Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
910
that the comments contain significant ington, DC 20460. The telephone num
information not contained elsewhere in ber is 703–603–8760.
the administrative record file which (2) Products may be added to the
could not have been submitted during NCP Product Schedule by the process
the public comment period and which specified in § 300.920.
substantially support the need to sig (b) Hazardous Substance Releases. [Re-
nificantly alter the response action. served]
All such comments and any responses [59 FR 47453, Sept. 15, 1994, as amended at 65
thereto shall be placed in the adminis FR 47325, Aug. 2, 2000]
trative record file.
§ 300.910 Authorization of use.
Subpart J—Use of Dispersants and (a) RRTs and Area Committees shall
Other Chemicals address, as part of their planning ac
tivities, the desirability of using appro
SOURCE: 59 FR 47453, Sept. 15, 1994, unless
priate dispersants, surface washing
otherwise noted. agents, surface collecting agents, bio
remediation agents, or miscellaneous
§ 300.900 General. oil spill control agents listed on the
NCP Product Schedule, and the desir
(a) Section 311(d)(2)(G) of the CWA
ability of using appropriate burning
requires that EPA prepare a schedule agents. RCPs and ACPs shall, as appro
of dispersants, other chemicals, and priate, include applicable preauthoriza
other spill mitigating devices and sub- tion plans and address the specific con-
stances, if any, that may be used in texts in which such products should
carrying out the NCP. This subpart and should not be used. In meeting the
makes provisions for such a schedule. provisions of this paragraph, preautho
(b) This subpart applies to the navi rization plans may address factors such
gable waters of the United States and as the potential sources and types of
adjoining shorelines, the waters of the oil that might be spilled, the existence
contiguous zone, and the high seas be and location of environmentally sen
yond the contiguous zone in connection sitive resources that might be im
with activities under the Outer Conti pacted by spilled oil, available product
nental Shelf Lands Act, activities and storage locations, available equip
under the Deepwater Port Act of 1974, ment and adequately trained operators,
or activities that may affect natural and the available means to monitor
resources belonging to, appertaining product application and effectiveness.
to, or under the exclusive management The RRT representatives from EPA
authority of the United States, includ and the states with jurisdiction over
ing resources under the Magnuson the waters of the area to which a pre-
Fishery Conservation and Management authorization plan applies and the DOC
Act of 1976. and DOI natural resource trustees shall
(c) This subpart applies to the use of review and either approve, disapprove,
any chemical agents or other additives or approve with modification the pre-
as defined in subpart A of this part authorization plans developed by Area
that may be used to remove or control Committees, as appropriate. Approved
oil discharges. preauthorization plans shall be in
cluded in the appropriate RCPs and
§ 300.905 NCP Product Schedule. ACPs. If the RRT representatives from
(a) Oil Discharges. (1) EPA shall main EPA and the states with jurisdiction
tain a schedule of dispersants and over the waters of the area to which a
other chemical or bioremediation prod preauthorization plan applies and the
ucts that may be authorized for use on DOC and DOI natural resource trustees
oil discharges in accordance with the approve in advance the use of certain
procedures set forth in § 300.910. This products under specified circumstances
schedule, called the NCP Product as described in the preauthorization
Schedule, may be obtained from the plan, the OSC may authorize the use of
Emergency Response Division (5202–G), the products without obtaining the
U.S. Environmental Protection Agen specific concurrences described in para-
cy, 1200 Pennsylvania Ave., NW., Wash- graphs (b) and (c) of this section.
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(b) For spill situations that are not accordance with paragraphs (a), (b),
addressed by the preauthorization and (c) of this section.
plans developed pursuant to paragraph (e) Sinking agents shall not be au
(a) of this section, the OSC, with the thorized for application to oil dis
concurrence of the EPA representative charges.
to the RRT and, as appropriate, the (f) When developing preauthorization
concurrence of the RRT representa plans, RRTs may require the perform
tives from the states with jurisdiction ance of supplementary toxicity and ef
over the navigable waters threatened fectiveness testing of products, in addi
by the release or discharge, and in con tion to the test methods specified in
sultation with the DOC and DOI nat § 300.915 and described in appendix C to
ural resource trustees, when prac part 300, due to existing site-specific or
ticable, may authorize the use of area-specific concerns.
dispersants, surface washing agents,
surface collecting agents, bioremedi § 300.915 Data requirements.
ation agents, or miscellaneous oil spill (a) Dispersants. (1) Name, brand, or
control agents on the oil discharge, trademark, if any, under which the dis
provided that the products are listed persant is sold.
on the NCP Product Schedule. (2) Name, address, and telephone
(c) The OSC, with the concurrence of number of the manufacturer, importer,
the EPA representative to the RRT or vendor.
and, as appropriate, the concurrence of (3) Name, address, and telephone
the RRT representatives from the number of primary distributors or sales
states with jurisdiction over the navi outlets.
gable waters threatened by the release (4) Special handling and worker pre-
or discharge, and in consultation with cautions for storage and field applica
the DOC and DOI natural resource tion. Maximum and minimum storage
trustees, when practicable, may au temperatures, to include optimum
thorize the use of burning agents on a ranges as well as temperatures that
case-by-case basis. will cause phase separations, chemical
(d) The OSC may authorize the use of changes, or other alterations to the ef
any dispersant, surface washing agent, fectiveness of the product.
surface collecting agent, other chem (5) Shelf life.
ical agent, burning agent, bioremedi (6) Recommended application proce
ation agent, or miscellaneous oil spill dures, concentrations, and conditions
control agent, including products not for use depending upon water salinity,
listed on the NCP Product Schedule, water temperature, types and ages of
without obtaining the concurrence of the pollutants, and any other applica
the EPA representative to the RRT tion restrictions.
and, as appropriate, the RRT rep (7) Effectiveness. Use the Swirling
resentatives from the states with juris Flask effectiveness test methods de-
diction over the navigable waters scribed in appendix C to part 300. Man
threatened by the release or discharge, ufacturers shall submit test results and
when, in the judgment of the OSC, the supporting data, along with a certifi
use of the product is necessary to pre- cation signed by responsible corporate
vent or substantially reduce a hazard officials of the manufacturer and lab-
to human life. Whenever the OSC au oratory stating that the test was con
thorizes the use of a product pursuant ducted on a representative product
to this paragraph, the OSC is to inform sample, the testing was conducted
the EPA RRT representative and, as using generally accepted laboratory
appropriate, the RRT representatives practices, and they believe the results
from the affected states and, when to be accurate. A dispersant must at
practicable, the DOC/DOI natural re- tain an effectiveness value of 45 per-
sources trustees of the use of a prod cent or greater to be added to the NCP
uct, including products not on the Product Schedule. Manufacturers are
Schedule, as soon as possible. Once the encouraged to provide data on product
threat to human life has subsided, the performance under conditions other
continued use of a product shall be in than those captured by these tests.
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(8) Dispersant Toxicity. For those Liquids (and the Calculation of Dy
dispersants that meet the effectiveness namic Viscosity).’’
threshold described in paragraph (a)(7) (iv) Specific Gravity—Use ASTM—D
above, use the standard toxicity test 1298–85(90), ‘‘Standard Test Method for
methods described in appendix C to Density, Relative Density (Specific
part 300. Manufacturers shall submit Gravity), or API Gravity of Crude Pe
test results and supporting data, along troleum and Liquid Petroleum Prod
with a certification signed by respon ucts by Hydrometer Method.’’
sible corporate officials of the manu (v) pH—Use ASTM—D 1293–84(90),
facturer and laboratory stating that ‘‘Standard Test Methods for pH of
the test was conducted on a representa Water.’’
tive product sample, the testing was (10) Dispersing Agent Components.
conducted using generally accepted Itemize by chemical name and percent-
laboratory practices, and they believe age by weight each component of the
the results to be accurate. total formulation. The percentages will
(9) The following data requirements include maximum, minimum, and aver-
incorporate by reference standards age weights in order to reflect quality
from the 1991 or 1992 Annual Books of control variations in manufacture or
ASTM Standards. American Society formulation. In addition to the chem
for Testing and Materials, 1916 Race ical information provided in response
Street, Philadelphia, Pennsylvania to the first two sentences, identify the
19103. This incorporation by reference major components in at least the fol
was approved by the Director of the lowing categories: surface active
Federal Register in accordance with 5 agents, solvents, and additives.
U.S.C. 552(a) and 1 CFR part 51. 1 (11) Heavy Metals, Cyanide, and
(i) Flash Point—Select appropriate
Chlorinated Hydrocarbons. Using
method from the following:
standard test procedures, state the
(A) ASTM—D 56–87, ‘‘Standard Test
concentrations or upper limits of the
Method for Flash Point by Tag Closed
following materials:
Tester;’’
(B) ASTM—D 92–90, ‘‘Standard Test (i) Arsenic, cadmium, chromium,
Method for Flash and Fire Points by copper, lead, mercury, nickel, zinc,
Cleveland Open Cup;’’ plus any other metals that may be rea
(C) ASTM—D 93–90, ‘‘Standard Test sonably expected to be in the sample.
Methods for Flash Point by Pensky- Atomic absorption methods should be
Martens Closed Tester;’’ used and the detailed analytical meth
(D) ASTM—D 1310–86, ‘‘Standard Test ods and sample preparation shall be
Method for Flash Point and Fire Point fully described.
of Liquids by Tag Open-Cup Appa (ii) Cyanide. Standard calorimetric
ratus;’’ or procedures should be used.
(E) ASTM—D 3278–89, ‘‘Standard Test (iii) Chlorinated hydrocarbons. Gas
Methods for Flash Point of Liquids by chromatography should be used and
Setaflash Closed-Cup Apparatus.’’ the detailed analytical methods and
(ii) Pour Point—Use ASTM—D 97–87, sample preparation shall be fully de-
‘‘Standard Test Method for Pour Point scribed. At a minimum, the following
of Petroleum Oils.’’ test methods shall be used for
(iii) Viscosity—Use ASTM—D 445–88, chlorinated hydrocarbon analyses: EPA
‘‘Standard Test Method for Kinematic Method 601—Purgeable halocarbons
Viscosity of Transparent and Opaque (Standard Method 6230 B) and EPA
Method 608—Organochlorine pesticides
1 Copies of these standards may be obtained and PCBs (Standard Method 6630 C). 2
from the publisher. Copies may be inspected
at the U.S. Environmental Protection Agen 2 These test methods may be obtained
cy Superfund Docket, located at 1235 Jeffer from: Standard Methods for the Examination
son Davis Highway, First Floor, Arlington, of Water and Wastewater, 17th Edition,
VA 22202 or send mail to Mail Code 5305G, American Public Health Association, 1989; or
1200 Pennsylvania Ave., NW., Washington, Method 601—Purgeable halocarbons, 40 CFR
DC, or at the Office of the Federal Register, part 136 and Method 608—Organochlorine pes
1100 L Street, NW., Room 8401, Washington, ticide and PCBs, 40 CFR part 136. Copies may
DC 20408. Continued
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(12) The technical product data sub- (7) Toxicity. Use standard toxicity
mission shall include the identity of test methods described in appendix C
the laboratory that performed the re to part 300.
quired tests, the qualifications of the (8) Follow the data requirement spec
laboratory staff, including professional ifications in paragraph (a)(9) of this
biographical information for individ section.
uals responsible for any tests, and lab- (9) Surface Washing Agent Compo
oratory experience with similar tests. nents. Itemize by chemical name and
Laboratories performing toxicity tests percentage by weight each component
for dispersant toxicity must dem of the total formulation. The percent-
onstrate previous toxicity test experi
ages will include maximum, minimum,
ence in order for their results to be ac
and average weights in order to reflect
cepted. It is the responsibility of the
quality control variations in manufac
submitter to select competent analyt
ical laboratories based on the guide- ture or formulation. In addition to the
lines contained herein. EPA reserves chemical information provided in re
the right to refuse to accept a submis sponse to the first two sentences, iden
sion of technical product data because tify the major components in at least
of lack of qualification of the analyt the following categories: surface active
ical laboratory, significant variance agents, solvents, and additives.
between submitted data and any lab- (10) Heavy Metals, Cyanide, and
oratory confirmation performed by Chlorinated Hydrocarbons. Follow speci
EPA, or other circumstances that fications in paragraph (a)(11) of this
would result in inadequate or inac section.
curate information on the dispersing (11) Analytical Laboratory Require
agent. ments for Technical Product Data. Fol
(b) Surface washing agents. (1) Name, low specifications in paragraph (a)(12)
brand, or trademark, if any, under of this section.
which the surface washing agent is (c) Surface collecting agents. (1) Name,
sold. brand, or trademark, if any, under
(2) Name, address, and telephone which the product is sold.
number of the manufacturer, importer, (2) Name, address, and telephone
or vendor. number of the manufacturer, importer,
(3) Name, address, and telephone or vendor.
number of primary distributors or sales
(3) Name, address, and telephone
outlets.
(4) Special handling and worker pre- number of primary distributors or sales
cautions for storage and field applica outlets.
tion. Maximum and minimum storage (4) Special handling and worker pre-
temperatures, to include optimum cautions for storage and field applica
ranges as well as temperatures that tion. Maximum and minimum storage
will cause phase separations, chemical temperatures, to include optimum
changes, or other alterations to the ef ranges as well as temperatures that
fectiveness of the product. will cause phase separations, chemical
(5) Shelf life. changes, or other alterations to the ef
(6) Recommended application proce fectiveness of the product.
dures, concentrations, and conditions (5) Shelf life.
for use depending upon water salinity, (6) Recommended application proce
water temperature, types and ages of dures, concentrations, and conditions
the pollutants, and any other applica for use depending upon water salinity,
tion restrictions. water temperature, types and ages of
the pollutants, and any other applica
be inspected at the U.S. Environmental Pro tion restrictions.
tection Agency Superfund Docket, located at (7) Toxicity. Use standard toxicity
1235 Jefferson Davis Highway, First Floor, test methods described in appendix C
Arlington, VA 22202 or send mail to Mail
Code 5305G, 1200 Pennsylvania Ave., NW.,
to part 300.
Washington, DC, or at the Office of the Fed (8) Follow the data requirement spec
eral Register, 1100 L Street, NW., Room 8401, ifications in paragraph (a)(9) of this
Washington, DC 20408. section.
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(9) Test to Distinguish Between Sur (2) Name, address, and telephone
face Collecting Agents and Other number of the manufacturer, importer,
Chemical Agents. or vendor.
(i) Method Summary—Five milli (3) Name, address, and telephone
liters of the chemical under test are number of primary distributors or sales
mixed with 95 milliliters of distilled outlets.
water and allowed to stand undisturbed (4) Special handling and worker pre-
for one hour. Then the volume of the cautions for storage and field applica
upper phase is determined to the near tion. Maximum and minimum storage
est one milliliter. temperatures.
(5) Shelf life.
(ii) Apparatus.
(6) Recommended application proce
(A) Mixing Cylinder: 100 milliliter
dures, concentrations, and conditions
subdivisions and fitted with a glass for use depending upon water salinity,
stopper. water temperature, types and ages of
(B) Pipettes: Volumetric pipette, 5.0 the pollutants, and any other applica
milliliter. tion restrictions.
(C) Timers. (7) Bioremediation Agent Effective
(iii) Procedure—Add 95 milliliters of ness. Use bioremediation agent effec
distilled water at 22 °C, plus or minus 3 tiveness test methods described in ap
°C, to a 100 milliliter mixing cylinder. pendix C to part 300.
To the surface of the water in the mix (8) Bioremediation Agent Toxicity
ing cylinder, add 5.0 milliliters of the [Reserved].
chemical under test. Insert the stopper (9) Biological additives.
and invert the cylinder five times in (i) For microbiological cultures, fur
ten seconds. Set upright for one hour nish the following information:
at 22 °C, plus or minus 3 °C, and then (A) Listing of each component of the
measure the chemical layer at the sur total formulation, other than micro-
face of the water. If the major portion organisms, by chemical name and per
of the chemical added (75 percent) is at centage by weight.
the water surface as a separate and (B) Listing of all microorganisms by
easily distinguished layer, the product species.
is a surface collecting agent. (C) Percentage of each species in the
(10) Surface Collecting Agent Compo composition of the additive.
nents. Itemize by chemical name and (D) Optimum pH, temperature, and
percentage by weight each component salinity ranges for use of the additive,
of the total formulation. The percent- and maximum and minimum pH, tem
ages should include maximum, min perature, and salinity levels above or
imum, and average weights in order to below which the effectiveness of the
reflect quality control variations in additive is reduced to half its optimum
manufacture or formulation. In addi capacity.
(E) Special nutrient requirements, if
tion to the chemical information pro
any.
vided in response to the first two sen
(F) Separate listing of the following,
tences, identify the major components
and test methods for such determina
in at least the following categories:
tions: Salmonella, fecal coliform,
surface action agents, solvents, and ad
Shigella, Staphylococcus Coagulase
ditives. positive, and Beta Hemolytic
(11) Heavy Metals, Cyanide, and Streptococci.
Chlorinated Hydrocarbons. Follow (ii) For enzyme additives, furnish the
specifications in paragraph (a)(11) of following information:
this section. (A) Listing of each component of the
(12) Analytical Laboratory Require total formulation, other than enzymes,
ments for Technical Product Data. Fol by chemical name and percentage by
low specifications in paragraph (a)(12) weight.
of this section. (B) Enzyme name(s).
(d) Bioremediation Agents. (1) Name, (C) International Union of Bio
brand, or trademark, if any, under chemistry (I.U.B.) number(s).
which the agent is sold. (D) Source of the enzyme.
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control agents in paragraph (f) of this turers’ test results. EPA also reserves
section and EPA will consider listing the right to verify test results and con
those products on the NCP Product sider the results of EPA’s verification
Schedule under the miscellaneous oil testing in determining whether the dis
spill control agent category. EPA will persant meets listing criteria. EPA
inform the submitter in writing, within will, within 60 days of receiving a com
60 days of the receipt of technical prod plete application as specified in
uct data, of its decision on adding the § 300.915(a) of this part, notify the man
product to the Schedule. ufacturer of its decision to list the
(4) Certification. OSCs may request a product on the Schedule, or request ad
written certification from manufactur ditional information and/or a sample of
ers that produce sorbent materials that the product in order to review and/or
consist solely of the materials listed in conduct validation sampling. If EPA
paragraph (g)(1) of this section prior to requests additional information and/or
making a decision on the use of a par a product sample, within 60 days of re
ticular sorbent material. The certifi ceiving such additional information or
cation at a minimum shall state that sample, EPA will then notify the man
the sorbent consists solely of the mate- ufacturer in writing of its decision to
rials listed in § 300.915(g)(1) of the NCP. list or not list the product.
The following statement, when com (3) Request for review of decision. (i)
pleted, dated, and signed by a sorbent A manufacturer whose product was de
manufacturer, is sufficient to meet the termined to be ineligible for listing on
written certification requirement:
the NCP Product Schedule may request
[SORBENT NAME] is a sorbent material and EPA’s Administrator to review the de-
consists solely of the materials listed in termination. The request must be made
§ 300.915(g)(1) of the NCP. in writing within 30 days of receiving
(h) Mixed products. Manufacturers of notification of EPA’s decision to not
products that consist of materials that list the dispersant on the Schedule.
meet the definitions of two or more of The request shall contain a clear and
the product categories contained on concise statement with supporting
the NCP Product Schedule shall submit facts and technical analysis dem
to EPA the technical product data onstrating that EPA’s decision was in-
specified in this section for each of correct.
those product categories. After review (ii) The Administrator or his des
of the submitted technical product ignee may request additional informa
data, and the performance of required tion from the manufacturer, or from
dispersant effectiveness and toxicity any other person, and may provide for
tests, if appropriate, EPA will make a a conference between EPA and the
determination on whether and under manufacturer, if appropriate. The Ad
which category the mixed product ministrator or his designee shall render
should be listed on the Schedule. a decision within 60 days of receiving
[59 FR 47453, Sept. 15, 1994, as amended at 65 the request, or within 60 days of receiv
FR 47325, Aug. 2, 2000] ing requested additional information,
if appropriate, and shall notify the
§ 300.920 Addition of products to manufacturer of his decision in writ
Schedule. ing.
(a) Dispersants. (1) To add a dispers (b) Surface washing agents, surface col
ant to the NCP Product Schedule, sub lecting agents, bioremediation agents, and
mit the technical product data speci miscellaneous oil spill control agents. (1)
fied in § 300.915(a) to the Emergency Re To add a surface washing agent, sur
sponse Division (5202–G), U.S. Environ face collecting agent, bioremediation
mental Protection Agency, 1200 Penn agent, or miscellaneous oil spill con
sylvania Ave., NW., Washington, DC trol agent to the NCP Product Sched
20460. A dispersant must attain an ef ule, the technical product data speci
fectiveness value of 45 percent or great fied in § 300.915 must be submitted to
er in order to be added to the Schedule. the Emergency Response Division
(2) EPA reserves the right to request (5202–G), U.S. Environmental Protec
further documentation of the manufac- tion Agency, 1200 Pennsylvania Ave.,
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