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A PROJECT REPORT
Submitted by
LOGESH. R (2016110016)
of
BACHELOR OF ENGINEERING
in
MATERIALS SCIENCE AND ENGINEERING
NOVEMBER 2019
ANNA UNIVERSITY: CHENNAI 600 025
BONAFIDE CERTIFICATE
Professor
was studied using experimental analysis, involving the use of Ball Dot Impact
Testing Machine. Two different types of skin materials were used, namely E-
glass fibres and Basalt fibres. The effect of introduction of Non-Newtonian fluid
Experimental Analysis showed that the composites with basalt fibre skin
with E-Glass fibre skin. It was also found that the composites with Non-
of sandwich composites.
TABLE OF CONTENTS
1 Introduction 1
1.1 General 1
1.2 Sandwich Composites 2
1.2.1 Structure of a Sandwich Composite 2
1.2.2 Applications 2
1.3 Composites in the Aviation Industry 3
1.3.1 Materials used as skins 4
1.3.1.1 Basalt Fibers 4
1.3.1.2 E-Glass Fibers 6
1.3.2 Core Materials 9
1.3.2.1 H-130 PVC Foam 9
1.3.3 Adhesives used 10
1.4 Non-Newtonian Fluid - Dilatant 11
1.5 Problems Identified 12
1.6 Impact of the problem 12
1.7 Objectives of the Study 13
2 Literature Survey 14
3 Experimental Procedure 17
3.1 Materials 17
3.2 Foam Cutting and Drilling 17
3.3 Introduction of Non-Newtonian Fluid 18
3.3.1 Method of Preparation 18
3.3.2 Method of Reinforcing the Fluid 19
3.4 Fabrication Processes 19
3.4.1 Hand Lay-up 19
3.4.1.1 Issues faced in the fabricated Samples 20
3.4.2 Vacuum Bag Moulding 20
4 Impact Testing 23
4.1 Ball Dot Impact Tester 23
5 Experimental Results and Analysis 25
5.1 Sample 1 25
5.2 Sample 2 26
5.3 Sample 3 27
5.4 Sample 4 28
5.5 Results and Interpretation 29
6 Conclusion 29
7 References 30
LIST OF TABLES
1.1 GENERAL
Composite materials are being extensively used in the aviation industry. Bird
Strike events, highly prevalent in the aviation industry, causes not only
catastrophic damage, but also causes significant downtime of an aircraft due to
maintenance, during which the damaged part has to be repaired or even replaced
as a whole. Bird impact on a vulnerable component, such as an engine or
windscreen, can result in serious damage to the aircraft and even loss of life.
Aircraft components are also liable to be hit by hail stones during heavy rains.
Severe convection weather such as hail has long been the potential threat to the
safety of aircraft. Even a short while passing through the hailstone regions, it is
sufficient to cause damage to aircraft structure such as depression, cracking and
even piercing if crushed with hailstone at a high speed.
The impact may not be visible from outside i.e. the fuselage may seem
unaffected, but the inner packaging of sandwich composite structures would be
severely damaged. The current crops of Commercialised composites such as
Glass Fibre Composite and Carbon Fibre Composite may well result in BARELY
VISIBLE IMPACT DAMAGE and eventually, delamination of the structure.
So, the materials used for inner packaging (Sandwich composites) should be
designed in such a way that it withstands High and Low velocity impacts without
causing BVID so as to increase the reliability and Life span of the Aircraft.
Thus, the aim of this experiment is to analyse and study the impact
behaviours of H-130 PVC Foam based Sandwich composites, when subjected to
events such as a bird strike, hailstorm or other low velocity impacts and their
potential in replacing the existing composite structures. Sandwich Composites
are highly preferred due to their High Strength to Weight ratio and structural
versatility.
1.2 SANDWICH COMPOSITES
The skin layers are usually two thin and stiff layers, which are attached on both
sides of a thick, light-weight core material. Both the skin and core are bonded to
each other using an adhesive or bonding material.
1.2.2 Applications
Sandwich composite panels are being widely used in various fields such as:
• Carbon Fibres
• Kevlar/Aramid fibres
• Glass Fibres
• Basalt fibres, etc.
3. Low cost alternative and can replace carbon fiber in some applications
including filament winding
10. Compatible with many resins - unsaturated polyester, vinyl ester, epoxy,
phenolic, etc.
Property Value
E-Glass or electrical grade glass was originally developed for stand off
insulators for electrical wiring. It was later found to have excellent fibre forming
capabilities and is now used almost exclusively as the reinforcing phase in the
material commonly known as fibreglass.
Properties that have made E-glass so popular in fibreglass and other glass
fibre reinforced composite include:
• Low cost
• Non-flammable
• Resistant to heat
Composition: 54%SiO2-15%Al2O3-12%CaO
Both Open- and Closed-cell Structured foams and metal foams are used as
Core materials.
• Polyethersulfone foam
• Polyethylene foam
• Polyvinylchloride foam
• Polyurethane foam
• Polystyrene foam
• Syntactic foam
• Balsa wood
• Honeycombs etc.
PVC foams came into use as core materials in the 70’s. It is a rigid, light weight
and moisture resistant foam with a closed cell structure. Technically, it is an
Interpenetrating Polymer Network (IPN) of PVC and polyurea. The interaction
of these polymers gives the foam its unique characteristics.
PVC foams are available in a variety of densities from 45 kg/m 3 to 400 kg/m3.
Among them, the foam used for this study is H-130 PVC Foam, having a density
of 130 kg/m3.
Table 3: Properties of PVC Foams
• Epoxy resin
• Polyurethane resin
• Acrylic adhesive
• Contact Cement
• Resorcinol
• Polyvinyl Acetate (PVA)
1.4 NON-NEWTONIAN FLUID - DILATANT
PROPERTY VALUE
• Aircrafts are always subjected to Bird Strike during take-off and landing,
which is one the potential problem faced by the aviation industry.
• In US alone, it has been reported that more than 1,56,114 Bird Strikes has
caused 1,72,151 hours of downtime and $208 million losses.
• Due to this, the composite structures currently used (those made from
Carbon, Glass and Kevlar fibres) are more prone to BVID (Barely Visible
Impact Damage)
✓ The Paper inferred that PVC Foam core was less affected by the
adverse environments
✓ It was also found that there was a significant decrease in the
strength of interfacial layers between the core and the skin.
• “Effect of graphene nano-pellets on the mechanical properties of
Basalt/epoxy composites” by Mehmet Bulut et.al
The Dilatant was prepared by mixing Corn Flour with Distilled Water at a ratio
of 3:1. The mixture was subjected to continuous stirring and should be maintained
at room temperature. After some time, the required consistency of Dilatant was
achieved and they were transferred to the holes drilled in the Foam. When left
undisturbed for a long time, it gets hardened.
The prepared non-Newtonian Fluid was then reinforced into the drilled holes
manually by sealing one end of the hole, using a sealant tape. After the dilatant
hardens, the tape is removed. The foam is then used for fabrication of the desired
sandwich composite.
Hand lay-up is the most common and least expensive open-molding method
because it requires the least amount of equipment. Fibre reinforcements are
placed by hand in a mold and resin is applied with a brush or roller.
This process is used to make both large and small items, including boats, storage
tanks, tubs and showers.
• Partial Curing
• Low Adhesiveness of Epoxy
Resin
• Distortedness of Fibres in the
composite
• Overflow of Resin in the Setup
• Porosity in the Structure
Figure 8: Sandwich
• Low Impact Resistance Composite Fabricated using
Hand Lay-up process
The ball-dot impact test is used for determining the impact resistance of
composites and various other materials (e. g. susceptibility to breaking and
cracking), using a chrome plated steel ball. The ball is made to fall on the mounted
specimen at different heights. The impact behaviour of the specimen is then
analysed using the test results.
TEST CONDITIONS:
5.1 SAMPLE 1:
SAMPLE DETAILS:
Designation: EG 1
Core Material: H130 PVC Foam
Skin: E-Glass (Bidirectional) x 3
P.E: Range of 5J to 15J
Designation: EG 2
Core Material: H130 PVC Foam
Skin: E-Glass (Bidirectional) x 3
Reinforcement: Non-Newtonian Fluid
P.E: Range of 5J to 15J
Designation: BS 1
Core Material: H130 PVC Foam
Skin: Basalt (Bidirectional) x 3
P.E: Range of 5J to 15J
Designation: BS 2
Core Material: H130 PVC Foam
Skin: Basalt (Bidirectional) x 3
Reinforcement: Non-Newtonian Fluid
P.E: Range of 5J to 15J
➢ For the sample BS-1 (Basalt fibre – PVC foam based sandwich composite),
bulging and crack initiation started at the drop height of 1000 mm itself.
➢ The impact resistance was maximum for the Basalt fibre – PVC foam based
sandwich composite with a reinforcement of non-Newtonian fluid (BS-2).
➢ But the effect is maximum for the Basalt fibre based composites.
CONCLUSION:
• The H-130 PVC Foam-Basalt Fibre with non-Newtonian Fluid
reinforcement based sandwich composites so fabricated showed a greater
resistance to the impact loads than the other Basalt and E-Glass based
composites.
REFERENCES
• Journal on “Advanced body armour utilizing shear thickening fluids”,
by Y. S. Lee , E. D. Wetzel, R.G. Egres Jr and N.J. Wagner (2002)