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what is measurable
and make measurable
that which is not.
Galileo Galilei (1564-1642)
Viscometer
(Original Instruction)
Further information
Published and printed by Anton Paar GmbH, Austria
Copyright © 2019 Anton Paar GmbH, Graz, Austria
Address of the instrument producer: Anton Paar GmbH
Anton-Paar-Str. 20
A-8054 Graz / Austria – Europe
Tel: +43 (0) 316 257-0
Fax: +43 (0) 316 257-257
E-Mail: info@anton-paar.com
Web: www.anton-paar.com
Date: October2019
Document number: D89IB001EN-O
Viscometer
(Original Instruction)
Contents
1 Safety Instructions.................................................................................................................................. 5
1.1 General Safety Instructions............................................................................................................... 5
1.2 Special Safety Instructions................................................................................................................ 6
1.3 Conventions for Safety Messages .................................................................................................... 6
1.4 Safety Signs on the Instrument......................................................................................................... 6
2 SVM X001 - An Overview........................................................................................................................ 8
2.1 Intended Use of the Instrument......................................................................................................... 8
2.2 Functional Components .................................................................................................................... 9
2.3 Operating Elements on Main Screen .............................................................................................. 10
3 Installing the Instrument ...................................................................................................................... 12
3.1 Installation Requirements ............................................................................................................... 12
3.2 Installing the Instrument.................................................................................................................. 12
3.3 Switching On/Off ............................................................................................................................. 14
3.4 Steps After Initial Installation........................................................................................................... 14
4 Calibration, Calibration Correction and Adjustments ....................................................................... 15
4.1 Performing Calibration .................................................................................................................... 15
5 Performing a Measurement.................................................................................................................. 16
5.1 Standard Filling of SVM .................................................................................................................. 17
5.2 Measuring ....................................................................................................................................... 18
6 Cleaning................................................................................................................................................. 21
6.1 Cleaning Liquids ............................................................................................................................. 21
6.2 Standard Cleaning and Check ........................................................................................................ 22
6.3 Cleaning Housing and Touch Screen ............................................................................................. 25
7 Upkeep and Additional Cleaning......................................................................................................... 26
7.1 Leak Test ........................................................................................................................................ 27
7.2 Rinsing the Thermostat Tube.......................................................................................................... 29
7.3 Cleaning the Measuring Rotor ........................................................................................................ 29
7.4 Replacing O-Rings.......................................................................................................................... 33
8 Maintenance and Repair....................................................................................................................... 34
8.1 Maintenance Performed by an Authorized Anton Paar Service Engineer ...................................... 34
8.2 Repair Performed by an Authorized Anton Paar Representative ................................................... 34
Appendix A: Technical Data ................................................................................................................... 35
Appendix A.1: Measuring Performance ................................................................................................ 35
Appendix A.2: General Technical Data................................................................................................. 37
Appendix B: Wetted Parts....................................................................................................................... 39
Appendix B.1: Wetted Parts.................................................................................................................. 39
Appendix B.2: Potentially Wetted Parts ................................................................................................ 40
4 D89IB001EN-O
1 Safety Instructions
1 Safety Instructions
• Read the documentation before using SVM. • In case of damage or malfunction, do not con-
tinue operating SVM. Do not operate the instru-
• Follow all hints and instructions contained in the
ment under conditions which could result in
documentation to ensure the correct use and
damage to goods and/or injuries and loss of life.
safe functioning of SVM.
• Check SVM for chemical resistance to the sam-
• The documentation is a part of the product.
ples and cleaning agents.
Keep this document for the complete working
life of the product and make sure it is easily
Maintenance and service
accessible to all people involved with the prod-
uct. If you receive any additions or revisions to • The results delivered by SVM not only depend
the documentation from Anton Paar GmbH, on the correct functioning of the instrument, but
these must be treated as part of the documenta- also on various other factors. We therefore rec-
tion. ommend you have the results checked (e.g.
plausibility tested) by skilled personnel before
consequential actions are taken based on the
1.1 General Safety Instructions results.
• Service and repair procedures may only be car-
Liability ried out by authorized personnel or by Anton
• This document does not claim to address all Paar GmbH.
safety issues associated with the use of the
instrument and samples. It is your responsibility Disposal
to establish health and safety practices and • Concerning the disposal of SVM, observe the
determine the applicability of regulatory limita- legal requirements in your country.
tions.
• Anton Paar GmbH only warrants the proper Returns
functioning of SVM if no adjustments have been • For repairs send the cleaned SVM (instrument)
made to the mechanics, electronics, and firm- to your Anton Paar representative. Only return
ware. the instrument together with the filled out RMA
• Only use SVM for the purpose described in the (Return Material Authorization) and the form
documentation. Anton Paar GmbH is not liable "Safety Declaration for Instrument Repairs".
for damages caused by incorrect use of SVM. Download the Safety Declaration form from our
website www.anton-paar.com.
Installation and use • Do not return instruments which are contami-
• SVM is not an explosion-proof instrument and nated by radioactive materials, infectious agents
therefore must not be operated in areas with risk or other harmful substances that cause health
of explosion. hazards.
• The installation procedure should only be car- Precautions for highly inflammable samples
ried out by authorized personnel who are famil- and cleaning agents
iar with the installation instructions.
• Observe and adhere to your national safety reg-
• Do not use any accessories or spare parts other ulations for handling the measured samples
than those supplied or approved by Anton Paar (e.g. use of safety goggles, gloves, respiratory
GmbH (see section 3 of the Reference Guide). protection etc.).
• Make sure all operators are trained to use the • Only store the minimum required amount of
instrument safely and correctly before starting sample, cleaning agents and other inflammable
any applicable operations.
D89IB001EN-O 5
1 Safety Instructions
materials near the SVM. counter cooling: Disconnect the cooling hoses
and empty the cooling liquid from SVM.
• Do not spill sample/cleaning agents or leave
their containers uncovered. Immediately remove • To move or lift the instrument, grasp the ledge
spilled sample/cleaning agents. on top of the instrument’s back side with one
hand. Place the other hand under the display on
• Make sure that the setup location is sufficiently
the front side. There is a hollow for your fingers.
ventilated. The environment of SVM must be
kept free of inflammable gases and vapors. • Carry the instrument in front of you and keep it
close to your body.
• Connect SVM to the mains via a safety switch
located at a safe distance from the instrument.
In an emergency, turn off the power using this
switch instead of the power switch on SVM.
1.3 Conventions for Safety Messages
• Supply a fire extinguisher. The following conventions for safety messages are
used in this document:
• Ensure the sufficient supervision of SVM during
operation.
DANGER
1.2 Special Safety Instructions Description of risk.
Danger indicates a hazardous situation which, if
• Do not use SVM to measure fluids of the IIC
not avoided, will result in death or serious injury.
group according to EN 60079-14, such as e.g.
carbon disulfide or acetylene.
• Do not use SVM to measure fluids above WARNING
temperature class T3 according to ATEX
Directive 2014/34/EU, such as e.g. diethyl ether. Description of risk.
Warning indicates a hazardous situation which, if
• Read all safety data sheets of used sample and not avoided, could result in death or serious
cleaning liquids. Handling caustic liquids, acids, injury.
or biologically hazardous, easily flammable
liquids etc. involves a serious health risk for the
operator. Use appropriate protective equipment
CAUTION
(protective gloves, safety goggles, protective
clothing, fume hood...). Description of risk.
• If liquid was spilled over SVM, disconnect the Caution indicates a hazardous situation which, if
instrument from the mains. Clean and dry the not avoided, could result in minor or moderate
housing. If you suspect that liquid got into the injury.
instrument, have SVM cleaned and checked for
NOTICE
electrical safety by a service technician.
Description of risk.
• Compressed air for drying the measuring cells Notice indicates a situation which, if not avoided,
must be dry, free from oil and particles. The could result in damage to property.
pressure must be limited to a max. pressure of
200 kPa (= 2 bar = 29 psi). Suitable air prepara-
tion units are available from Anton Paar GmbH. 1.4 Safety Signs on the Instrument
Refer to the SVM Product Description List.
Transport NOTICE
• Empty the measuring cell and all hoses and Take care that the warning symbols remain
disconnect the waste container before you clearly legible.
move or lift the instrument. If operating with
6 D89IB001EN-O
1 Safety Instructions
SVM 3001 –
2
Optional Cooling Connectors
3 1
CAUTION
CAUTION
SVM 3001 –
Hot surface, risk of injury Spillage of liquids, cold surface
This symbol calls attention to the fact that the This symbol on SVM 3001 calls attention to the
measuring cell lock can get very hot. fact that the counter cooling connectors can be
• Do not touch the measuring cell lock and the very cold and that in case of accident liquid can
sample inlet/outlet without adequate flow from these connectors. Depending on the
protective measures (gloves) or make sure used cooling liquid and counter cooling
that the measuring cell temperature is lower temperature the cooling liquid can be a risk for
than 60 °C (140 °F) before touching these your health.
parts. • Do not touch the cold connectors with bare
• Do not remove the measuring rotor if the fingers. Risk of injury.
measuring cell temperature is not between • Keep all safety regulations that apply to the
15 °C (59 °F) and 50 °C (122 °F). used coolant.
• The applied coolant must not chemically
attack the wetted parts of the cooling circuit.
CAUTION • If using tap water for cooling, ensure free flow
through the system (open end).
• Make sure that connected cooling hoses do
Wear protective gloves
not get bent or entangled with objects or per-
sons.
Wear protective goggles • If using ethanol for cooling, remove it from the
SVM’s cooling circuit immediately after finish-
Risk of injury, liquid squirting out ing the low temperature measurements. Fol-
This symbol refers to rinsing the measuring cell low all safety instructions as described in
lock. It calls attention to the fact that liquid could section 1.1.
suddenly squirt out of the measuring cell lock if
you apply force and pressure builds up during In case of accidental leakage:
the rinsing procedure. The liquid could be hot. • Avoid skin contact and inhaling potential
vapors. Use appropriate protective equip-
Do not proceed with the rinsing when feeling ment (protective gloves, protective cloth-
resistance. Always wear protective equipment. ing,...).
D89IB001EN-O 7
2 SVM X001 - An Overview
2.1 Intended Use of the Instrument • pure hydrocarbon solvents and mixtures (e.g.
naphtha, toluene, hexane...)
SVM is intended for measuring dynamic viscosity • heavy heating oils, crude oils (treated), waxes,
and density of liquid, mainly oily samples and simul- vacuum distillates with high melting point or high
taneously calculating their kinematic viscosity and viscosity at elevated temperatures. For measur-
other related measuring quantities. ing these substances you need the Hot Filling
Attachment. For details on the attachment and
SVM 2001 exact specifications of measurable substances,
see Reference Guide.
SVM 2001 is designed for measuring at constant
temperature. It covers a measuring temperature • others: glycol (e.g. antifreeze), glycerine,...
range from 15 °C (59 °F) to 100 °C (212 °F). You
• with Option PEEK Rotor Bearings: some
can measure most of the samples listed for
samples with poor lubricity, such as silicone oils,
SVM 3001 within this range.
mixtures of water and glycol or glycerine, or sea
• Additional software function – upgradeable water. See also the Product Description List. For
mounting the optional bearings, see section 7.3.
With option "License Key SVM 2001 Viscosity In-
dex" (Mat. No. 199941), you can activate determi-
SVM 4001
nation of viscosity index and related parameters.
You get a license key (= unlock code). The first SVM 4001 contains two viscosity and two density
8 characters of the code are the serial number of the measuring cells in one housing. Each pair of cells
SVM 2001. If the SVM 2001 was ordered along with can be operated at a different measuring tempera-
this option, you get a certificate with the unlock ture within a range from 15 °C (59 °F) to 100 °C
code. Activate the option during initial installation. (212 °F).
Enter the unlock code here:
The cells are internally connected. You fill from the
- Menu > Service > Unlock Feature sample inlet (lower opening). The upper opening is
For further information, see the Reference Guide, the sample outlet. This design allows to access both
section 5.3.2.8 and table 34. viscosity cells for manual cleaning. Both visco cells
are closed with a measuring cell lock.
Due to the different construction, heating rates of
SVM 2001 are slower than those of SVM 3001. The sample liquid fills the cells in the following order:
8 D89IB001EN-O
2 SVM X001 - An Overview
The instrument software handles each pair of cells SVM 2001 / 3001 Right Side View
separately. For example, at the end of a calibration,
you can apply a suggested correction only to Cell 1,
while you reject it for Cell 2, or vice versa. To know
which data belong to which pair of cells, they come
with a prefix: "1)" or "2)".
SVM 4001 is ideally suited for testing lubricants and
for VI determination. Still, with SVM 4001, you can
measure most of the samples listed for SVM 3001
within the specified temperature range.
2 6 4 3 5 7 1
General
1 Xsample slot cover plate
NOTICE 2 Filling support
Risk of damage to the instrument 3 Measuring cell lock
4 Sample inlet
• Do not fill a sample if you do not know which 5 Sample outlet
cleaning liquid removes this sample. Make 6 Air pump outlet
sure the wetted parts of SVM are chemically 7 Splash guard
resistant to any tested sample or cleaning Fig. 4: SVM 2001 / SVM 3001 right side view
liquid.
SVM 4001 Right Side View
• Do not test any samples which harden or
solidify during the time they are in the 2 4
measuring cells.
6
• Do not test any samples that are specified in 5
1
section 1.2. 3
8
In case of further questions about your sample liquid
7
contact your local Anton Paar representative.
SVM is designed for use under ambient conditions
1 Xsample slot cover plate
as specified in appendix A.2. 2 Filling support
3 Measuring cell lock viscosity cell 1
4 Measuring cell lock viscosity cell 2
2.2 Functional Components 5 Sample inlet
6 Sample outlet
This section contains pictures and short 7 Air pump outlet
descriptions of all connectors and functional 8 Splash guard
components of SVM. Fig. 5: SVM 4001 right side view
4
2
1
1 3
D89IB001EN-O 9
2 SVM X001 - An Overview
13 7 6 3 1 2 4
2 1
1 USB interfaces (3 x)
2 Protection cover for USB interfaces
Fig. 7: SVM 2001 / SVM 4001 left side view
12 11 10 9 8 5
1 USB interface
2 VGA interface
3 RS-232 interface (COM)
4 Ethernet interface
5 CAN interface – to connect other measuring modules
6 "DRY AIR IN AIR PUMP" connector – to supply the
internal air pump with dry air
7 "DRY AIR IN INTERNAL" connector – to flood the
instrument’s inside with dry air
8 Power switch
9 Fuse holder
10 Power inlet
11 Type plate with serial number
12 Fan and venting slots
13 Carrying ledge
Fig. 8: SVM Rear view
Item 6 and 7: Find drying equipment in the Refer-
ence Guide.
10 D89IB001EN-O
2 SVM X001 - An Overview
Buttons area
Button Function
Opens the message list. A little yellow If not measuring, the cleaning button
note shows the number of messages in displays the following signs:
the list, if any. The button changes its
appearance depending on the current Red error sign: The cells are not clean.
error status: Yellow warning sign: The cells are not
Green OK sign: sufficiently clean for the selected
The general instrument status and the precision class.
error status of all measured samples of Green OK sign: The cells are sufficiently
the current sample list are OK. clean for the selected precision class.
Unfreezes the screen after a finished
Yellow warning sign:
measurement.
- The instrument (or system) has a
The screen is frozen.
minor problem (e.g. a calibration correc-
The screen is unfrozen. A continuous
tion point has expired).
reading of the current measuring values
- Filling warning for one or more samples
is shown.
of the current sample list a.
This button is not available if limited
Red error sign: visibility of measuring values is enabled.
- The instrument (or system) has a major See General Software Functions
problem that needs to be fixed before Reference Guide, "Value Visibility" or
you continue with measurements (e.g. appendix C, SVM Reference Guide.
the sample changer is blocked).
Displays information on using favorites.
- The required precision or repeatability
This icon is visible only if the quick
for one or more samples of the current
access area is expanded.
sample list could not be reached.
- One or more samples of the current a SVM 2001 does not provide filling warnings.
sample list could not be measured (e.g.
the density measuring cell is partly
empty and does not oscillate).
D89IB001EN-O 11
3 Installing the Instrument
12 D89IB001EN-O
3 Installing the Instrument
5 5
2
2 1 4 3
6 6
4
Connect the FEP hose 250x3x2 mm (4) as waste TIP: Place the waste hose correctly, otherwise a
hose to the sample outlet (see Fig. 11): sucking effect can occur and bubbles may be
sucked into the measuring cells. Low viscosity sam-
TIP: Remove the measuring cell lock first to have
ples, in particular, could leak from the measuring
enough room for your fingers.
cell. Place the waste hose in a way that it runs slight-
ly upwards into the waste bottle. See Fig. 11.
1. Screw one end of the hose into the sample
outlet. Tighten the hose connector with your
fingers. Connect a silicone hose to the air pump outlet:
2. Fix the free end of the waste hose to the waste 1. Cut a piece of approx. 320 mm (12.5 in) length
bottle. Attach the hose connector to one of the from the silicone hose contained in the
three holes in the lid. accessory kit.
The end of the FEP hose must be level with the 2. Attach the silicone hose to the air pump outlet.
PEEK screw connector. The hose must not
reach down into the waste bottle. Use the yellow 3. Attach an Adapter Luer hose (from the
marking to fix the hose in the connector. See accessory box) to the other end of the silicone
arrow. hose.
D89IB001EN-O 13
3 Installing the Instrument
14 D89IB001EN-O
4 Calibration, Calibration Correction and Adjustments
• Store the data of the standard liquid you plan to • The first table shows the status before
use in the Viscosity Standards Management correction. If you do not apply the correction, the
(see Reference Guide). displayed viscosity deviation persists.
• Define a calibration routine in the Calibration • The second table shows the status after
Management (see Reference Guide). correction. If you apply the correction, SVM
corrects the displayed viscosity deviation.
• Prepare the standard liquid to be used.
Degas the liquid. See Reference Guide. TIP: If you want to print or export the data, do so
before taking any further action. Rejecting, applying
• Fill a syringe with standard liquid: or saving the data closes this window.
- 5 mL syringe >> up to the 6 mL mark 5. Depending on the results, the instrument
- 10 mL syringe >> up to the 10 mL mark recommends an action. It marks the
recommended button with an arrow.
Procedure
The following limits prevent the application of erro-
During calibration, SVM 4001 displays all data of neous correction points (with too high deviation):
the following procedure for each pair of cells.
- ±5 %: normal viscosity range (> std. oil N7.5)
1. Tap <Menu> and select Adjustments > SVM - ±10 %: low-viscosity range (~ N7.5 => S3)
User Adjustments > Calibration. - ±20 %: ULV range (< std. oil S3).
2. Select a calibration from the drop-down list. • <Apply Correction>: The calibration measure-
3. Set the temperature (SVM 4001: temperatures) ment is valid (precision class and repeat devia-
at which you want to perform the calibration. tion fulfilled). The measured values deviate
SVM checks whether reference values are more than allowed from the reference values.
available at this (these) temperature(s). If you apply the correction, you correct the vis-
Optional: Set a Filling Temperature – required cosity deviation, i.e. you apply a correction fac-
only if the viscosity at calibration temperature is tor to SVM. The calibration and the fact that you
very high. SVM uses the filling temperature for applied it are saved: see Calibration History.
each refill (calibration takes longer). Tap
<Next>. TIP: Only users with administrator rights are al-
lowed to apply a calibration correction. Depending
Follow the instructions of SVM.
on your user level, SVM asks for an administrator
TIP: The cleaning value shows whether the density password.
oscillator is clean and dry. For calibration, the clean-
• <Save only History>: The calibration and its
ing value should reach at least 90 %.
results are saved in the Calibration History (see
4. At the end of calibration, SVM displays a Reference Guide). No correction is applied.
window "Calibration finished".
D89IB001EN-O 15
5 Performing a Measurement
5 Performing a Measurement
To perform a repeat measurement according to
ASTM D7042, refer to Fig. 13:
Most samples need no special preparation for filling
The following sub-sections describe all steps of them. Find special sample preparation procedures
performing measurement (sample preparation, in the Reference Guide.
filling, measuring,...) in detail.
Make sure that the cells are clean and dry (section 6.2).
Fill a 5 mL (SVM 4001: 10 mL) syringe. Fill 1.5 mL (2.5 mL) of sample into the cells (section 5.1).
Determination is ready.
16 D89IB001EN-O
5 Performing a Measurement
D89IB001EN-O 17
5 Performing a Measurement
NOTICE
Risk of damage to the measuring cells 2
The pressure when filling or pressing sample out
of the cells must not exceed 500 kPa = 5 bar
(72 psi), otherwise sample may leak out at the
bearings. This pressure corresponds to a force
of approx. 65 N on the plunger of a 5 mL syringe.
Take care especially with highly viscous
samples.
A too high pressure may also cause damage to
the measuring cells. In this case Anton Paar is
not liable for damage.
1 Syringe
2 Filling support (with Adapter Luer Lock)
4. Plug the syringe firmly into the filling support. Fig. 16: Filling the measuring cells of SVM 4001
5. Push the plunger of the syringe slowly and 6. The cells are now filled.
continuously down. Proceed with section 6.
- For SVM 2001 / 3001, fill at least 1.5 mL of
sample (3 mL for sample displacement).
- For SVM 4001, fill at least 2.5 mL of sample Find special sample filling routines in the Reference
(3 mL for sample displacement) Guide.
5.2 Measuring
After filling the measuring cells, enter a sample
1 name and change the quick settings parameters, if
required.
Quick settings
1. Tap <Quick Settings> on the main screen.
2. Tap on a quick settings parameter to highlight it.
2
Tap on the field in the "Parameter Select" col-
umn in order to enter a sample name/value or to
select a different input from the drop-down list.
Confirm the input by tapping <OK>.
3. When all quick settings parameters have been
defined, tap <OK> to save the input.
18 D89IB001EN-O
5 Performing a Measurement
1
2
3 4 5
6 7 8 9 10 11
12 13
1 1st line: viscosity stability indicators | RDV values 10 Yellow indicators: The instrument has not (yet)
2 2nd line: density stability indicators | RDD values reached the set precision class
3 Indicators required for the set class | White indicators: 11 Green indicators: The instrument has reached the set
Values do not fulfill any stability criteria: Unsteady precision class; this can also be the case for only one
4 Precision indicator not required for the set class of these two quantities (density or viscosity) while
5 No repeat deviation values available (single determi- measurement is still in progress
nation or first determination of repeat measurement) 12 Example 1: Repeat Measurement, in progress,
6 Set precision class: Ultrafast 1st determination, set precision class "precise",
7 Set precision class: Fast currently reached precision class "fast"
8 Set precision class: Precise 13 Example 2: Repeat Measurement, finished, set and
9 Set precision class: Ultraprecise (not available for reached precision class "precise"
SVM 2001)
Fig. 17: SVM precision widget
D89IB001EN-O 19
5 Performing a Measurement
20 D89IB001EN-O
6 Cleaning
6 Cleaning
To assure constant and high accuracy of your It has to be a good solvent for all sample
measurements, use regular and effective cleaning components. If this first cleaning liquid does not dry
routines. Clean the measuring cells immediately up fast and/or without leaving residues, a second
after each measurement. cleaning liquid is required.
TIP: If measuring similar, fully miscible samples, Cleaning liquid 2 must completely dissolve and
one sample can be replaced by the next. This re- remove cleaning liquid 1. It must easily evaporate by
quires more sample liquid, as the first sample batch a stream of dry air.
must be flushed completely from the measuring
TIP: Do not use a cleaning liquid with a boiling point
cells by the following one. In this case always clean
close to or lower than the measuring cell tempera-
the cells at the end of a work shift, but at least once
ture selected for cleaning. If the cleaning liquid boils,
every 24 hours.
it evaporates and cannot dissolve the substance in
the cells.
Wipe sample spills on the instrument immediately
with a soft tissue or dry cloth (section 6.3). Find detailed information on the chemical properties
of solvents in the Reference Guide.
At regular intervals, depending on the type of
sample and on the instrument’s frequency of use, Table 1: Recommended cleaning liquidsa
perform a special cleaning (Reference Guide) and
clean the measuring rotor (section 7.3). Sample / Condition Cleaning liquid
Always read the safety data sheet of a liquid Samples which are not Two cleaning liquids:
before you use it as cleaning liquid. soluble in petroleum Liquid 1: aromatic
benzine (e.g. some solvent e.g. toluene/
A suitable cleaning liquid must completely dissolve kinds of lube oils, xylene
and remove the sample. some heavy oils and Liquid 2: e.g.
The chemical quality must be high enough so that crude oils) / Max. cell petroleum benzine or
the cleaning liquid does not leave any residues (e.g. temperature: 100 °C a second rinsing with
particles). toluene
D89IB001EN-O 21
6 Cleaning
If you are not sure if a cleaning liquid is suitable for Remove the sample from the measuring cells:
your sample, perform a preliminary test in a test
• Suck low viscosity oils back into the syringe.
vessel. This shows if any phase separation,
Empty the syringe into the waste container.
precipitate or opalescence occurs.
• Fill the syringe with air. Connect it to the filling
For detailed information on selecting suitable
support. Push down the plunger to remove the
solvents, on solubility tests, on sample - solvent
sample from the measuring cells.
combinations and on solvent properties refer to the
Reference Guide. • You can also connect the air hose to the filling
support and switch on the air pump to push out
the sample.
You can monitor the cleaning procedure via the
Cleaning Screen. See section 6.2.2.
22 D89IB001EN-O
6 Cleaning
3
7. If required (e.g. for hard to remove samples),
repeat the above steps a few times.
8. Rinse the cells with some more cleaning liquid.
9. To dry the cells attach the air hose to the filling
support. See Fig. 22. Tap button to start
the air pump.
Wait for the air pump timeout (default: 120 s) or
stop the air pump by tapping button .
D89IB001EN-O 23
6 Cleaning
Ultrafast 60 %
Fast 70 %
1 2 Precise 80 %
Ultraprecise 90 %
24 D89IB001EN-O
6 Cleaning
D89IB001EN-O 25
7 Upkeep and Additional Cleaning
Rinse and dry the measuring cells - immediately after each measurement
(section 6.2) - if the cleaning value is not green
- if the instrument was not used for a long
period of time
Disassemble the viscosity cell and perform man- - once a day to once a month depending on
ual cleaning the number of samples and sample type
(section 7.3) - after measuring hard-to-remove samples
- if measuring results are suspicious
Clean the measuring cell lock - if the sample inlet does not move (smoothly)
(section 7.4 of the Reference Guide) or you cannot feel the resistance of the
spring (see section 7.3)
- after measuring hard-to-remove samples
Visual inspection of O-rings and rotor bearings - when manually cleaning the viscosity cell
(section 7.3)
Check measurement with a sample of known vis- - regularly, preferably daily or at least before
cosity and density starting a measurement series
(section 5)
26 D89IB001EN-O
7 Upkeep and Additional Cleaning
3 4
7.1 Leak Test
A leak test checks whether the measuring cells are
leak-tight. Leak-tightness is vital for correct function
of SVM and for stable and reliable measuring
values. Perform a leak test once a month, but
always after cleaning the rotor (see section 7.3) and 5
if SVM does not achieve stable measuring values.
The measuring cells must be clean and dry when
you perform a leak test. See section 6.2.1.
2 1
7.1.1 Complete Measuring Cell
1 Adapter Luer Lock on sample inlet
2 Adapter Luer Lock on sample outlet
Required equipment
3 Male Luer plug
• Glass syringe 4 Glass syringe
5 1 mL mark
• 2 Adapters Luer Lock 1/4"-28 UNF PEEK
Fig. 24: Leak test - pressing the plunger in to 1 mL
• 1 Male Luer plug
When you release the plunger, it should move
out at least to the 3 mL mark.
D89IB001EN-O 27
7 Upkeep and Additional Cleaning
1 3 mL mark
Fig. 25: Leak test start - Syringe plunger at 4 mL mark
28 D89IB001EN-O
7 Upkeep and Additional Cleaning
7.2 Rinsing the Thermostat Tube 5. Fill a suitable syringe with cleaning liquid or use
a wash bottle. Fill cleaning liquid into the
measuring cells until you see the liquid in the
This procedure means rinsing the inside of the
waste hose.
viscosity measuring cell without measuring rotor.
This serves to rinse the walls of the measuring cell - If using a syringe, leave it on the filling sup-
and the ceramic bearings inside the cell and on the port. Move the syringe’s plunger up and
measuring cell lock. down repeatedly for better cleaning. See
Fig. 22, p. 24.
Perform this procedure regularly (see Reference
Guide, section II). Always perform a standard - If using a wash bottle, the liquid should not
cleaning (section 6.2.1) first. reach the highest point of the waste hose.
See marks in Fig. 21, p. 23. This prevents
Required equipment that the liquid drains out of the cells due to
suction when removing the wash bottle.
• Cleaning liquid(s) (see section 6.1)
6. Rinse with some more cleaning liquid.
• Lint-free tissue paper
7. If required (e.g. for hard to remove samples),
• Protective gloves repeat the above steps a few times.
Procedure 8. To dry the cells attach the air hose to the filling
support. Tap button to start the air pump.
TIP: It is not necessary to switch off SVM.
Wait for the air pump timeout (default: 120 s) or
For SVM 4001, proceed as described in this sec- stop the air pump by tapping button .
tion. Perform the procedure for both viscosity cells.
CAUTION
Hot surface
7.3 Cleaning the Measuring Rotor
This symbol calls attention to the fact that the
Clean the measuring rotor at regular intervals (see
measuring cell can get very hot.
Reference Guide, section II) for good function of the
Do not remove the measuring rotor if the
viscosity cell.
measuring cell temperature is not between 15 °C
(59 °F) and 50 °C (122 °F). TIP: Combine this cleaning with a rinsing of the ther-
mostat tube. See section 7.2.
If you intend to retrofit an SVM with measuring rotor
2. Open the measuring cell lock and remove the
bearings made of PEEK (see section 2.1 or the
measuring rotor. See section 7.3, steps 1. to 7.
Product Description list), proceed as described in
3. Fix the measuring cell lock again. Turn it this section. Mount the PEEK bearings instead of
clockwise until you hear and feel a click. the original ceramic bearings when assembling the
measuring rotor.
4. Make sure that the inlet and waste hose are
connected.
D89IB001EN-O 29
7 Upkeep and Additional Cleaning
Required equipment
• Cleaning liquid(s) (see section 6.1)
• Cleaning brushes
• Puller for rotor bearings
• 1 Adapter Luer Lock 1/4"-28 UNF
• Lint-free tissue paper
• Q-tips (extra long)
• Small flat screw driver
• Protective gloves
General instruction
• Always use fresh tissue paper and cleaning
liquid.
Fig. 27: Opening the measuring cell lock
• Always wipe the brushes after using them – also
in-between cleaning steps. 2. Unscrew the waste hose from the sample outlet.
Screw an Adapter Luer Lock into the sample
• Place all parts on clean tissue paper. outlet. SVM 4001: Screw an Adapter Luer Lock
into the measuring cell lock of cell 2.
Procedure
3. Put on protective gloves.
TIP: It is not necessary to switch off SVM.
4. Wet some tissue paper with cleaning liquid and
For SVM 4001, proceed as described in this sec- wipe the inside of the measuring cell lock. Brush
tion. Perform the procedure for both viscosity cells. the sample inlet with the smallest brush
(2.7 mm).
NOTICE FOR SVM 4001
Push the sample inlet repeatedly into the cell
Risk of erroneous results and leakage
lock (see arrow in Fig. 28). The built-in spring
Handle the measuring rotors separately and one pushes it out again. The inlet must move
after the other. The measuring rotors or their smoothly in both directions.
parts must not be exchanged. Otherwise,
viscosity values are no longer valid. Leakage
might occur. 1
Keep each measuring rotor and its parts in a
separate, clearly marked vessel.
CAUTION
1 Sample inlet
Hot surface Fig. 28: Measuring cell lock
This symbol calls attention to the fact that the
measuring cell lock can get very hot. 5. In case the inlet moves jerkily, gets stuck or you
Do not remove the measuring rotor if the do not feel the resistance of the spring, proceed
measuring cell temperature is not between 15 °C according to section 7.4 (Reference Guide) .
(59 °F) and 50 °C (122 °F). If the sample inlet moves smoothly, continue as
follows:
1. Open the measuring cell lock by turning it
6. Take the turning measuring rotor out by the
counter-clockwise. There is no need to
drive disc. Use your fingertips or a small flat
disconnect the hose from the sample inlet.
screwdriver. Pull the measuring rotor out
sideways. See Fig. 29.
30 D89IB001EN-O
7 Upkeep and Additional Cleaning
NOTICE
1 Risk of damage to the titanium rotor
3 1 4 2
1 Measuring tube 2 3 1
2 Rotor bearing long with drive disc
3 Rotor bearing short
4 Titanium rotor 1 Q-tip – squeezing the soft cotton bud
2 Measuring tube with rotor inside
Fig. 30: Measuring rotor – parts when disassembled 3 Inserting the Q-tip by turning (soft end first)
Fig. 32: Removing the titanium rotor using the Q-tip
NOTICE
Risk of damage to the instrument 11. Wet the smaller brush (5 mm) with cleaning
liquid and insert it into the measuring tube.
Do not use force.
Brush the tube. Rotate the brush to clean the
Do not try to loosen the drive disc.
threads of the bearings.
9. Tilt the measuring tube and let the titanium rotor 12.Check the threads of the rotor bearings for
drop onto a sheet of tissue paper. sample residues. Brush them with cleaning
liquid.
If the titanium rotor sticks to the measuring tube,
you can remove it later using a Q-tip. 13.Wet sheets of tissue paper with cleaning liquid
and wipe all parts.
10.Unscrew the rotor bearing short using the puller
for rotor bearings. Pull the rotor bearing out of 14.Clean the ceramic bearings on the inner ends of
the measuring tube. You have to overcome the the rotor bearings and on the inside of the
resistance of the O-ring. measuring cell lock. Wet Q-tips with cleaning
liquid and wipe the ceramic bearings.
TIP: If the measuring tube slips through your fin-
gers, use a piece of rubber or comparable material In case of hard to remove residues, wet the tip
to get a better grip on it. of a brush and brush the ceramic bearings. Use
the smallest brush (2.7 mm) to clean the inside
For example, wrap a thin rubber protection glove of the rotor bearings. Then wipe the ceramic
several times around the measuring tube. bearings again.
D89IB001EN-O 31
7 Upkeep and Additional Cleaning
NOTICE Fig. 34: Rinsing the measuring cells from the outlet
Risk of damage to the ceramic bearing
21.Plug the air hose into the Adapter Luer Lock at
Clean the inside of the measuring cell with care. the sample outlet. Hold a sheet of tissue paper
There is a ceramic bearing inside. in front of the measuring cell opening and start
Do not use excessive force. Do not push the the air pump with button .
brush or Q-tip into the cell with great speed.
Do not use any other tool than the
recommended brush or Q-tips.
TIP: SVM 4001 – Before rinsing the cells, clean the 1 Gap – tighten the bearing until that gap is closed
parts of cell two as described above. In order to
rinse from cell 2, fix the measuring cell lock of cell 2 Fig. 36: Assembling the measuring rotor
(upper cell). Plug the syringe with cleaning liquid If you do not succeed with your fingers, use the
into the Adapter Luer Lock on of that measuring cell puller for rotor bearings to close a potential gap.
lock and rinse as described. Do not tighten the rotor bearing any further.
32 D89IB001EN-O
7 Upkeep and Additional Cleaning
25.Insert the measuring rotor into the thermostat • Utility knife (Stanley knife) or small cutting pliers
tube. The measuring rotor starts turning when it or tweezers
is in place.
• Protective gloves
26.Unscrew the Adapter Luer Lock from the sample
outlet. Procedure
27.Screw the waste hose into the sample outlet. TIP: For SVM 4001, proceed as described below.
Perform the procedure for both viscosity cells.
28.Fix the measuring cell lock. Turn it clockwise
until you hear and feel a click.
NOTICE FOR SVM 4001
Check whether the measuring cells are leak-tight Risk of erroneous results and leakage
(see section 7.1).
Handle the measuring rotors separately and one
after the other. The measuring rotors or their
7.4 Replacing O-Rings parts must not be exchanged. Otherwise,
viscosity values are no longer valid. Leakage
TIP: By default, SVM 3001 comes with might occur.
Kalrez® 0040 Spectrum O-rings. This material is
very expensive. You can use Viton® Extreme O- 1. Disassemble the measuring rotor and clean it.
rings if the following applies to your instrument and Check all parts for damages. See section 7.3.
applications:
• Chemical resistance of Kalrez® is not required.
• Elasticity at low temperatures (< -20 °C / -4 °F)
is not required, i.e. no operation at these low
temperatures.
Find suitable Viton® Extreme O-rings in the SVM
Product Description List.
SVM 2001 and SVM 4001 come with Viton ® Ex-
treme O-rings. If required, upgrade the chemical re-
sistance to Kalrez® 0040 Spectrum. 1 2 3
D89IB001EN-O 33
8 Maintenance and Repair
34 D89IB001EN-O
Appendix A: Technical Data
Shear rate typically 0.5 s-1 to 1100 s-1, depending on viscosity and temperature
a For temperatures below -20 °C (-4 °F) additional counter cooling is required.
Temperature reproducibility • 0.03 °C (0.054 °F) from 15 °C to 100 °C (59 °F to 212 °F)
• 0.05 °C (0.09 °F) outside the range specified above –
applies to SVM 3001 only
a Valid for ideal measuring and sample conditions within the works adjustment range by using petroleum
based viscosity and density standards. Suitable standards are listed in the SVM X001 Product Description
List (see "Viscosity Standard Liquids" / "Density Standard Liquids").
b Attested at the points of the works adjustment (see below) or at calibration correction points (see Reference
Guide). Specified reproducibility does not include the uncertainty of the standard used for verification.
c Attested for the works adjustment range (see below). Specified reproducibility does not include the uncer-
tainty of the standard used for verification.
D89IB001EN-O 35
Appendix A: Technical Data
3 6
9
11
5 SVM 2001
SVM 4001
1
10
4 2 12
7 8
3000 30000
1 Works adjustment range 9 100 °C (212 °F): Upper limit of temperature
2 Low temperature range measuring range of SVM 2001/4001
3 High temperature range 10 15 °C (59 °F): Lower limit of temperature measuring
4 Ultra low viscosity (ULV) range* range of SVM 2001 / SVM 4001
5 High viscosity range 11 Points of Full Range Adjustment (e.g. C-oil at 60 °C)
6 Extended high viscosity range – requires additional 12 Extremely high viscosity range with limited measur-
accessory for filling (see section II, Reference Guide) ability: Depending on the sample, reduced lubricity
7 3000 mPa·s: can limit the stability, determinability, repeatability and
Recommended filling viscosity at filling temperature reproducibility of measurements.
8 30000 mPa·s: Limit of viscosity measuring range
Fig. 38: Viscosity works adjustment range and other viscosity/temperature measuring ranges
*) There is no special ULV adjustment for SVM. The Full Range Adjustment covers also this range. Use
calibration correction to improve results.
Table 6: SVM Precision Classes
36 D89IB001EN-O
Appendix A: Technical Data
Maximum recommended filling viscosity 3000 mPa·s (3000 mm²/s) at filling temp.
Net weight SVM 15.9 kg (35.0 lbs) 17.6 kg (38.7 lbs) 17.8 kg (39.2 lbs)
Shipping weight (incl. standard supply) 20.5 kg (45.1 lbs) 22.2 kg (48.8 lbs) 22.4 kg (49.3 lbs)
Maximum pressure filling 500 kPa = 5 bar (72 psi) relative, no suction allowed
Maximum pressure measuring 100 kPa = 1 bar (14.5 psi) relative, no suction allowed
Housing material
Top & side cover Aluminum, coated with a poly acrylate resin varnish
Cover of Xsample slot Styrene-butadiene, coated with a poly acrylate resin varnish
D89IB001EN-O 37
Appendix A: Technical Data
Pollution degree 2
Overvoltage category II
Interface specifications
RS-232 printer settings Baud rate: 9600; Parity: None; Stop bit: 1; Data bits: 8
WARNING
High voltage. Risk of injury or death. NOTICE
Risk of damage to the instrument
Serious injuries are possible through high
voltage if the following hints are not adhered to. Connect only Anton Paar equipment to the CAN
Only connect devices to the interfaces that interface and adhere to the following limits. The
comply with PELV (protective extra-low voltage) CAN interface power supply is limited to 72 W.
according to IEC 61140 or with SELV (safety Power at the CAN is only available if no
extra-low voltage) according to IEC 60950. Xsample 530 is installed.
38 D89IB001EN-O
Appendix B: Wetted Parts
Material Part
FEP (Fluorinated Ethylene Propylene) • Hose between filling support and sample inlet
• Waste hose
PTFE (Poly Tetra Fluoro Ethylene) Sealing cone inside measuring cell lock
D89IB001EN-O 39
Appendix B: Wetted Parts
Material Part
Material Part
40 D89IB001EN-O