic types of fiber-optic cable
• The lower end of the preform ◦ The difference is whether the fiber is free to move inside
is heated to melting, and the
fiber is drawn by stretching. a tube with a diameter much larger than the fiber or is
inside a relatively tight-fitting jacket
• The thickness of fiber is
controlled by the drawing They are referred to as loose-tube and tight-
rate. buffer cables.
• As the material leaves the
preform, a mechanical feeder Both methods of construction have advantages
ensures a continuous flow of ◦ Loose-tube cables—all the stress of cable pulling is taken
material. up by the cable’s strength members and the fiber is free
• Any lag or overpressure to expand and contract with temperature
would cause inconsistencies
in the flow and therefore in ◦ Tight-buffer cables are cheaper and generally easier to
the diameter of the fiber. use
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Tight Buffered Fiber Cable Module:


Fiber Optic Cable Construction

33 (a) Tight buffered fiber optic cable. (b) Loose-tube fiber optic cable. (c) Ribbon fiber optic cable 35

Specialty Optical Fibers


Loose Buffered Fiber Cable Module:

Three types of PMF’s: (a) Panda style, (b) Photonic crystal fibers: (a) Solid core
Elliptical -clad and (c) Bow-tie structure and (b) hollow core
structure

Different PCF structures: (a) Honeycomb, (b) Bragg hollow core, (c) Hexagonal
34 lattice solid- core, (d) Large hollow core hexagonal 36
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• Silicon tetrachloride or tetrachlorosilane=SiCl4 =Silicon tetrachloride


or tetrachlorosilane is the inorganic compound with the formula SiCl4.
It is a colourless volatile liquid that fumes in air. It is used to produce
high purity silicon and silica for commercial applications.
• Germanium tetrachloride= GeCl4 = Germanium tetrachloride is a
colourless, fuming liquid with a peculiar, acidic odour. It is used as an
intermediate in the production of purified germanium metal. In
recent years, GeCl4 usage has increased substantially due to its use as
a reagent for fiber optic production.
• GERMANIUM DIOXIDE-GeO2

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