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Drying is simply removal of water from any solid substance by thermal means but
below the boiling point of temperature. Food drying is one of the oldest methods in
human civilization for prevention of food. Food industries are now one of the most
developing industries in India. Food preservation is key factor affecting the quality of
product and a long life product is the one desired by the manufacturers and the
consumers.
In this project we have fabricated a batch type tray dryer which is tested to dry
tomatoes and potatoes at varying temperatures such as 60, 70 and 80 degrees
centigrade at constant flow rate of air and at regular time intervals the weight of the
sample was recorded initially and the amount of initial sample was kept constant
which was 100grams.
Keywords: Drying, Kinetic data, drying periods, Theoretical and experimental time
required, Moisture Ratio
o CONTENTS
Chapter 6:-
Chapter 7:-
o Conclusion 30
References 31
List of Figures
In order to increase the aggregate value of food products, research in the area of dehydration
has been widely extended to search products with few alterations in their nutritional
characteristics.
The drying rate is so small for biological materials compared with other materials that they
require a longer drying time. This long drying time induces to high drying cost. Therefore,
the understanding of the drying system, process and equipment, is essential for food
engineers to design an optimized drying system.
Drying is generally applied to removal of relatively small amount of water from solid
material to reduce the content of residual liquid to an acceptable low value.
Wide variety of dehydrated foods that are now available to the consumer (snacks, dry mixes
and soups, dried fruits etc.) and the increasing concern for meeting quality specification and
conserving energy emphasize the need for a thorough understanding of the drying operation
and the problems related to the design and operation of dryers.
In the case of dryers design has become an increasingly challenging problem aiming at the
evaluation of appropriate type of equipment, its associated flow sheet structure, its optimum
construction characteristics and operating conditions of each unit involved in the overall flow
sheet. Although the modelling of drying processes is well developed with adequate
comprehension of the process itself most models incorporate a large number of
thermophysical properties and transport conditions which in most cases are only in precisely
known producing inaccurate or erroneous results on large scale industrial applications.
Tray dryers constitute an important family of convective dryers where the drying medium is
hot air or combustion gases coming from a furnace. They are adaptable to the drying of
almost any material that can be put in a tray.
In general batch or semi-batch operation is used. In all cases design efforts in this field focus
on the determination of appropriate equipment configuration that is number of parallel
processor lines trucks and determination of lot sizing and corresponding operational
condition within each processor.
The solids to be dried may be in many different forms—flakes, crystals, powders, slabs or
continuous sheets and may have widely differing properties. The liquid to be vapourized
maybe on the surface of solid , as in drying salt crystals, it may be entirely in the solid, as in
solvent removal from sheet of polymer or it may be partly outside partly inside.
DRYING
Drying is a mass transfer process consisting of the removal of water or another solvent by
evaporation from a solid, semi-solid or liquid. This process is often used as a final production
step before selling or packaging products.
To be considered "dried", the final product must be solid, in the form of a continuous sheet
(e.g., paper), long pieces (e.g., wood), particles (e.g., cereal grains or corn flakes) or powder
(e.g., sand, salt, washing powder, milk powder). A source of heat and an agent to remove the
vapor produced by the process are often involved. In bioproducts like food, grains, and
pharmaceuticals like vaccines, the solvent to be removed is almost invariably water.
In drying, relatively small amount of water or other liquid is removed from a solid or semi
solid material (using thermal energy) , whereas in evaporation relatively large amount of
water is removed from solutions. Drying involves the removal of water at a temperature
below the boiling point, while evaporation involves the removal of water as vapour at its
boiling point. Drying involves circulation of hot air or other gas over a solid material for
removal of water, whereas evaporation involves use of steam heat for removal of water. To
obtain dried product is the main aim of drying while to obtain concentrated solutions is the
main purpose of evaporation.
DRYING MECHANISM
In some products having relatively high initial moisture content, an initial linear reduction of
the average product moisture content as a function of time may be observed for a limited
time, often known as a "constant drying rate period". Usually, in this period, it is surface
moisture outside individual particles that is being removed. The drying rate during this period
is mostly dependent on the rate of heat transfer to the material being dried. Therefore, the
maximum achievable drying rate is considered to be heat-transfer limited. If drying is
continued, the slope of the curve, the drying rate, becomes less steep (falling rate period) and
eventually tends to nearly horizontal at very long times.
The product moisture content is then constant at the "equilibrium moisture content", where it
is, in practice, in equilibrium with the dehydrating medium. In the falling-rate period, water
migration from the product interior to the surface is mostly by molecular diffusion, i,e. the
water flux is proportional to the moisture content gradient. This means that water moves from
zones with higher moisture content to zones with lower values, a phenomenon explained by
the second law of thermodynamics. If water removal is considerable, the products usually
undergo shrinkage and deformation, except in a well-designed freeze-drying process.
The drying rate in the falling-rate period is controlled by the rate of removal of moisture or
solvent from the interior of the solid being dried and is referred to as being "mass-transfer
limited". This is widely noticed in hygroscopic products such as fruits and vegetables, where
drying occurs in the falling rate period with the constant drying rate period said to be
negligible.
METHODS OF DRYING
Freeze drying or lyophilization is a drying method where the solvent is frozen prior
to drying and is then sublimed, i.e., passed to the gas phase directly from the solid
phase, below the melting point of the solvent. It is increasingly applied to dry foods,
beyond its already classical pharmaceutical or medical applications. It keeps
biological properties of proteins, and retains vitamins and bioactive compounds.
Pressure can be reduced by a high vacuum pump (though freeze drying at atmospheric
pressure is possible in dry air). If using a vacuum pump, the vapour produced by
sublimation is removed from the system by converting it into ice in a condenser,
operating at very low temperatures, outside the freeze drying chamber.
Supercritical drying (superheated steam drying) involves steam drying of products
containing water. This process is feasible because water in the product is boiled off,
and joined with the drying medium, increasing its flow. It is usually employed in
closed circuit and allows a proportion of latent heat to be recovered by recompression,
a feature which is not possible with conventional air drying, for instance. The process
has potential for use in foods if carried out at reduced pressure, to lower the boiling
point.
Natural drying takes place when materials are dried with unheated forced air, taking
advantage of its natural drying potential. The process is slow and weather-dependent,
so a wise strategy "fan off-fan on" must be devised considering the following
conditions: Air temperature, relative humidity and moisture content and temperature
of the material being dried. Grains are increasingly dried with this technique, and the
total time (including fan off and on periods) may last from one week to various
months, if a winter rest can be tolerated in cold areas.
Spray drying is a method of producing a dry powder from a liquid or slurry by
rapidly drying with a hot gas. This is the preferred method of drying of many
thermally-sensitive materials such as foods and pharmaceuticals. A consistent particle
size distribution is a reason for spray drying some industrial products such as
catalysts. Air is the heated drying medium; however, if the liquid is a flammable
solvent such as ethanol or the product is oxygen-sensitive then nitrogen is used.
Drum drying is a method used for drying out liquids from raw materials with drying
drum. In the drum-drying process, pureed raw ingredients are dried at relatively low
temperatures over rotating, high-capacity drums that produce sheets of drum-dried
product. This product is milled to a finished flake or powder form. Modern drum
drying techniques results in dried ingredients which reconstitute immediately and
retain much of their original flavour, colour and nutritional value.
DRYING KINETICS
Drying kinetics play a significant role in the selection of dryers. Apart from simply deciding
the residence time required, it limits the types of suitable dryers. Location of the moisture
(whether near surface or distributed in the material), nature of moisture (free or strongly
bound to solid), mechanisms of moisture transfer (rate-limiting step), physical size of
product, conditions of drying medium (e.g., temperature, humidity, flow rate of hot air for a
convective dryer), pressure in dryer (low for heat-sensitive products), etc., have a bearing on
the type of suitable dryer as well as the operating conditions. Most often, not more than one
dryer type will likely meet the specified selection criteria.
The above formula shows formula for calculating moisture content on dry and wet basis. This
formula was used to calculate the moisture content in this project.
DEFINITIONS
In drying operations with various terms are used which are defined below containing of
substance and humidity relations with the dry bulb and wet bulb temperature
1. Bound moisture:- the moisture content by substance which exit equilibrium vapour
pressure less than that of pure liquid at the same temperature.
2. Unbound moisture:- it refers to the moisture contained by a substance which exerts
and equilibrium vapour pressure equal to that of pure liquid at same temperature
3. Free moisture:- free moisture is that moisture content by a substance in excess of
equilibrium moisture only the free moisture can be evaporated and free moisture
content of solid depends upon the vapour concentration in the air
4. Equilibrium moisture content:- it is the moisture content of a substance that is in
equilibrium with its vapour in the gas phase under the specified humidity and
temperature of the hot gas or air it represents the limiting moisture content to which or
given material be dried under constant drying conditions
5. Moisture content on wet basis: - the ratio of the weight of moisture to the weight of
the wet feed material.
6. Moisture content on dry basis: - The moisture of wet feed material on dry basis is
defined as the ratio of weight of the moisture weight of the solids present in the wet
feed material.
7. Critical moisture content: - it is the moisture content of a material at which the
constant rate period ends and the falling rate period starts.
8. Constant rate period: - it is the part of the drying process during which the rate of
drying expressed as the moisture evaporated per unit time per unit area of drying
surface remains constant.
9. Falling rate period:- it is that part of the drying process during which the rate of
drying varies with time and instantaneous drying rate period expressed as the amount
of moisture evaporated per unit time per unit area of drying surface continuously
decreases.
10. Relative humidity (RH):- is the ratio of the partial pressure of water vapour to
the equilibrium vapour pressure of water at a given temperature
11. Humidity is the amount of water vapour present in the air. Water vapour is the
gaseous state of water and is invisible. It is the ration of the mass of water vapour to
the mass of dry air present in air-water vapour mixture under any given set of
conditions.
12. Saturation humidity (Hs):- it is the humidity of air when it is fully saturated with
water vapours.
13. Percentage humidity: - it is the ratio of humidity of air to the humidity of saturated
air.
14. Dry bulb temperature: - the temperature of air-water vapour mixture recorded by a
thermometer whose bulb is kept dry is called dry bulb temperature.
15. Wet bulb temperature: - The temperature of air-water vapour mixture recorded by a
thermometer whose bulb is kept wet by wrapping a wet cloth in the open air is called
wet bulb temperature.
16. Dew point: - when the air water-vapour mixture is cooled and starts to condense is
known as the dew point temperature.
RATE OF DRYING
Drying periods
In drying, it is necessary to remove free moisture from the surface and also
moisture from the interior of the material. If the change in moisture content for a material
is determined as a function of time, a smooth curve is obtained from which the rate of
drying at any given moisture content may be evaluated.
The form of the drying rate curve varies with the structure and type of material, and two
typical curves are shown in Figure . In curve 1, there are two well-defined zones: AB,
where the rate of drying is constant and BC, where there is a steady fall in the rate of
drying as the moisture content is reduced. The moisture content at the end of the constant
rate period is represented by point B, and this is known as the critical moisture content.
Curve 2 shows three stages, DE, EF and FC.
The stage DE represents a constant rate period, and EF and FC are falling rate periods. In
this case, the Section EF is a straight line, however, and only the portion FC is curved.
Section EF is known as the first falling rate period and the final stage, shown as FC, as
the second falling rate period.
As the moisture content decreases the constant rate period ends at a definite moisture content
and during further drying, the rate decreases. The point terminating the constant rate period is
called critical point or critical moisture content. It is defined as average moisture content of
the material and the transition between two periods.
PROJECT OBJECTIVES
To fabricate a tray dryer.
To study and compare drying kinetics of the sample.
To calculate and compare the theoretical time required for drying with the actual time
required.
To calculate the efficiency of the fabricated dryer.
CHAPTER 2: -
LITERATURE REVIEW
1. Faculty of engineering caritas university, amorji nike, emne, enugu state, Okoye
clara ogechukwu,he studied and designed a corn and cob tray dryer. The main
objective was to design a corn dryer for the farmers of particular region thus
protecting its quality and spoilage of corn. The study provided them a high rate of
drying which was further used for forming a design data.
Eleven out of the twelve sensors used in the electronic nose system indicated flavour
degradation of all dried samples compared with the fresh tomatoes. The values of the
hue angles recorded for the dried tomatoes ranged between 51.81o and 61.95o,
revealing that the dried tomatoes were yellow hued, thus indicating less browning.
The drying characteristics curves were evaluated against the Page, Henderson and
Pabis, and the Logarithmic mathematical models but the Page model best described
the drying of tomato slices. The effective moisture diffusivity coefficient increased
with increasing drying temperature and was found to be 5.13×10-10 m2s-1, 6.45×10-
10
m2s-1, 8.44×10-10 m2s-1, and 10.26 ×10-10 m2s-1 at respective hot air temperatures of
50, 60, 70, and 80oC with activation energy for moisture removal of 22.28 KJ/mol.
8. Sana Ben Mariem, Salah Ben Mabrouk et.al......studied convective drying kinetics of
tomato slices was conducted in order to identify the characteristic parameters of such
high moisture content product and to establish mathematical models of the drying
kinetic for various range of temperatures typically encountered in industrial dryers.
The results allow the calculation of the effective diffusivity and the activation energy.
Drying experiments were conducted in Thermal Process Laboratory of the Research
and Technology Centre of Energy. The drying characteristics of tomato were studied
at 38°C, 44°C, 52°C, 57°C and 64°C with three air flow rates of 1ms-1, 2ms-1 and
3ms-1. The drying continues until samples' mass reaches a final moisture content of
11%. Some different mathematical models available in the literature (Newton, Page,
Henderson and Pabis, Two-term, modified Wang and Singh, Logarithmic ...) were
used and compared to estimate drying curves of tomatoes. The results indicated that to
reach a final moisture content of 11% at 38°C, 44°C, 50°C, 57°C and 64°C, the
drying time for 1 m/s, respectively, was 22.4h, 18.5h, 16.7h, 13.5h and 9.9h. For an
air flow rate of 1ms-1, 2ms-1 and 3ms-1, the drying time of tomato slices at 50°C were
16.7h, 14.2h and 11.7h, respectively. The effective diffusivity and activation energy
varied from in the temperature range (38°C - 64°C). Out of the considered
mathematical models, the drying curves were fitted to Logarithmic and Two-Term
equation.
CHAPTER 3: -
METHODOLGY
1. Fabrication procedure.
2. Experimental procedure.
FABRICATION PROCEDURE
The fabrication procedure provides the information about the dimensions, materials used and
specification required for fabrication of experimental setup.
1. Dryer: -
The body of the dryer is made-up of iron sheets of height 60cm and breadth
45 and 38cm. The frame of the dryer consists of 2mm thickness angle rod 40cm length which
is welded to the square pipes and 60cm distance i.e. along the height. The support for trays is
situated at 19cm and 36cm from the base.
The converging section that connects the body and chimney is made up of
metal sheet of 2mm of thickness and converging angle is 40 to 50O.
The chimney is made up of metal sheet of 2mm of thickness, the length and
breadth of the chimney is 13.5 cm and height is 11cm. One end of the chimney this joint to
the converging section.
The inner surface of the whole dryer is insulated by two layers 20mm thick
thermocol. The door is of dimensions 60*45cm and is made up of the same material that of
dryer body. The door is provided with two locks that completely seal the dryer.
For mobility of the dryer 4 wheels are attached to the base on the corners
with the help of screws, the height of the wheels is 7.5cm thus increasing the height of dryer
and making it to a total of 100cm height.
Fig 1: - Drying Section
2. Heater Box: -
Heater box is the box consisting the heating element (nichrome
coil) fixed on a hot plate made from clay. The power rating of heating coil is 1500W. The
diameter of the heating plate is 17.8cm.
5. Blower: -
The properties of blower are as follows
Power 500W
Speed of impeller 13000 rpm
Air flow rate 0.88m3/min
Material of construction HDPE
Fig 4: - Blower
EXPERIMENTAL SETUP
0.25
0.2
Rate of drying
0.15
Rate of drying
0.1
0.05
0
0 0.04 0.22 0.89 1.33 2.67 4.76 5.98 7.26
Average moisture content
Fig 6: - Drying rate vs average moisture content for tomato at temperature 80OC
Result: -
1. Critical moisture content (Xc) =4.76
2. Equilibrium moisture content (Xe) =0.04
3. Time required for drying (experimental) =7200 seconds
2. FOR POTATO AT TEMP. 80OC
0.18
0.16
0.14
0.12
Drying Rtae
0.1
0.06
0.04
0.02
0
0 0.01 0.06 0.17 0.48 0.69 0.95 1.24 1.36
Fig 7: - Drying rate vs average moisture content for potato at temperature 80OC
Result:-
1. Critical moisture content (Xc)= 0.48
2. Equilibrium moisture content(Xe)= 0.01
3. Time required for drying (experimental)= 6600 seconds
CHAPTER 5: -
KINETICS OF DRYING
Moisture content versus time graphs shows that moisture content decreases with increase in
time period for different temperatures of 60, 70 and 80°C. The figure portraits a negative
slope behavior at beginning and constant behavior later on where it is concluded that
moisture content could not be removed (bound moisture) further with increase in time period.
1.2
0.8
0.2
0
600
4800
time
1200
1800
2400
3000
3600
4200
5400
6000
6600
7200
0
1.2
0.8
0.4
0.2
0
time 0 600 1200 1800 2400
0.8
0.4
0.2
0
time 0 600 1200 1800 2400
From the above graphs it is observed that a smooth curve is obtained when tomato is
being dried giving a steady reduction in moisture. While in case of potato sudden
minor fluctuations are observed in each curve due to presence of more bound
moisture.
CHAPTER 6: -
RESULTS AND DISCUSSION
Where,
T= 4166 seconds
𝑇ℎ𝑒𝑜𝑟𝑒𝑡𝑖𝑐𝑎𝑙 𝑡𝑖𝑚𝑒 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑑
Efficiency of Dryer = × 100
𝐸𝑥𝑝𝑒𝑟𝑖𝑚𝑒𝑛𝑡𝑎𝑙𝑙𝑦 𝑡𝑖𝑚𝑒 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑑
4166
= × 100
7200
= 57.86%
Calculation of theoretical time for Potato at 80OC
T = 3644 + 1112
T = 4757 seconds
𝑇ℎ𝑒𝑜𝑟𝑒𝑡𝑖𝑐𝑎𝑙 𝑡𝑖𝑚𝑒 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑑
Efficiency of Dryer = × 100
𝐸𝑥𝑝𝑒𝑟𝑖𝑚𝑒𝑛𝑡𝑎𝑙𝑙𝑦 𝑡𝑖𝑚𝑒 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑑
4757
= 6600 × 100
= 72.07%
DRIED PRODUCT
a. Dried potato at temp. 80OC
Fig 11
DISCUSSION
o As per efficiencies calculated above it is observed that the dryer fabricated by
us gives more efficiency in case of potato compared with tomato.
o The graphical representation of drying rate versus average moisture content is
more stable in case of tomato.
o Kinetic data curves of drying of each temperature are approximately overlap
each other.
CHAPTER 7: -
CONCLUSION
Hence we conclude that the dryer fabricated by us gives optimal efficiency that is 50-
70%. We successfully completed experimental runs at varying temperatures that are
60, 70 and 80 degree centigrade at fixed flow rate of air and at regular time interval.
This project helped us to know about drying kinetics and how they can be
implemented. It also helped us to acquire thorough knowledge about the drying
period, time required for drying i.e. theoretically and experimentally.
We also compared the drying kinetics of the sample at various temperatures. There
are also some fluctuations observed during drying of potatoes due to presence more
bound moisture which is difficult to remove. The drying rate decreases with decrease
in moisture content due to absence of free or unbound moisture. Dried tomato is of
less weight compared to dried potatoes due to more moisture in it.
REFERENCES
1. Design and development of corn cob try dryers BY Okoye clara ogechukwu
4. Unit operations of chemical engineering Warren McCabe, Julin Smith and Peter
Harriot
7. Influence of Air Temperature on the Drying Kinetics and Quality of Tomato Slices by
Abano E. E1, Ma. H1, and W. Qu.
11.