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REFERENCE STANDARD
CALDIE CALDIE
ASSAB 88 SLEIPNER
NIMAX NIMAX
UNIMAX UNIMAX
CORRAX CORRAX
STAVAX ESR STAVAX ESR 420 Mod. 1.2083 ESR SUS 420J2
POLMAX POLMAX
ROYALLOY ROYALLOY
PRODAX
ASSAB MM40
ASSAB 8407 SUPREME ORVAR SUPREME H13 Premium 1.2344 ESR SKD 61
DIEVAR DIEVAR
HOTVAR HOTVAR
Edition D140715
2
ASSAB 8407 SUPREME
General Applications
ASSAB 8407 Supreme is a chromium-molybdenum- DIE CASTING
vanadium alloyed tool steel which is characterised by:
Tin, lead Aluminium
Part zinc alloys magnesium
High level of resistance to thermal shock and HRC alloys, HRC
thermal fatigue Dies 46-50 42-48
Good high-temperature strength Fixed inserts, cores 46-52 44-48
Excellent toughness and ductility in all
Sprue parts 48-52 46-48
directions
Good machinability and polishability Nozzles 35-42 42-48
Excellent through-hardening properties Ejector pins (nitrided) 46-50 46-50
Good dimensional stability during hardening Plunger, short-sleeve
(normally nitrided) 42-46 42-48
Austenitising 1020–
1040–1050°C
temperature 1030°C
HOT PRESSING
Material Aust. temp. HRC
Aluminium,
1020-1030°C 44-52
magnesium alloys
PLASTIC MOULDING
Part Aust. and tempering temp. HRC
IMPROVED TOOLING PERFORMANCE Injection moulds
Austenitising 1020-1030°C
Compression/ 50-52
Tempering 250°C
The name “SUPREME” implies that by special processing transfer moulds
techniques and close control, the steel attains high
purity and a very fine structure. Further, ASSAB 8407
Supreme shows significant improvements in isotropic OTHER APPLICATIONS
properties compared to conventionally produced AISI
Application Aust. and tempering temp. HRC
H13 grades.
Severe cold
Austenitising 1020-1030°C
These improved isotropic properties are particularly punching, 50-52
Tempering 250°C
scrap shears
valuable for tooling subjected to high mechanical and
thermal fatigue stresses, e.g., die casting dies, forging tools Austenitising 1020-1030°C
and extrusion tooling. In practical terms, tools may be Hot Shearing Tempering 250°C 50-52
used at somewhat higher working hardnesses (+1 to 2 Tempering 575-600°C 45-50
HRC) without loss of toughness. Since increased hardness Shrink rings
slows down the formation of heat checking cracks, Austenitising 1020-1030°C
(e.g., for cemented 45-50
Tempering 575-600°C
improved tool performance can be expected. carbide dies)
3
ASSAB 8407 SUPREME
Properties
All specimens are taken from the centre of a 407 x 127 Effect of time at high temperatures on hardness
mm bar. Unless otherwise indicated, all specimens were
hardened 30 minutes at 1025°C, quenched in air and
Hardness, HRC
tempered 2 + 2 h at 610°C to 45 ± 1 HRC.
50
45
PHYSICAL DATA
500°C
Hardened and tempered to 44-46 HRC.
40
Density 600°C
7800 7700 7600
kg/m3 30
Modulus of elasticity
210 000 180 000 140 000
MPa 25
Coefficient of 650°C
thermal expansion - 12.6 x 10 -6 13.2 x 10 -6
20
per °C from 20°C
1 10 100 1000
Thermal Time, h
conductivity 25 29 30
W/m °C
MECHANICAL PROPERTIES
Impact energy, J
Approximate tensile strength at room temperature.
100
20
Approximate strength at elevated temperatures
Longitudinal direction. 0
100 200 300 400 500ºC
Testing temperature
Rm, Rp0.2 A5, Z
MPa %
2000 100
1800 Z 90
1600 80
1400 70
1200 60
Rm
1000 50
800 40
600 Rp0.2 30
400 20
200 A5 10
0
100 200 300 400 500 600 700ºC
Testing temperature
4
ASSAB 8407 SUPREME
Heat treatment
SOFT ANNEALING Hardness, grain size and retained austenite as
functions of austenitising temperature
Protect the steel and heat through to 850°C. Then cool
in the furnace at 10°C per hour to 650°C, then freely in air. Grain
Size
ASTM Hardness, HRC Retained austenite, %
60
Grain size
10 58
STRESS RELIEVING
56
After rough machining, the tool should be heated 8 Hardness
54
through to 650°C, holding time 2 hours. Cool slowly
to 500°C, then freely in air. 6
52
4 50
48
46 Retained austenite 6
HARDENING
Soaking time = time at hardening temperature after the The lowest tempering temperature which should be
tool is fully heated through. used is 250°C. The minimum holding time at tempering
temperature is 2 hours. To avoid “temper brittleness”,
Protect the tool against decarburisation and oxidation during do not temper in the range 425–550°C, see graph.
hardening.
Tempering graph
Hardness, HRC Retained austenite, %
60
Austenitising temp.
QUENCHING MEDIA
1050°C
55
High speed gas/circulating atmosphere
Vacuum (high speed gas with sufficient positive
50 1020°C
pressure). Interrupted quench is recommended for 1025°C
distortion control, or when quench cracking is a Temper brittleness zone
concern.
45
Martempering bath or fluidised bed at 450–550°C,
then cool in air
Martempering bath or fluidised bed at approx. 40 6
180–220°C, then cool in air Retained austenite
Warm oil
35 4
Note 1: Temper the tool as soon as its temperature
reaches 50–70°C.
30 2
Note 2: In order to obtain the optimum properties for
the tool, the cooling rate should be fast, but not at a
level that gives excessive distortion or cracks. 25
100 200 300 400 500 600 700ºC
Tempering temperature (2h + 2h)
5
ASSAB 8407 SUPREME
80
Air hardened Min. -0.02 -0.05 ±0
from 1020°C Max. +0.03 +0.02 +0.05
60
Temper brittleness zone Vacuum hardened Min. +0.01 -0.02 +0.08
from 1020°C Max. +0.02 -0.04 +0.12
40
20
DIMENSIONAL CHANGES DURING TEMPERING
Dimensional change, %
100 200 300 400 500 600ºC + 0.12
Tempering temperature (2h + 2h) + 0.08
+ 0.04
Tempering within the range 425–550°C is normally
not recommended due to the reduction in toughness 0
properties. - 0.04
- 0.08
- 0.12
100 200 300 400 500 600 700 ºC
Tempering temperature (1h + 1h)
CCT graph
Austenitising temperature 1025°C. Holding time 30 minutes.
°C
1100
Austenitising temperature 1025ºC
Holding time 30 minutes
1000
AC = 940ºC
3
900
AC = 840ºC
800 1
Pearlite
700 Carbides
600
400 1 707 1
Bainite 2 673 6
MS 3 613 105
300
4 613 316
5 599 527
200 6 592 1054
7 560 2772
Martensite
100 8 519 5271
9 483 7944
Mf 1 2 3 4 5 6 7 8 9 10 10 222 20768
1 10 100 Hours
6
ASSAB 8407 SUPREME
Machining recommendations
The cutting data below are to be considered as guiding MILLING
values and as starting points for developing your own
best practice. Face and square shoulder milling
P10
Carbide P20 - P30
Coated
designation Coated
carbide or
- End milling
ISO carbide
cermet
†
High speed steel Type of milling
Cutting data
parameters Carbide
Solid High speed
indexable
DRILLING carbide steel
insert
* For coated HSS drill, vc~ 28–30 m/min 1 For coated HSS end mill, vc~ 55–60 m/min
2 Depending on radial depth of cut and cutter diameter
GRINDING
Carbide drill
Wheel recommendation
7
ASSAB 8407 SUPREME
Preheating
325 - 375ºC 325 - 375ºC
Depth of nitriding temp.1
Maximum
Gas nitriding at 10 0.12 interpass 475°C 475°C
510°C 30 0.20 temp.2
Plasma nitriding 10 0.12 Cooling 20 - 40ºC/h for the first 2 to 3 hours and
at 480°C 30 0.18 rate then freely in air
Nitrocarburising Hardness
– in gas at 2.5 0.11 after 50 - 55 HRC 50 - 55 HRC
580°C welding
– in salt bath at 30 0.06
580°C
Heat treatment after welding
*
Depth of case = distance from surface where hardness is 50 HV0.2 over base
hardness Hardened Temper at 25°C below the original
condition tempering temperature.
Nitriding to case depths >0.3 mm is not recommended
for hot work applications. 8407 Supreme can be nitrided Soft anneal the material at 850°C
Soft
in the soft annealed condition. The hardness and depth in protected atmosphere.
annealed
Then cool in the furnace at 10°C per hour
of case will, however, be reduced somewhat in this case. condition
to 650°C, then freely in air.
8
ASSAB 8407 SUPREME
Polishing Photo-etching
ASSAB 8407 Supreme exhibits good polishability in the ASSAB 8407 Supreme is particularly suitable for
hardened and tempered condition. Polishing after grinding texturing by the photo-etching method. Its high level of
can be effected using aluminium oxide or diamond paste. homogeneity and low sulphur content ensure accurate
and consistent pattern reproduction.
TYPICAL PROCEDURE
1. Rough grinding to 180–320 grain size using a wheel
The ESR Tool Steel Process
or stone.
The starting material for our tool steel is carefully
2. Fine grinding with abrasive paper or powder, down to
selected from high-quality recyclable steel.
400–800 grain size.
Together with ferroalloys and slag formers, the
3. Polish with diamond paste grade 15 (15µm grain size) recyclable steel is melted in an electric arc furnace.
using a polishing tool of soft wood or fibre. The molten steel is then tapped into a ladle.
4. Polish with diamond paste 8–6–3 (8–6–3µm grain
size) using a polishing tool of soft wood or fibre. The deslagging unit removes oxygen-rich slag.
5. When demands on surface finish are high, grade 1
Then deoxidation, alloying and heating of the steel
bath are carried out in the ladle furnace. Vacuum
(1µm grain size) diamond paste can be used for final
degassing removes elements such as hydrogen,
polishing with a fibre polishing pad.
nitrogen and sulphur.
ESR PLANT
In uphill casting, a controlled flow of molten steel
from the ladle filled the prepared moulds, and
solidfies into ingots.
Subsequently, the steel can go directly to our
rolling mill or to the forging press. Our premium
steel grades go to our ESR furnace, where they
are melted once again in an electroslag remelting
process. This is done by melting a consumable
electrode immersed in an overheated slag bath.
Controlled solidification in the steel bath results
in an ingot of high homogeneity, thereby removing
marcrosegregation. Melting under a protective
atmosphere gives an even better steel clealiness.
HOT WORKING
From the ESR plant, the steel goes to the rolling
mill or to our forging press to be formed into round
or flat bars.
Prior to delivery, all bar materials are heat treated
to either soft-annealed condition, or hardened and
tempered condition.
9
ASSAB 8407 SUPREME
MACHINING
Further information
Before putting into stock, flat-bar profiles are
machined to the required size and exact tolerance. For further information, i.e., steel selection, heat
Whilst larger round dimensions are turned in lathe, treatment, application and availability, please contact our
where the steel bars rotate against a stationary ASSAB office nearest to you.
cutting tool. Peeling is performed on smaller round
dimensions via cutting tools that revolve the bars
for removal of surface defects.
To safeguard the quality and integrity of our
tool steels, we perform surface inspection and
ultrasonic testing on all bars. We then cut off and
discard the bar ends and any defects that are found
during inspection.
Coefficient
Temper Hot yield Creep Heat
ASSAB grade of thermal Ductility
resistance strength strength conductivity
expansion
ALVAR 14
ASSAB 8407 2M
ASSAB 8407 SUPREME
DIEVAR
HOTVAR
QRO 90 SUPREME
10
ASSAB 8407 SUPREME
Jiangxi*
ASSAB Tooling (Dong Guan)
Co, Ltd., Jiangxi Branch
Tel : +86 769 2289 7888
Fax : +86 769 2289 9312
info.jiangxi@assab.com
11
Choosing the right steel is of vital importance. ASSAB engineers
and metallurgists are always ready to assist you in your choice of
the optimum steel grade and the best treatment for each application.
ASSAB not only supplies steel products with superior quality, we offer
state-of-the-art machining, heat treatment and surface treatment
services to enhance steel properties to meet your requirement in
the shortest lead time. Using holistic approach as a one-stop solution
provider, we are more than just another tool steel supplier.