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OPERATING INSTRUCTIONS
Version 2.0
Person responsible: KRE
November 2010 (revised April 2011)
ItN Nanovation AG
Untertürkheimer Str. 25
D-66117 Saarbrücken
www.itn-nanovation.com
info@itn-nanovation.de
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Table of content
1 General Information................................................................................................. - 1 -
2 Safety Instructions .................................................................................................. - 4 -
2.1 Personnel Qualifications ................................................................................................. - 5 -
2.2 Personal Protective Equipment and Measures............................................................. - 5 -
3 Transport and Storage ............................................................................................ - 7 -
4 General Technical Information ............................................................................... - 8 -
4.1 The ceramic makes the difference! ................................................................................ - 8 -
4.2 Technical description .................................................................................................... - 11 -
4.3 Characteristic Values for Filterable Substances ........................................................ - 16 -
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4.4 P & I Diagram of CFM Systems ................................................................................... - 18 -
5 Installing the Membrane Filtration System .......................................................... - 20 -
5.1 General flow diagram..................................................................................................... - 21 -
5.2 Float Switches ................................................................................................................ - 22 -
5.3 Hose Connections.......................................................................................................... - 24 -
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5.4 Installing CFM Systems ............................................................................................... - 24 -
5.5 Installing the filtration pump......................................................................................... - 26 -
6 Operational Modes ................................................................................................ - 31 -
6.1 Filtration mode ............................................................................................................... - 31 -
6.2 Backflush mode ............................................................................................................. - 34 -
6.3 Automatic Detergent Assisted Backflushing (ADAB) ................................................ - 37 -
6.4 ADAB cleaning on air .................................................................................................... - 40 -
6.4.1 General information ................................................................................................. - 40 -
6.4.2 Cleaning procedure ................................................................................................. - 42 -
6.4.3 Discharging step-by-step......................................................................................... - 42 -
6.4.4 Restart ..................................................................................................................... - 43 -
7 Chemical Cleaning................................................................................................. - 45 -
7.1 Calculation of dosing volume ....................................................................................... - 45 -
7.2 Cleaning with citric acid ................................................................................................ - 47 -
7.3 “Emergency cleaning” with sodium hypochlorite...................................................... - 48 -
8 Servicing and Maintenance................................................................................... - 51 -
8.1 Maintenance of ceramic flat membranes (CFM) ......................................................... - 52 -
8.2 The Log Book ................................................................................................................. - 53 -
9 Contact ................................................................................................................... - 57 -
10 Hazard warning notices and safety instructions ................................................. - 58 -
11 Lifting of the Filtration Unit................................................................................... - 69 -
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1 General Information
It is absolutely necessary that the assembly personnel and the responsible operating
personnel/users read these operating instructions before handling, installation, start-up,
operation or maintenance of the filtration system. Make these instructions always
available at the place of use. These operating instructions contain fundamental rules and a
strict compliance will help to avoid risks and ensure reliability as well as durability of the
filtration system.
It is necessary to observe not only the instructions provided in the following, but also the local
regulations, e.g. given by the industrial workmen’s compensation insurers (accident
prevention regulations). In case that ItN supplies any electrical system (e.g. PLC for test or
container plants), please refer to the German Standard DIN VDE 0100 (German Association
for Electrical, Electronic & Information Technologies) and the local standards and applicable
regulations.
Tasks during handling, installation, start-up, operation and maintenance must be carried out
in accordance with the regulations given by these operation instructions. Necessary tasks
that are not listed are to be carried out in accordance with the customary rules of technology
and safety instructions.
Exclusion of Liability:
Please understand that ItN Nanovation AG rejects any liability for consequences arising from
failure to observe the information and rules of these operating instructions.
2 Safety Instructions
The safety instructions given by these operating instructions, the local accident prevention
regulations and all of the user’s internal work flow descriptions, plant regulations and safety
regulations, must be observed. Failure to observe the safety instructions can result in danger
for persons, the environment as well as for the filtration system. All existing safety and
protection equipment must be reviewed periodically. As a rule, cleaning and maintenance
work may be performed only when the filtration system is at a standstill. Unauthorized
modifications of the filtration system are prohibited and require manufacturer approval.
The membrane filtration system must be transported only using suitable means of transport
and secured against shifting and falling off during transport using suitable transportation
safety devices. If temporary storage of the membrane filtration system is necessary, it must
take place on a suitable, level surface. While in storage, possible damages to the membrane
filtration system through environmental influences or extraneous cause must be avoided.
For the product group CFM Systems®, ItN Nanovation AG in Germany developed ceramic
coating slurries based on nanoparticles. Depending on the filtration application and customer
requirements, ItN can produce defined nano-coatings with specific separation characteristics.
Filtration
Module Filtration
Rack
Technical Data CFM Systems® T-Series Filtration Unit and Filtration Rack
CFM Systems® Filtration Unit consisting of: CFM Systems® Filtration Rack consisting of:
1 up to 16 modules, each Defined number of filtration units
one with 4.0 m² filter area
Aeration connection
Ceramic flat membranes,
Permeate
pore size 200 nm
drain
Clamping system
Aerator unit
Top frame
Temperature of media: 5 - 45 °C
Ambient temperature: 5 - 45 °C
pH-value: 3 - 10 stable range of operation
Filtration pressure (abs.): max. -650 mbar for 12 consecutive hours
Back flush pressure: max. 1,5 bar for 1 hour per month
Note: ItN Nanovation AG has to verify the actual field of application and process
parameters. Depending on changing parameters, the functionality of the water
treatment system and the filtration performance (flow in l/m²h) may vary.
The feed flow into the membrane chamber should be constant, realized e.g. by a feed pump
discharging a constant volume into the membrane chamber or a gravity overflow.
Accumulated concentrated solids have to be discharged from the membrane chamber
periodically and can be recirculated completely or partially in an upstream collection
container or septic tank. In order to reduce a high concentration of solids in the membrane
chamber, the ratio between feed flow (inflow) and filtration flow (permeate) should be 5:1.
For safety reasons, the membrane chamber should feature an emergency overflow!
Alternatively the filtration section could also feature a submerged pressure sensor which can
define different operation statuses.
Please note that once a T-Series filtration unit has been disassembled, new O-sealing
rings must be utilized before re-assembling (please refer to ItN’s T-HP Assembly
Manual).
It must be ensured that no tools or other objects that could damage the filtration membranes
are placed on top of the filtration unit/rack. The filtration unit/rack is placed on the bottom of
the membrane chamber. The bottom of the membrane chamber must be level so that the
filtration unit is standing plumb-vertical. The filtration unit/rack must be submerged meaning
that the ceramic membranes are completely covered with the respective medium. The fill
level in the membrane chamber has to be least 10 - 15 cm over the top of the filtration
unit/rack.
Figure 5 illustrates a better level difference. In this case the filtration pump must apply a
pressure of 0,05 bar in order to overcome the level of 0,5 m. The total suction pressure is
only slightly influenced.
H = 0,5 m
In case that the filtration pump is installed below the water surface level of the membrane
chamber (see Figure 6), the level difference contributes to the filtration pressure in a positive
manner. Because of the gravity flow, the same filtration performance with at lower pump
performance (pump frequency) can be reached.
H = 1,5 m
6 Operational Modes
The following chapter will introduce the main operational modes of CFM Systems® on basis
of principle piping and instrumentation diagrams. Actual piping and instrumentations may
vary from the following illustrations.
A displacement pump, e.g. a gear pump (P-01), intakes the treated water (permeate) through
the membranes whereas solids, microorganisms and bacteria are retained. Between the
filtration volume and the frequency of the pump an almost linear correlation exists, that
means that the filtration volume has to be adjusted via the pump frequency. A certain volume
of permeate is collected in a storage tank (B-01) and is used for backflushing and ADAB
cycles. Excess permeate will overflow in order to percolate or to be saved for any permeate
reuse application, e.g. for landscaping or irrigation.
In order to control the formation of cake-layers and deposits on the membranes, a periodic
backflushing by reversing the flow direction of the filtration pump has to be initiated. With a
certain pressure and filtration pump frequency, permeate in the permeate storage tank is
discharged back through the membranes. A short break between stopping filtration and
starting backflush cycle assists a gentle reversal of the flow direction of the gear pump.
During filtration breaks and system shutdowns, the magnet valve (V-01) is closed in order to
prevent the permeate storage tank (B-01) from draining. The membrane aeration is
generated by a compressor (P-04) which operates permanently.
If an ADAB cleaning cycle is started, the filtration process is stopped immediately. The
dosing pump (P-02 or P-03) discharges a defined amount of chemical concentrate, e.g.
sodium hypochlorite or citric acid, into the permeate storage tank (B-01) as shown in figure 9.
This blend of permeate and a concentrated chemical is used as a cleaning solution with a
defined concentration and is backflushed through the membranes (see figure 10).
Each ADAB cleaning process is defined by a certain number of ADAB cycles, and each
ADAB cycle is defined by a certain backflushing and residence time during which the
cleaning solution reacts with the membrane. As soon as the residence time is over, one
ADAB cycle is completed. After the completion of all ADAB cycles, the ADAB cleaning
process is finished and the filtration can be restarted manually or by a control system
automatically.
The ADAB cleaning process can be repeated using a different cleaning solution if necessary.
Please make sure that no chemicals are mixed in the permeate tank and check the fill
level in the permeate tank before dosing another chemical! Using different tanks for
different cleaning solutions is recommended! Please consult ItN for further information.
After discharging of the filtration chamber is finished, the aeration (membrane blower) as well
as the recirculation/discharging pump has to be stopped.
6.4.4 Restart
After completing the ADAB on-air cleaning process, the membrane chamber must be re-filled
before filtration process is restarted. The CFM Systems® filtration process is an
underpressure process. Suction pumps have to be stopped anytime when fil level
comes under minimum (Please see chapter 5.2)! Because of oxidation processes certain
reaction gases may be formed during ADAB cleaning processes. These gases have to be
vented through a venting valve (V-02) before restart.
Theoretically, the mechanical stability of CFM Systems® allows a cleaning with a high
pressure cleaner. Please ask ItN for permission before starting such a procedure.
7 Chemical Cleaning
Without the written permission of ItN, no other chemicals than sodium hypochlorite and citric
acid are allowed for bringing into contact with CFM Systems®. Disregarding this limitation
result in a cancelation of ItN’s Warranty Terms. The chemical cleaning has to be carried
out with potable water only. If permeate is intended for the use as a basis for the cleaning
solution, ItN has to be informed in order to approve this application. Please consult ItN in
case that alternative chemicals shall be used or for special cleaning requirements.
Vpermeate ⋅ c cleaning ⋅ 10 −6
Vdosing =
c concentrate
The following exemplary calculation regarding the needed dosing volume for 1L of a 600ppm
cleaning solution shall help to clarify the mentioned terms.
In order to ensure a safe operation of the membrane filtration system and to prevent
damages to the environment, people or system components, regular maintenance and
service activities have to be conducted. The user has to carry out all maintenance work that
essentially consists of status and function checks as well as checking of the most important
operating parameters. Additionally, all status, function and operating parameter checks must
be documented in a log book (please refer to chapter 8.2). Deviations from target values and
malfunctions must be noted in a log book and eliminated immediately with the help of
responsible maintenance personnel. Malfunctions that could adversely affect safety must be
reported to the responsible expert personnel immediately. All described intervals and duties
only relate to parts and components delivered by ItN Nanovation AG, but e.g. unusual noises
of pumps, compressors and any other component should be recorded as well. The
operating instructions described in this document must be observed for all arising
tasks!
9 Contact
ItN Nanovation AG
Untertürkheimer Straße 25
66117 Saarbrücken
GERMANY
www.itn-nanovation.com
cfm@itn-nanovation.com
WARNING OF HEAVY
COMPONENTS!
Some components may be heavy.
Always ensure that adequate
workforce is available. We
recommend for the handling of the
Filtration Modules at least 2 persons!
RISK OF BREAKAGE!
Some components are fragile (in
particular the ceramic membranes).
Always handle all components with
care. We recommend wearing gloves
in case of any damage! Please follow
the safety instructions in this
document.
Please make sure that the filtration units are only been lifted with an adequate lifting
device to ensure a vertical force on the threaded rod! Please ask ItN for a lifting
crossbar as shown below.