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Article history: Fatigue testing was performed on riblet structured AA 2024 T351 thin sheets. Main focus was put on the
Received 23 April 2014 influence of different riblet geometries on fatigue life in the very high cycle fatigue (VHCF) regime. Exper-
Received in revised form 13 June 2014 iments on bare as well as on clad sheets were conducted at an ultrasonic frequency of around 20 kHz with
Accepted 16 June 2014
fully reversed axial loading (R = 1). While for bare material the riblet structure reduces lifetime by
Available online 24 June 2014
around one order of magnitude, the clad material is not negatively affected by the surface structure.
The threshold for fatigue failure of clad material is governed by the remaining thickness of the cladding
Keywords:
below the riblet structure. Finite element (FEM) simulations show that an optimal VHCF performance is
Very high cycle fatigue
AA 2024
reached, if the thickness of the clad layer below the riblet valleys is around 25% of the riblet diameter.
Cladding Ó 2014 Elsevier Ltd. All rights reserved.
Riblet structures
FEM simulations
http://dx.doi.org/10.1016/j.ijfatigue.2014.06.008
0142-1123/Ó 2014 Elsevier Ltd. All rights reserved.
S. Stille et al. / International Journal of Fatigue 68 (2014) 48–55 49
stress intensity at the crack tip has to be overcome for further crack material state, the riblet rolling was performed. Subsequently,
propagation. For that reason, if the stress is below the threshold, the material was precipitation hardened to the T4 state by solution
cracks are stopped at the interface and therefore, a sharp transition annealing at 500 °C for 80 min, quenching in water and natural
in the S/N-curve can be observed if fatigue tests are extended to the ageing for 8 days, which results in similar mechanical properties
VHCF regime [16]. of the AA 2024 sheets as in the T351 state without additional
Riblet surface structures induce an additional stress concentra- cold-working after the riblet structuring process. A more detailed
tions in the material. The influence of U-shaped notches with dif- description of the riblet rolling process as well as further details
ferent dimensions on fatigue life of bare AA 2024 T4 has been on the relevant parameters are provided in the study by Pöplau
studied by Li et al. [12]: a reduction in VHCF strength of around et al. [19].
60% was found for specimens with a notch depth and radius of The comparability of the T4 and the T351 temper has been
0.5 mm. Nevertheless, as recently shown by the authors of the ensured by tensile testing and indentation measurements. Table 2
present study [16], the notch effect in riblet structured clad mate- summarizes the results. In the T4 temper, the material shows with
rial is more complicated than just a simple stress increase in the 442 MPa only a slightly higher tensile strength than in the T351
vicinity of the notch if the cyclic loading leads to plastification of state. Furthermore, the measured hardness of the T4 state is with
the cladding. In this case the stress intensity of fatigue cracks 137 HV0.5 only slightly higher than in the as-received state. The
reaching the interface between cladding and substrate can be two material states have thus been considered to be comparable.
reduced and hence the fatigue strength is only slightly reduced
or even increased by the riblet structure.
3. Experimental details
In this work we focus on the influence of different diameters of
semi-circular riblet structures on the fatigue behavior and damage
Fatigue testing was performed using an ultrasonic fatigue test-
mechanisms. This is done for both, clad and bare material. Semi-
ing machine (UFTE). Details of the setup can be found in [20,21].
circular riblet structures are chosen because they can be produced
The sample preparation is described in detail in [16]. Specimens
on an industrial scale much more easily than sharp, blade-like
were taken from the structured material along (L-direction) and
structures. For structuring, a rolling process is applied as described
normal (T-direction) to the riblet orientation. Since in the active
in [17,18]. Since AA 2024 is a well studied material, it provides a
drag reduction system riblets are oriented normal to the load
suitable reference for our study. A further aim of this work is to
direction, most fatigue tests were performed at specimens in
optimize the riblet dimensions for the potential use in above men-
T-direction. For comparison some tests were made on samples in
tioned active drag reduction systems with respect to VHCF loading.
L-direction. The cladding on the backside of structured clad
specimens was removed prior to testing by grinding and polishing.
Measurements were performed at an ultrasonic frequency of
2. Material
approximately 19.1 kHz with zero mean stress (R = 1) at room
temperature.
Experiments were performed on commercially available AA
To assess the influence of localized cold working due to the roll-
2024 thin sheets produced by AMAG rolling GmbH (Randshofen,
ing process, micro-indentation tests were performed on polished
Austria). Sheets were received in the T351 temper. Details of the
cross sections of flat and riblet structured material. A Berkovic type
material properties and the chemical composition of the as-
indenter was used with a testing force of 1 mN in order to achieve a
received material can be found in [16]. Bare as well as clad sheets
sufficient lateral resolution. Indentations at such a small testing
were tested. Table 1 gives an overview on the investigated sheet
force suffer from indentation size effects and thus result in
materials. The clad material differs in sheet thickness as well as
increased hardness values and larger scatter compared to conven-
in thickness of the clad layer. In order to study the effect of riblet
tional hardness measurements. Nevertheless, measurements at the
size on fatigue behavior, different riblet diameters have been cho-
same testing force are comparable. Near surface residual stresses
sen for different types of sheets (see Table 1). Riblet rolling was
induced by the rolling process were analyzed by X-ray diffraction
performed along the rolling direction of the sheet (L-direction).
(XRD) using the sin2 W method [22]. Sample surfaces and polished
Polished cross sections of the studied materials and riblet
cross sections were studied by optical and electron microscopy
geometries are presented in Fig. 1. Clad specimens were structured
(SEM).
in the as-received state (T351). 2 mm thick clad sheets were struc-
tured with a riblet diameter of 80 lm, whereas for 1.6 mm thick
clad sheets a diameter of 300 lm was chosen. Sheets with 4. Results
300 lm riblets had to be stretched after rolling to remove curva-
ture of the sheets after rolling. In contrast to the well suited rolling The results of the mircoindentation measurements are summa-
behavior of the clad material, the bare material is much harder rized in Table 3. Measurements in riblet structures were performed
than the CP Al cladding. Consequently, rolling of bare material in on polished cross sections along paths from the riblet surface to the
the T351 temper led to poor riblet geometry and high wear of interior of the material. The distance between the indentations was
the rolling equipment. To overcome this problem, sheets were 5 lm. As can be seen, riblet rolling of the bare sheets led to a
rolled in the soft-annealed O state. For this, the material was slightly increased hardness from 194 to 215 HV0.01. Nevertheless,
annealed at 400 °C for 3 h and subsequently cooled down slowly considering the strong scatter of the data, this change, which is
(30 °C/h) to 250 °C. Afterwards, the furnace was turned off, leading attributed to the heat treatment after riblet rolling, is not consid-
to a faster cooling rate down to room temperature. In this soft ered to be significant. For clad specimens also just a slightly
Table 1
Key parameters of the studied specimens.
Fig. 1. Polished cross sections of the tested material. (a) 2 mm Thick clad sheet [16]. (b) Structured specimen with 80 lm riblet diameter [16]. (c) 1.6 mm Thick clad sheet. (d)
Structured specimen with 300 lm riblet diameter. (e and f) 2 mm Thick bare sheet with riblet structure (100 lm riblet diameter).
Table 2 Table 4
Mechanical properties of the material after heat treatments. Near-surface residual stresses determined by XRD.
Fig. 2. S/N-curves of bare material and literature data from [11] and [14]. Arrows Fig. 4. S/N-curves for 1.6 mm thick clad material and literature data from [23].
indicate run-out specimens. Red horizontal lines are corrected literature data [14] Arrows indicate run-out specimens. The dashed lines indicate threshold levels
taking into account the mean stress sensitivity according to [14]. (For interpretation below which only run-outs up to some 109 load cycles were observed.
of the references to color in this figure legend, the reader is referred to the web
version of this article.)
5. Discussion
polished prior to testing and thus are not affected by induced lengths below the intersection point of the two straight lines in
residual stresses. This is in good agreement with both, the Fig. 5, the threshold for failure is the fatigue limit of bare sheets
Smith–Watson–Topper approach and the mean stress sensitivity (comparable to the substrate), extracted from Fig. 2 (corrected val-
correction mentioned above: fatigue testing results for specimens ues), whereas for microstructurally long cracks, the threshold is
pffiffiffiffiffiffi pffiffiffiffiffi
with riblets along sample orientation are in good agreement determined by rth ¼ K max;th =1:122 pa. (K max;th ¼ 2:1 MPa m for
with residual stress corrected values of the flat material. The AA 2024 [11], a is the crack length). For further details on the con-
further reduction in fatigue strength in case of riblet structures struction of the Kitagawa–Takahashi diagram, refer to [16]. This
perpendicular to the load direction is attributed to the notch interpretation of VHCF strength also holds for material with differ-
effect which rises the surface stress in the riblet valley by around ent sheet thickness and riblet geometries tested in the present
67%, as has been found in an elastic FEM calculation (not shown study (cf. Fig. 5): the threshold levels for fatigue failure are deter-
here). This value is – in case of identical riblet height to width mined by the cladding thickness at the crack location. For both rib-
ratio – independent from the riblet diameter. let geometries, the rolling process locally reduces the cladding
The failure mechanism of the clad material has been discussed thickness, leading to an increased fatigue threshold value.
in detail in [16] by using a Kitagawa–Takahashi diagram, which is The influence of riblet orientation can be explained in the fol-
used to assess whether cracks in the cladding can propagate into lowing way: in perpendicular riblet orientation, cracks are always
the substrate. For microstructurally short cracks, i.e. cracks with initiated in the riblet valleys. Contrary, for riblets along the
Fig. 6. Finite element analysis of stress redistribution in the clad layer during cyclic loading. (a) FEM model for parameter study and geometry optimization. (b–e) Stress
distribution at maximum load during the 500th load cycle: (b) clad layer for 80 lm large riblets [16]. (c) Clad layer for 300 lm large riblets. (d) Upper part of the substrate
below the 80 lm large riblets [16]. (e) Upper part of the substrate below the 300 lm large riblets. Nominal stress amplitudes were generally adapted to the threshold values
for failure in the corresponding S/N-curves.
S. Stille et al. / International Journal of Fatigue 68 (2014) 48–55 53
samples direction, cracks occur across the riblets at many locations initiation at the surface (at a few 104 load cycles) the plastification
in the gauge length. Therefore, one cannot calculate the stress of the cladding during cyclic loading leads to a stress redistribution
intensity of through-cladding cracks using the remaining cladding in the near surface region of the specimen. Therefore, a similar cal-
thickness below the riblet valleys. Instead of this, an effective culation has been performed for the 300 lm large riblets. The sim-
cladding thickness has to be used, which will be higher than the ulation was performed again by modeling one riblet in 2D with
local thickness in the valleys, resulting in a higher stress intensity. plane strain conditions, similar to the geometry presented in
Furthermore, for riblets along the load direction, similarly to Fig. 6a. The specimen was exposed to an oscillating displacement
flat specimens [16], no notch effect and therefore no stress on one side, assuming symmetric boundary conditions on the other
redistribution (see discussion below) occurs. If one assumes that side. Whereas the substrate was considered fully elastic, for the
for structured and flat specimens the same stress intensity thresh- clad layer isotropic hardening was assumed. (For further details
old (Kmax,th) has to be exceeded for crack propagation into the on the FEM model, refer to [16]). The resulting stabilized stress dis-
substrate, the effective cladding thickness calculates as tribution in the clad layer after 500 load cycles for both, 80 and
300 lm large riblets are summarized and compared with each
rfat;flat 2 other in Fig. 6b and c. (The nominal substrate stress amplitudes
aeff ¼ a ;
rfat;riblets flat in both cases were adapted to the threshold values for fatigue in
the corresponding S/N-curves). In both cases, a region of peak
with: rfat,flat and rfat,riblets: fatigue threshold for flat material and stress below the riblet valley occurs. Since under the valleys of
riblets along the sample direction, respectively and aflat: cladding the smaller riblets a significantly thicker clad layer remains, the
thickness of the flat material. The resulting effective cladding thick- effective stress at the interface is smaller than in case of the
ness is 51.4 lm for 80 lm riblets and 58.8 lm for 300 lm riblets, 300 lm riblets (cf. Fig. 6d). In contrast, the bigger riblets
respectively. As expected, these values and therefore also the fati- (300 lm) result in a significantly thinner clad layer below the rib-
gue thresholds lie between the ones for riblets normal to sample let structure which shifts the peak stress region into the interface.
direction and flat material. This explanation holds nicely for the Consequently, the local effective interface stress is risen from 100
80 lm riblets. For the 300 lm riblets, one has to take into account to 121.6 MPa (cf. Fig. 6e). These modified stress levels are indicated
the notch effect for perpendicular oriented riblets, which signifi- in the Kitagawa diagram (Fig. 5) by open symbols.
cantly raises the stress in the riblet valleys and thus compensates The very different stress distribution in case of 80 lm and
the higher fatigue threshold to some extent. 300 lm big riblets and its effect on fatigue threshold raises the
Beside these findings, an interesting point to address are the question of an optimum riblet geometry with respect to fatigue
clearly different fatigue thresholds for both riblet geometries in life. Since the thickness of the clad layer is supposed to govern
normal orientation (125 MPa for 80 lm riblets and 100 MPa for the fatigue threshold level, this parameter has been studied in
300 lm riblets). As shown by FEM calculations in [16], before crack detail in an extended version of the previously used FEM model
Fig. 7. Parameter study of interface stress and stress intensity vs. cladding thickness (considered equal to crack length in the cladding). Red arrows indicate the cladding
thickness of the investigated fatigue specimens. (a) Effective interface stress (rx) for 80 lm large riblets. (b) Effective interface stress (rx) for 300 lm large riblets. (c) Resulting
stress intensity of cracks in the 80 lm large riblet structure. (d) Resulting stress intensity of cracks in the 300 lm large riblet structure. (For interpretation of the references to
color in this figure legend, the reader is referred to the web version of this article.)
54 S. Stille et al. / International Journal of Fatigue 68 (2014) 48–55
as shown in Fig. 6a. The nominal substrate stress as well as the thicknesses, the notch effect dominates and strongly raises the
effective interface stress have been considered at maximum load interface stress, and – as for the smaller riblets – the interface
in the stabilized state after 500 load cycles in a small region of stress reaches the nominal substrate stress at a remaining cladding
5 lm size, as indicated in Fig. 6a. In a parameter study for both rib- thickness of 1/4 of the riblet diameter. The minimum interface
let diameters, the thickness of the clad layer below the riblet valley stress level, which is 2.3% below the nominal substrate stress, is
was varied. The nominal substrate stress amplitude was set to the reached at a cladding thickness below the riblet valley of
threshold level for failure, taken from the S/N-graphs. The results d = 120 lm. For higher cladding thicknesses the interface stress
for both geometries are summarized in Fig. 7. asymptotically approaches to the nominal stress level. The
Fig. 7a and b shows the resulting stress (rx) in the substrate difference in the shape of both curves (and thus the strength of
near the interface below the riblet valleys. For very thin clad layers, the effect of stress distribution) might be caused by the different
the interface stress is dominated by the notch effect of the riblets, nominal stress amplitude that leads to a different level of cladding
i.e. significantly higher interface stresses occur compared to the plastification, which induces a different stress level in the clad
nominal substrate stress. If the cladding thickness below the riblets layer and results in a different degree of stress modification at
reaches around 1/4 of the riblet diameter, the interface stress the interface.
equals the nominal substrate stress. For 80 lm big riblets, there The resulting stress intensity at the crack tip, calculated as
pffiffiffiffiffiffi
is a plateau region up to 60 lm cladding thickness under the riblet K I ¼ 1:122rx pa (rx: applied stress normal to the sample direc-
valley where the interface stress is lowered by around 8.4% com- tion, a: crack length), is plotted for both riblet sizes in Fig. 7c and
pared to the nominal substrate stress. For thicker clad layers, the d. a was assumed to be equal to the thickness of the clad layer
interface stress rises again, even above the nominal level. The below the riblet valleys. For rx, the effective interface stress from
300 lm big riblet structure has a slightly different influence on the FEM calculation was chosen. As presented in the graph, the
the effective interface stress. Again, for very small cladding influence of the effective stress modifies the shape of the KI–a
curves. In both cases, the stress intensity has a plateau value for
a = 1/4 of the riblet diameter (d). If the clad thickness is further
increased, the higher stress intensity leads to an easier fatigue
crack propagation into the substrate. Nevertheless, thinner
remaining cladding thicknesses than 1=4 d are not recommended
due to the previously discussed notch effect and therefore, the
optimum cladding thickness below the riblet structure is a = 1=4 d.
6. Conclusion
Acknowledgments [10] Edwards PR, Earl MG, Britain ARC. A comparative study of the fatigue
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