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Stable
Emulsifier free concept Foaming stability
viscosity
pH range (2-8)
Elegant sensorial profile
Compatibility with solvents
Suspending properties
Zen attitude in SKIN care, formulas with active ingredients : tailor made viscosity
9 Fluid formulas: cream gels, emulsions, chassis
9 Thick formulas: cream gels, emulsions, chassis
C/4582/GB/05/July 2013 3
Extreme electrolyte resistance
Aqueous gel
140000
120000
100000 AMAZING
(mPa.s)
80000
CHASSIS
60000
40000 BEHAVIOR
20000
0
0 2 4 6 8 10
NaCl %
Brookfield Viscosity M1
Actives % pH
LV M3 V6
Aqueous gel 0% 5.8 50 000 mPa.s
Glycolic Acid 4% 3.3 45 000 mPa.s
Magnesium chloride 0.1% 5 40 000 mPa.s
SEPICONTROL™ A5* 4% 4.7 52 000 mPa.s
Zinc gluconate 1% 5.5 48 000 mPa.s
Zn gluconate / Mg gluconate 1%/1% 5.7 47 000 mPa.s
EDTA 0.2% 8.5 41 000 mPa.s
Compatibility of SepiMAX™ ZEN 2% with active ingredients in aqueous gel
Viscosity remains constant after addition of the active ingredients and the
aqueous gel is stable over time
* SEPICONTROL™ A5 – CAPRYLOYL GLYCINE & SARCOSINE & CINNAMOMUM ZEYLANICUM BARK EXTRACT
C/4582/GB/05/July 2013 5
Extreme electrolyte resistance
Mineral aqueous gel
C/4582/GB/05/July 2013 6
Sensory profile
Aqueous gel
60000
2% SepiMAX ZEN
40000
3% SepiMAX ZEN
20000
0
0 2 4 6 8 10
pH
SEPIMAX™ ZEN
2%
Ethanol ≅ 95%
C/4582/GB/05/July 2013 9
Suspending properties
Aqueous gel
Example of particles
A SepiMAX™ZEN Polyacrylate Crosspolymer-6 0.15 A SepiMAX™ZEN Polyacrylate Crosspolymer-6 0.5
Cold process
No neutralization
pH 2-8 Low viscosity challenge
With electrolytes
High viscosity challenge
C/4582/GB/05/July 2013 12
ZEN attitude in Skin care
Low viscosity – Cream gel
Powder A 2% _ _ _
In presence of electrolytes,
formulate your pourable cream gels
with SepiMAX™ ZEN.
Powder A : Ammonium acryloyldimethyl taurate/VP copolymer
C/4582/GB/05/July 2013 13
Low viscosity /Serum rich in actives
A Aqua/Water Up to 100%
Glycerin 3.00%
Monopropylene Glycol 1.00%
Amber translucent serum
Pump jar
PHYTOAGE™ 0.25%
SEPIVITAL™ EPC 0.20%
Serum dedicated to skin of 60+ with Bis PEG-18 Methyl Ether Dimethyl Silane 2.00%
freshness during application,
EDTA Tetrasodique 0.10%
Quick penetration, soft finish and
comfortable sensation over time
B AQUAXYL™ 3.00%
Cocktail of active ingredients which answer
to specific needs of 60+ : SEPITONIC™ M4 1.00%
9 SEPITONIC™ M4 restructures the skin C SIMULSOL™ 1292 DF 0.50%
and provides a real « breath » of oxygen
to the cells ; skin is more dense and Parfum/Fragrance 0.04%
more resistant Tocopherol 0.10%
9 Double anti-ageing performance of
PHYTOAGE™ which fights photo-induced Phenoxyethanol & Ethylhexyl Glycerin 1.00%
ageing and hormonal ageing by means
of its “hormone-like” structure. D SEPIMAX™ ZEN 1.00%
9 Powerful antioxidant, SEPIVITAL™ EPC
helps combat the phenomena of aging .
9 AQUAXYL™ moisturizes the skin
Performance of SEPIMAX™ ZEN: at only 1%,
it stabilizes this extra-rich in electrolytes
cocktail of active ingredients by keeping a
translucent aspect Appearance Amber translucent gel
pH 6.6
Viscosity 1M at RT 5.600 mPa.s Brookfield S3S6
Viscosity 1M at 45°C 4.620 mPa.s Brookfield S3S6
Viscosity recovery at RT 5.680 mPa.s Brookfield S3S6
(after 1M at 45°C)
Stability* 1M at RT, 45°C, cycles -5/+40°C
Fluid Geltrap (Gel in Oil) /Emulsion with Aluminium
chloride
ANTIPERSPIRANT CARE
FLUID Geltrap Emulsion
Geltrap Formulation A
LANOLTM 99 6.00 %
EASYNOVTM 2.50 %
EASYNOV allows to realize new
formulation forms extra-rich in
Phenoxyethanol & Ethylhexylglycerin 1.00 %
water by a cold process with gentle Parfum/Fragrance 0.10 %
stirring : the GELTRAP emulsions
B
Easy offer to support
SEPIMAX™ ZEN 0.50 %
formulations with stressfull
active ingredients in AQUAXYLTM 3.00 %
association with SEPIMAX™ ZEN
Aqua/Water up to 100%
Aluminium chlorohydrate 50% 30.00 %
Geltrap Formulation A
LANOLTM 99 5.30 %
EASYNOVTM 2.00 %
EASYNOV allows to realize new
formulation forms extra-rich in
Phenoxyethanol & Ethylhexylglycerin 1.00 %
water by a cold process with gentle Parfum/Fragrance 0.10 %
stirring : the GELTRAP emulsions
B
GELTRAP emulsions offer SEPIMAX™ ZEN 0.70 %
surprising textures : a sensation of
comfort and suppleness. Glycerin 14.00 %
Aqua/Water up to 100%
The GELTRAP concept allows to
formulate extra high level of
glycerin without any tacky effect
A MONTANOV™ L 1.00%
SIMULSOL™ 165 1.00%
Caprylic Capric Triglyceride 4.00%
Fluid white emulsion
Packaging : Pump bottle
Neopentyl Glycol Diethylhexanoate 4.00%
Isostearyl Isostearate 1.50%
Designed in FRANCE.
Dimethicone 1.00%
The wait is over… Add actives with ease—
robust stability guaranteed. Mission
impossible with the duo SEPIMAX™ ZEN + B Aqua / Water Qsp 100%
MONTANOV™ L becomes possible. Glycerin 5.00%
SEPIMAX™ ZEN challenges to stabilize Disodium EDTA 0.10%
chassis whatever viscosity
Sodium Hydroxide 12% Qs pH=5.5–6
Light and quick absorbing emulsion thanks
to MONTANOV™ L.
SOLAGUM™ AX−SEPIMAX™ ZEN association C SEPIMAX™ ZEN 1.00%
helps to stabilize fluid formulas rich in
ectrolyte. SOLAGUM™ AX 0.50%
A modern, fluid and smooth texture.
Easy to use.
D Phenoxyethanol & Ethylhexylglycerin 1.00%
Parfum / Fragrance 0.03%
160000
Brookfield Viscosity
120000
(mPa.s)
100000
60000
20000
0
0 2 4
% NaCl
In presence of electrolytes,
formulate cream gels
with high viscosity stable over time
C/4582/GB/05/July 2013 18
ZEN attitude in Skin care
High viscosity – Cream gel
Challenge
« High viscosity » Mineral oil Isononyl Caprylic capric
BROOKFIELD LV M4 V6
isononanoate trygliceride
100 000 mPa.s
with 2% NaCl
pH< 5.5
C/4582/GB/05/July 2013 19
ZEN attitude in Skin care
High viscosity – Emulsion
MONTANOV™ L 3% 3% 3%
Caprylic/Capric
20% 20% 20%
triglyceride
SepiMAX™ ZEN 1% 1% 1%
Zinc Gluconate - 1% -
Sodium PCA - - 3%
BROOKFIELD Viscosity
(mPa.s)LV M3 V6
84 500 92 500 69 000
A MONTANOV™ L 1.00%
SIMULSOL™ 165 2.00%
Thick white cream LANOL™ P 2.00%
Presentation: in jar Isostearyl Isostearate 3.00%
Designed in FRANCE.
Caprylic Capric Triglyceride 5.00%
The wait is over… Add actives with Neopentyl Glycol Diethylhexanoate 5.00%
ease—robust stability guaranteed. Dimethicone 1.00%
Mission impossible becomes
possible with SEPIMAX™ ZEN. B Aqua / Water Up to 100%
A modern, creamy and smooth Glycerin 5.00%
texture.
Light and quick absorbing emulsion Disodium EDTA 0.10%
thanks to MONTANOV™ L. Sodium Hydroxide 12% 0.07%
SOLAGUM™ AX−SEPIMAX™ ZEN
association boosts electrolyte C SEPIMAX™ ZEN 1.50%
resistance and smoothes texture. SOLAGUM™ AX 0.50%
*
80/20% ratio when mixed with cocktails
EU07209, EU07211B, EU07212, EU07213,
D Phenoxyethanol & Ethylhexylglycerin 1.00%
EU07228, EU07229, EU07230, EU07231, Parfum / Fragrance 0.03%
EU07232, EU07233, EU07234, EU07235
Ideal to
formulate at
natural skin pH
« Foaming emulsions » with a soft & creamy skin feel, and a stable
foam.
23
C/4582/GB/05/July 2013
ZEN attitude in Hygiene care
Thickening capacity
8,000
7300
7,000
6,000
5,000
NaCl
4,000
Sepimax ZEN
3,000
2,000
910
1,000
340
0 50 50 50
0 0.5 1 1.5 2
Dose (%)
24
C/4582/GB/05/July 2013
ZEN attitude in Hygiene care
Foaming formula
1) Thickens t0
2) Stabilizes
Foam aspect / t10’
stability
3) Texturizes (SEPPIC method
57CO058
the foam x100)
t20’
A Aqua/Water Up to 100%
Color 0.08%
Translucent slight pink fluid cream gel
Pump jar B SEPIMAX™ ZEN 2.50%
Texture dedicated to "water addict" C PEG-7 Glyceryl Cocoate 5.00%
sensitive skin!
This non-foaming formula is a mild Helianthus Annuus (Sunflower) Seed Oil 1.00%
remover; after rinse-off, skin is fresh
and ultra-soft! PROTEOL™ APL 3.00%
SEPIMAX™ ZEN stabilizes 3% of anionic
surfactant (with a high level of salts) D Phenoxyethanol & Ethylhexylglycerin 1.00%
and oily phase which avoids drying out
the skin Parfum/Fragrance 0.10%
PROTEOL™ APL provides a mild
cleansing of the face AQUAXYL™ 3.00%
AQUAXYL™ moisturizes the skin
Cold Process
SepiMAX™ ZEN
More elastic polymeric network G’ >>> G’’, Common profile between
temperature stable SEPIGEL™/SIMULGEL™ and
SEPIPLUS™/SEPINOV™
⇒ Strong stabilizing properties Elastic network, resistant to
⇒ Pick-up available with “recovery effect” in high shear stress
concentration
⇒ Slight viscosity maturation after manufacturing
Shear-thinning profile
More Newtonian flow
# ⇒ No viscosity maturation after
manufacturing
⇒ Feel consistent in application
C/4582/GB/05/July 2013 29
Activate synergies
Skin & Hygiene care
- Synthetic polymers
- Natural gums
- NaCl
Stability
Texture
Cost/Performance
C/4582/GB/05/July 2013 30
SKIN CARE
Eggs 2 ways
EU07257B
Refreshing egg whites
A MONTANOV™ 82 1.00%
MONTANOV™ 202 1.00%
SEPIMAX™ ZEN 0.60%
Hydrogenated polydecene 5.00%
2-Ethylhexyl palmitate 8.00%
Light yellow cream with salt particles
Packing:Jar B D.I. Water To 100%
Glycerine 4.00%
A special emulsion with salt crystals that SOLAGUM™ AX 0.40%
provide an unexpected and luxurious texture C NaCL 30.00%
Only 1% Montanov 202 + 1% Montanov
82+0.6% Sepimax ZEN stabilize this formula D Fragrance 0.10%
which contains 30% salt! 5-chloro-2-methyl-2H-isothiazol-3-one/2-
methyl-2H-isothiazol-3-one/benzylalcohol 0.10%
This emulsifier and polymer combination 0.1% Colorant 0.30%
create the unique skin feeling.
The emulsion works to smooth and clean
skin while achieving ZEN.
Procedure
LAB-SILVERSON ROTOR STATOR-300g
Mix part B and stir until uniform. Heat phase A and B to 85℃
separately. Add phase B to phase A, homogenize for 4
minutes at 4000rpm. Stir the emulsion with an anchor at
100rpm for 10 min and cool down with a water bath at
100rpm. Add part C and D at 45℃. Stop stirring at 30℃.
Characteristics
• Appearance Light yellow cream with salt particles
• pH Around5.3
• Viscosity 1M at RT 59,900 mPa.s BROOKFIELD LV4 6rpm
Viscosity 1M at 45°C 10,200 mPa.s BROOKFIELD LV4 6rpm
Viscosity recovery at RT 36800 mPa.s BROOKFIELD LV4 6rpm
(after 1M at 45°C)
All information contained herein is intended merely to demonstrate the utility of SEPPIC products, and should not be construed as granting license to practice any compositions or
methods covered by a patent or a patent application. All information contained in this specific technical documentation is believed to be accurate and has been set up by SEPPIC
according to its own described methods and processes.SEPPIC however does not assume any liability or risks involved in the use of its products for the preparation and the
assessment of the hereinabove formulation since the condition of use are beyond its control. SEPPIC customer must insure that the duplication of the hereinabove formulation is www.seppic.com
not infringing any intellectual property rights and that it complies with any regulatory status.
Regulatory status
For cosmetic applications
CAS Number : 1190091-71-4
Specific regulation Compliance
Country or Region Identifier
or Status (Yes/No)
Directive 76/768/EEC
Yes
POLYACRYLATE
EUROPE and Reg 1223/2009 CROSSPOLYMER-6
C/4582/GB/05/July 2013 38
SepiMAX™ ZEN’S MECHANISM
Electrostatic Polymer
water
repulsions chain Hydrophobic group
Hydrophobic Cross-linker
Microgel interactions
C/4582/GB/05/July 2013 39
SepiMAX™ ZEN’S MECHANISM
1 2
Brookfield Viscosity (mPa.s)
50000
45000
40000
35000
30000
25000
20000
15000
10000
5000
0
0 2 4 6 8 10
% NaCl
C/4582/GB/05/July 2013 40
SepiMAX™ ZEN’S MECHANISM
Pure water 1 2
C/4582/GB/05/July 2013 41
Contacts
Nota
The analytical specifications warranted are only those mentioned on the certificate of analysis supplied with each delivery of the product.
Except as set forth above, SEPPIC* makes no warranties, whether express, implied or statutory, as to the product which is the subject of this document. Without limiting
the generality of the foregoing, SEPPIC* makes no warranty of merchantability of the product or of the fitness of the product for any particular purpose. Buyer assumes all
risk and liability resulting from the use or sale of the product, whether singly or in combination with other goods. The information set forth herein is furnished free of
charge and is based on technical data that SEPPIC* believes to be reliable. It is intended for use by persons having technical skill and at their own discretion and risk.
Since conditions of use are outside SEPPIC*'s control, SEPPIC* makes no warranties, express or implied, and assumes no liability in connection with any use of this
information. Nothing herein is to be taken as a license to operate under or a recommendation to infringe any patents.
* SEPPIC being :
SEPPIC S.A. Head Office SEPPIC Japan Office SEPPIC Italia Srl
22 Terrasse Bellini 75, quai d'Orsay Air Liquide Japan's office Via Quarenghi 27
92806 Puteaux 75007 Paris Granpark Tower 3-4-1 Shibaura 20151 Milano
FRANCE FRANCE Minato-ku, Tokyo 108-8509 ITALY
Tel. : +33 (0)1 42 91 40 00 JAPAN Tel : +39 02 38009110
info.seppic@airliquide.com Tel : +81 3 6414 6725 italy.seppic@airliquide.com
japan.seppic@airliquide.com
SEPPIC Inc. SEPPIC Poland Office SEPPIC Brasil SEPPIC Colombia SAS
30, Two Bridges Road, suite 210 CCIF Rua Libero Badaro, 182 Calle 71 n°10-40
Fairfield, Ul. Widok 8 8° andar - Centro Edificio Orbe 71 of 401
New Jersey 07004-1530 00-023 Varsovie 01008-000 Sao Paolo SP Bogota
USA POLAND BRAZIL COLOMBIA
Tel. : +1 973 882 5597 Tel : +48 22 690 68 73 Tel : +55 11 3242 3911 Tel : +571 702 44 48
us.seppic@airliquide.com poland.seppic@airliquide.com brasil.seppic@airliquide.com colombia.seppic@airliquide.com
C/4582/GB/05/July 2013 42