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The purpose of this lab is to obtain a sample of ethyl acetate (ethyl ethanoate) by
mixing and distilling samples of ethanol and acetic acid with sulfuric acid as a catalyst.
Procedure:
2. Measured out and mixed 10.2 mL of ethanol and 11.8 mL of acetic acid in a
\f 5. Too much heat was added to the hot water bath, and the container with the
Erlenmeyer flask.
9. Waited 15 minutes after the boiling of the solution, and then poured the
10. Turned the cold water (which was connected to the condenser) on.
11. Heated the distilling flask with the Bunsen burner at a controlled temperature
12. Prepared a solution of 1.5 g Na CQ and 5.0 mL of distilled water and shook
2 3
well.
13. Poured liquid solution into a separatory funnel and added the distillate from
Figure 1
Calculations:
Beaker with Ethyl Acetate (239.9 g.) - Empty Beaker (228.6 g.) = Amount of Ethyl
Acetate (11.3 g.)
Percent Error
Conclusion
Overall our lab went accident free except for the beaker of water breaking at the
beginning. We restarted the lab afterwards and everything seemed to be working fine.
All of our pipes and hosing were tight, and we did not have any leaks that were evident.
We did have to wait a day to separate the solution which then had precipitates form and
we think that letting it sit might have thrown off how much Ethyl Acetate we actually
Part I :
Name of
Ethanol Sulfuric Acid Acetic Acid
Compound
Amount of 12 mL
9.0 mL 15 drops
Compound
Part I I :
Observations: Heated flask for 15 minutes not exceeding 85°C. Compounds, after
being combined, smelled like nail polish remover.
Part I I I :
Observations: Smelled like nail polish remover. The total weight of the Ethyl Acetate
was 11.3g. , H