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ERODE SENGUNTHAR ENGINEERING COLLEGE Calculate the rate of sublimation from a cylinder of naphthalene 0.

075m ID by
PERUNDURAI, ERODE -638 057 0.6m long into a stream of pure CO2 flowing at a velocity of 6 m/s at 1 atm. and
1000C. The vapor pressure of naphthalene at 1000C and 1 atm. may be taken as
IV Year-B. Tech., Degree (Chemical Engineering)
10 mmHg and the diffusivity of naphthalene in CO2 as 5.15x10-6 m2/s. The [AN] CO2
INTERNAL ASSESMENT TEST - III 14 density and viscosity of air are 0.946 kg/m3 and 0.021CP respectively at
operating condition. Cf = 0.023(Re)-0.2. Use analogy (13)
Credit: 3 Course code - CH6505 Course Name – Mass Transfer - I R-2013 (OR)
Date : 16.10.2018 mode Maximum marks:100 Explain differential gas - liquid contactors and its applications (13) [RE] CO2
Time: 1.30 P.m. to 4.30p.m. `ANSWER ALL THE QUESTIONS Duration: 3Hr. Sodium acetate solution is available at a temperature of 70 0C with a solute
content of 58 %. Find out
Bloom’s i. % of saturation
Q.No. Part- A ( 10 x 2 = 20 Marks) COs
Level ii. Yield of crystal formed if 2000 kg of solution is cooled to 100c
1 State Fick’s first law of diffusion. CO1 [AN] CO5
[RE] iii. % of yield
2 Define Sherwood & Lewis number. [RE] CO1 Data:
Solubility at 700C =146gm of sodium acetate / 100gm of H2o
3 Give the Wilke-Lee equation and its use. [RE] CO1 15
Solubility at 100C =121gm of sodium acetate / 100gm of H2o (13)
4 Define the term overall mass transfer coefficient. [RE] CO2 OR
Define NTU and HTU. CO2 Briefly explain the following terms:
5 [RE] i. Various methods of Super Saturation
6 What is JD factor? [RE] CO2 ii. Mier’s super saturation theory. [RE] CO5
7 What is the principle of crystallization? [RE] CO5 iii. Kelvin equation.
State McCabe's DL law of crystal growth. CO5 iv. Importance of crystal size. (13)
8 [RE] Bloom’s
9 Write the material and energy balance for Swenson-Walker crystallizer. [RE] CO5 Q.No Part- C ( 1 x 15 =15 Marks)
Level
Cos
10 How is the mother liquor separated from the crystals? [RE] CO5 A Swenson walker crystallizer has to produce 800kg per hour of FeSo4.7H20
Part- B (3 x 13 = 39 Marks) crystals. The saturated solution enters the crystallizer at 490c and slurry leaves at
270c, cooling water enters the crystallizer jacket at 150c and leaves at 210c. The
Ammonia gas (A) diffuses through Nitrogen gas (B) under steady state
conditions with Nitrogen Non diffusing. The total pressure is 1.013 x 10 5 Pa. overall mass transfer coefficient has been estimated to be 175 kcal / hr m2 0c.
and the temperature is 298K. The diffusion path is 0.15m. The partial There are 1.3m2 of cooling surface per meter of crystallizer length.
i. Estimate the cooling tower requirements in kg / hr [UN] CO5
pressure of Ammonia at one end is 1.5 x 10 4 Pa and at the other end is 5 x [UN] CO1
103 Pa. The diffusivity for the mixture at 1.013 x 10 5 Pa. and 298K is 2.3 x ii. Determine the number of crystallizer sections, each sections being 3m long
16. Data:
10-5 m2/sec. Calculate i. Flux of Ammonia (ii) Equimolal counter diffusion
Saturation solution of FeSO4 at 490C and 270C contain 140 parts and 74 parts of
flux, assuming that Nitrogen also diffuses. (13)
11 FeSo4.7H20 per 100 parts of free water respectively. Average specific heat of the
(OR)
initial solution is 0.70 and the heat of crystallization is 15.8 kcal/kg. (15)
An ethanol (A)-water (B) solution in the form of a stagnant film 2.0 mm thick
at 293 K is in contact at one surface with an organic solvent in which OR
ethanol is soluble and water is insoluble. Hence, Ng = 0. At point 1 the Classify the types of industrial crystallizers and Explain with neat sketch, the
working of a Swenson-Walker crystallizer and its industrial applications. (15)
[RE] CO5
concentration of ethanol is 16.8 weight% and the Solution Density is ρ1 =
[UN] CO1
972.8 kg/m3. At point 2 the concentration of ethanol is 6.8 wt% and ρ2 = The following course outcome are assessed:-
988.1 kg/m3. The diffusivity of ethanol is 0.74 x 10-9 m2/s. Calculate the COURSE OUTCOME MARKS
Steady state flux NA. (13)
CO1 To introduces the mass transfer principles 45
(i) How will you estimate the diffusivity for multi component diffusion? CO2 To study the diffusion interphase mass transfer co-efficient 71
(ii) Discuss diffusion of fluid through solids (13) [RE] CO1 To familiarize students with crystallization equipment’s commonly used in
12 CO5 64
(OR) industries
Explain various theories of mass transfer and its applications. (13) [RE] CO2 Prepared by Bloom’s level Keywor Marks
d
Derive the equation for Interface and overall Mass Transfer co-efficient in [RE] CO2 Remembering RE 100 Approved by
Binary and Multi component system. ( 13) Understanding UN 54
(OR)
Applying AP --
Sulphur dioxide is absorbed from air into water in a Packed Absorption
13 Analyzing AN 26
tower. At certain in the tower, Mass Transfer flux is 0.027 kmol and SO2/m2 M P MURUGESAN
h and the liquid phase concentrations in mole fraction are 0.0025 and 0.0003 Evaluating EV -- Dr.P.AKILAMUDHAN
[UN] CO2 & Creating CR -
respectively at the two-phase interface and in the bulk liquid. If the HoD/CHEM
M.V.RATNAM 180 (Including
diffusivity of SO2 in water is 1.7 X 10-9 m2/sec, determine the Mass AP/CHEM TOTAL
Transfer co-efficient, KC and film thickness (13) Choices)

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