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This document contains 16 questions related to analyzing coal samples. The questions involve calculating various properties of coal such as calorific value, percentage composition of carbon, hydrogen, nitrogen, sulfur, and ash content using data from experiments like bomb calorimetry and Kjeldahl analysis.
This document contains 16 questions related to analyzing coal samples. The questions involve calculating various properties of coal such as calorific value, percentage composition of carbon, hydrogen, nitrogen, sulfur, and ash content using data from experiments like bomb calorimetry and Kjeldahl analysis.
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Attribution Non-Commercial (BY-NC)
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This document contains 16 questions related to analyzing coal samples. The questions involve calculating various properties of coal such as calorific value, percentage composition of carbon, hydrogen, nitrogen, sulfur, and ash content using data from experiments like bomb calorimetry and Kjeldahl analysis.
Copyright:
Attribution Non-Commercial (BY-NC)
Formati disponibili
Scarica in formato PDF, TXT o leggi online su Scribd
SCHOOL OF ENGINEERING AND TECHNOLOGY, crucible was then heated without cover, until a constant weight was obtained.
ithout cover, until a constant weight was obtained. The residue
SHARDA UNIVERSITY was found to weigh .21 g. Calculate the percentage of fixed carbon. 6. 3.00 g of coal sample was kjeldahlised and NH3 gas evolved was absorbed in 40 ml of INDUSTRIAL CHEMISTRY (ME-A&B) N/10 H2SO4. After absorption, the excess(residual)acid required 10 ml of N/10 NaOH for ASSIGNMENT 1 exact neutralization. Calculate the percentage of nitrogen in the coal sample. DATE: 10-09-2010 7. 0.20 g of a coal sample on combustion produces 0.40 g of CO2 and 0.18 g of water. SUBMISSION DATE: 16-09-2010 Calculate the %C and %H. 8. 0.8 g of a coal sample was burnt completely in a bomb calorimeter. The washing was 1. A sample of coal: C= 93%, H= 6%, ash = 1%. The following data were obtained when then heated with BaCl2 and precipitated as as BaSO4. The precipitates were then filtered, the coal was tested in a bomb calorimeter: dried and weighed as 0.08 g. calculate the % of Sulphur in fuel. Weight of the coal burnt = 0.92 g 9. 1.8 g of coal was weighed in a silica crucible. After heating for one hr. at 110°C, the residue was weighed 1.680 g. The crucible next was then covered by vented lid and was Weight of water taken = 550g strongly heated for exactly 7 min. at 950±50°C. The residue was weighed 0.910 g. the Water equivalent of bomb and calorimeter = 2,200 g crucible was then heated without cover, until a constant weight was obtained. The residue Rise in temperature = 2.42ºC was found to weigh .250 g. determine the ash, moisture, volatile matter and fixed carbon Fuse wire correction = 10.0 cal in the coal sample. Acid correction = 50.0 cal 10. 1.0 g of a coal sample was burnt completely in a bomb calorimeter. The calorific Calculate the gross and net calorific value of coal, assuming the latent heat of value of the fuel aws 8600 cal/g. The washing was then heated with BaCl2 and condensation of steam is 580 cal/g. precipitated as as BaSO4. The precipitates were then filtered, dried and weighed as 0.1 g. 2. The following data is obtained in bomb calorimeter experiment: calculate the % of Sulphur in fuel. Weight of the crucible = 3.649 g 11. 1.00 g of coal sample was kjeldahlised and NH 3 gas evolved was absorbed in 50 ml of Weight of the crucible+ fuel = 4.678 g N/10 H2SO4. After absorption, the excess (residual) acid required 15 ml of N/10 NaOH Weight of water taken = 2200 g for exact neutralization. Calculate the percentage of nitrogen in the coal sample. Water equivalent of bomb and calorimeter= 570 g 12. A sample of coal containing C, H, N, S and O was analysed as follows: Rise in temperature = 2.3ºC (i) 0.24 g of the sample on combustion gave 0.792 g of CO2 and 0.216 g of H20. Fuse wire correction = 3.8 cal (ii) 1.4 g of the sample was Kjeldahlised and the ammonia liberated was absorbed in 50.0 Acid correction = 62.6 cal ml of N/l0 H 2S04, The resultant solution required 10.0 ml of N/10 NaOH for complete Cooling correction = 0.0047ºC neutralisation. Cotton thread correction = 1.6 cal (iii) 3.2 g of the sample was analysed by for sulphur analysis and gave 0.233 g of BaS04. Calculate the gross and net calorific value of the fuel sample. The fuel contains 6.5% Find the percentage of C, H, N, S and O in the coal. hydrogen. Assuming the latent heat of condensation of steam is 580 cal/g. 13. 2.5 g of a coal sample was taken in a silica crucible weighing 19.35 g. After heating 3. 0.72 g of fuel containing 80% carbon, when burnt in a bomb calorimeter, increased in an electric oven at 105· 110°C for 1 hour, the crucible weighed 21. 765 g. The residue the temperature of water from 27.3ºC to 29.1º C. If the calorimeter contains 250 g of was then ignited at 700· 750°C to a constant weight when the crucible weighed 19.595 g. water and its water equivalent is 150 g, Calculate the HCV of the fuel in KJ/kg. (ii) In another experiment, 2.5 g of the same sample was heated in a platinum crucible (weighing 19.345 g), Covered with a vented lid, at a temperature at 950 ± 20°C for 4. A sample of coal: C= 90%, H= 8%, ash = 2%. The following data were obtained when exactly 7 minutes. After cooling, the crucible weighed 20.873 g. the coal was tested in a bomb calorimeter: (iii) Calculate the percentage of fixed carbon. Weight of the coal burnt = 0.90 g 14. A sample of coal contains C = 61%, O = 32%, H = 6%, S = 0.5%, N = 0.2% and ash = 0.3%. Calculate the GCV and NCV by Dulong – Petit’s formula. Weight of water taken = 800 g 15. A sample of coal was analysed for content of moisture, volatile matter and ash. From Water equivalent of bomb and calorimeter = 2,000 g the following data calculate the percentages of the above quantities. Rise in temperature = 2.4ºC (i) Weight of coal taken = 3.0 gm Fuse wire correction = 10.0 cal (ii) Weight of coal taken after heating to 100oC = 2.761 gm (iii)Weight of coal after heating the covered crucible at 950 ± 20oC = 2.125 gm Acid correction = 60.0 cal (iv) Constant weight obtained at the end of the experiment = 0.357 gm Calculate the gross and net calorific value of coal, assuming the latent heat of 16. By Kjeldahl’s method, 2.75 g of coal was analysed, The NH3 evolved was absorbed condensation of steam is 587 cal/g. in 50 ml of 0.05N H 2SO4. After absorption the excess acid required 10.25 ml of 0.05 N NaOH for exact neutralization. 2.5 g of the same coal sample in qualitative analysis gave 5. A coal sample was analyzed as follows: 0.2651 g of BaSO4. Calculate the percentage of N and S. Exactly 1.4 g of coal was weighed in a silica crucible. After heating for one hr. at 110- 115°C, the residue was weighed 1.0 g. The crucible next was covered by vented lid and was strongly heated for exactly 7 min. at 950±50°C. The residue was weighed 1.00 g. the Ms. Geeta Durga
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