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Ramberg-Osgood Parameters for

A. J. Rafanelli
63-37 Sn-Pb Solder •f\

2P& Raytheon Company, As part of a fracture properties study, the Ramberg-Osgood parameters were eval- (
Submarine Signal Division,
uated for 63-37 Sn-Pb (tin-lead) solder. This work was a preliminary step in ex-
Portsmouth, Rl 02871
perimentally determining J-integral values via the Hutchinson-Rice-Rosengren
(HRR) power law for hardening materials. Consideration was given to both en-
gineering strain and true strain when plotting the curves. Results disclosed little
effect of either engineering or true strain at linear stress levels. For a strain-hardening
exponent of 1.0, a material constant of 0.9849 was determined.

Introduction
Research is currently being performed to measure/determine for hardening materials. First, when solder deforms plastically,
fracture properties of 63-37 Sn-Pb (tin-lead by weight percent, strain hardening occurs. Strain or work hardening is an artifact
respectively) solder. In evaluating stress fields at a crack tip, of plastic deformation. When a metal deforms plastically, the
the energy release rate is a significant parameter. Due to the shear stress needed to produce slip continuously increases as
elastic-plastic nature of solder, i.e., a plastic zone existing at shear strain increases (Dieter, 1986). Next, recalling that solder
the crack tip, the energy release rate is expressed as the J- is a hardening material (Lau et al., 1987) application of the
integral (Broek, 1987). The J-integral, proposed by Rice (1968), HRR power law is proposed to determine the J-integral. The
characterizes the stress-strain field at a crack tip by integrating HRR power law is expressed as follows (Nigam, 1988):
a path far from the crack tip and substituting this path for
another close to the crack tip. The integrated path, taken far (1)
enough away from the plastic zone, can be used to analyze «o "b
crack tip region behavior since the J-integral is path inde-
Since the Ramberg-Osgood equation is:
pendent (Barsom and Rolfe, 1987).
Basic stress-strain data for 63-37 Sn-Pb solder, tested at e a a
—=—+ a o (2)
room temperature, disclose a predominantly plastic nature al- 0
to 0o
though some elastic behavior is present at approximately 1000
to 3000 psi (Rafanelli, 1989). Accordingly, research has been one can see that the former Eq. (1) is a simplified form of the
initiated to measure the J-integral for this material. The HRR latter (2). This special case is the condition of small non-linear
(Hutchinson, 1968, Rice and Rosengren, 1968) power law for strain, i.e., a/a0—0 (Broek, 1987). Accordingly, since the HRR
hardening materials is the approach utilized. Two quantities, power law is a special case of the Ramberg-Osgood equation,
namely a material constant a and a strain-hardening exponent, the material constant a and strain hardening exponent "n"
n are needed for the HRR analysis. This paper reports on the need to be determined.
experimental results, via use of the Ramberg-Osgood tensile
stress-strain relations, to obtain these two quantities. Experimentation
The procedure for determining the material constant a and
Background the strain-hardening exponent n is a combination of experi-
mental and analytical methods. The experimental methodology
Description of the Ramberg-Osgood method and justifica-
was greatly aided by previous work of Nigam (1988) in his
tion for its use have been previously discussed in a longer
dynamic and elastic-plastic fracture studies of Homalite^-100
version of this paper (Rafanelli, 1991). In short, it was deter-
polymer, 4340 steel, and 7075-T6 aluminum.
mined that, since the material did not truly conform to Hooke's
law, Young's modulus and the yield strength would be insuf- The first step in experimentation was to generate stress versus
ficient to accurately define a stress-strain curve and, conse- strain (engineering) curves. Five samples were tested. Due to
quently, a third parameter is required (Ramberg-Osgood, 1943). space limitations, however, curves for only one sample are
shown (Fig. 1). Next, engineering strain was converted to true
At this point, a brief explanation should be provided to
strain (Dieter, 1986) by use of Eq. (3):
illustrate the connection between the Ramberg-Osgood relation
and determination of the J-integral via the HRR power law e = ln(e+l) (3)
and stress versus true strain plots were then generated (Fig.
Contributed by the Electrical and Electronic Packaging Division and presented
at the Winter Annual Meeting, Atlanta, Ga., December 1-6, 1991 of THE AMER-
2). Since the material does not follow Hooke's law, the two
ICAN SOCIETY OF MECHANICAL ENGINEERS. Manuscript received by the EEPD parameters, Young's modulus and yield strength, are insuf-
August 1991. Paper No. 91-WA/EEP-21. ficient to describe the curve, as previously discussed. Conse-

234/Vol. 114, JUNE 1992 Transactions of the ASME

Copyright © 1992 by ASME


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strain (/Jf )
Fig. 1 Stress versus engineering strain (or 63-37 Sn-Pb solder

4000 6000 7000 S000 9000


strain <//f )

Fig. 2 Stress versus true strain for 63-37 Sn-Pb solder

quently, a third parameter is required. Ramberg-Osgood (1943) Furthermore, at the intersection of the horizontal line and
proposed the use of the secant yield strength of slope approx- Ramberg-Osgood secant yield strength line, a vertical is dropped
imating that of the yield strength for 0.2 percent offset. Recall to the x-axis. The abscissa value is e0, a Ramberg-Osgood strain
that the secant yield strength is the ordinate of the intersection quantity, which is used in the HRR power law and Ramberg-
of a line through the origin with slope of mE and the stress- Osgood relation (Eqs. (1) and (2), respectively).
strain curve, where m is a constant of value between 0 and 1.
For this case, m was chosen equal to 1. Also, the lines used
to determine the Ramberg-Osgood and 0.2 percent offset yield
strengths are denoted as the Ramberg-Osgood and offset yield Analysis
strength lines, respectively. Overlaying the Ramberg-Osgood Having determined the Ramberg-Osgood secant yield
and offset yield strength lines, the secant yield strength <70 can strength <J0 and strain e0» the HRR quantities a (material con-
be determined for all plots, i.e., stress versus engineering and stant) and n (strain hardening exponent) can be calculated.
true strains. A horizontal line is drawn starting from the in- Recalling Eq. (1):
tersection of the offset yield strength line and stress-strain curve
to the 7-axis. The ordinate value isCT0-Figure 3 illustrates a (1)
typical construction. eo

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Ramberg-Osgood
yield strength 1

£7 = s e c a n t y i e l d s t r e n g r.h
secant yield strain
Ramberg -Osgood s e c a i t . plrl
ut 0=
= Ramberc -Osgood s e c a i t y eld strain
f.h
0

strain (//C )

Fig. 3 Typical construction on a stress versus true strain curve to


determine <r0 and <0

Table 1 Summary of Ramberg-Osgood and HRR parameters Table 2 Summary of Ramberg-Osgood and HRR parameters
from stress versus engineering strain data from stress versus true strain data
Sample °o £o E a n Sample oo eo E a n
1 5187 1762 3.19 (10)6 1.1200 1.0 1 5200 2100 2.50 (10)6 0.9522 1.0
2 4750 2062 2.38 (10)6 1.0825 1.0 2 5850 2350 2.00 (10)6 1.1520 1.0
3 5250 1333 4.00 (10)6 1.1253 1.0 3 5400 1750 3.00 (10)6 0.9077 1.0
4 5250 2000 2.67 (10)6 1.0499 1.0 4 5300 2100 2.50 (10)6 0.9179 1.0
5 4750 1762 2.31 (10)6 1.1347 1.0 5 4700 1890 2.50 (10)6 0.9948 1.0
Mean 5037 1784 2.91 (10)6 1.1025 1.0 Mean 5290 2038 2.50 (10)6 0.9849 1.0
1 5187 1762 3.19 (10)6 4.4275 2.0 1 5200 2100 2.50 (10)6 1.9050 1.5
2 4750 2062 2.38 (10)6 4.8430 2.0 2 5850 2350 2.00 (10)6 1.1521 1.5
3 5250 1333 4.00 (10)6 3.3758 2.0 3 5400 1750 3.00 (10)6 1.6175 1.5
4 5250 2000 2.67 (10)6 4.4100 2.0 4 5300 2100 2.50 (10)6 1.8018 1.5
5 4750 1762 2.31 (10)6 4.5354 2.0 5 4700 1890 2.50 (10)6 1.9288 1.5
Mean 5037 1784 2.91 (10)6 4.3183 2.0 Mean 5290 2038 2.50 (10)6 1.6810 1.5
1 5187 1762 3.19 (10)6 2.2280 1.5 1 5200 2100 2.50 (10)6 3.8095 2.0
2 4750 2062 2.38 (10)6 2.2910 1.5 2 5850 2350 2.00 (10)6 6.2425 2.0
3 5250 1333 4.00 (10)6 1.9490 1.5 3 5400 1750 3.00 (10)6 2.8829 2.0
4 5250 2000 2.67 (10)6 2.1520 1.5 4 5300 2100 2.50 (10)6 3.5375 2.0
5 4750 1762 2.31 (10)6 2.2680 1.5 5 4700 1890 2.50 (10)6 3.7401 2.0
Mean 5027 1784 2.91 (10)6 2.1776 1.5 Mean 5290 2038 2.50 (10)6 4.0425 2.0

An arbitrary value of e is selected for each set of curves. Values e,h = eoa[a/a0]" (4)
of E are best selected along the linear portion of each curve.
(The stress-engineering strain and stress-true strain groups of Figures 4 and 5 illustrate the stress versus Ramberg-Osgood
curves are referred to as sets.) For the selected value of e, a theoretical strains overlayed upon the experimentally derived
corresponding value of a is determined from each curve. Se- stress-engineering strain and stress-true strain curves, respec-
lecting a value for n, an iterative approach is used to determine tively. (Again, curves for one sample only are shown.) Ob-
a. For this study, each set of curves underwent three sequences viously no one value of n (and subsequently a) can be selected
of iterations for « = 1.0, 1.5, and 2.0. Each curve underwent to perfectly fit each curve. Thus, the final values of n and a
a minimum of five iterations. Tables 1 and 2 summarize the selected are those in which the most data falls on or near the
HRR quantities for the stress-engineering strain and stress-true experimental curve (Nigam, 1988). The curves suggest that the
strain cases. The results for each set of five curves are averaged n=l.O case is best. However, additional values of n, e.g.,
for each value of n. Values of elastic modulus E are also shown 1.0<«<1.5, would appear to provide improved curve fits.
for informational purposes. (Data in Tables 1 and 2 are for Inspection of Figs. 4 and 5 suggest little difference between
all five samples.) engineering and true strains with respect to Ramberg-Osgood
and HRR Power Law parameters.
The arbitrary selection of e along with its corresponding
value of a proves to be of little influence since it is chosen
from that portion of the stress-strain curve with constant slope.
However, the effectiveness of value selections for n is mani- Conclusions
fested by the quality of curve fits for stress versus a theoretical Results of stress-strain testing have disclosed little or no
strain elh as generated by rearranging the Ramberg-Osgood effects of engineering strain as opposed to true strain in gen-
equation, i.e., erating Ramberg-Osgood and HRR parameters for 63-37 tin-

236 / V o l . 114, JUNE 1992 Transactions of the ASME

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0 •ffl-n = 1.0 Of= 1.1200

^ -mi = 1 . 5 0!= 2.2280

© =*-n = 2 . 0 CX= 4.4275

9000 10000 11000 12000 13000

rain (/j£ )

Fig. 4 Ramberg-Osgood plots overlayed on stress versus engineering


strain curve

stress
(psi) • A
0 A
4000 -
A 0

0 / A o
3000 - 0/ A Q

-J A o
A e
2000 -
E/A Q

Fig. 5 Ramberg-Osgood plots overlayed on stress versus true strain


curve

lead solder. To date, the data also suggest that accuracy of Phil Thornton, D. Allberg, M. McCormick, and the Raytheon
the HRR strain-hardening exponent can be improved for values Company for their help and support. Finally, special thanks
between 1.0 and 1.5. However, since the data track relatively to Mrs. Barbara Medeiros for preparing and typing this man-
well for a strain-hardening exponent n = 1.0, the material con- uscript.
stant a is determined to be 0.9849 (mean value of the five
curves).
References
Barsom, John M., and Rolfe, Stanley, T., 1987, Fracture and Fatigue Control
Acknowledgment in Structures, Second Edition, Prentice-Hall Inc., Englewood Cliffs, NJ, pp.
The author would like to thank Dr. Arun Shukla of the 574, 575.
Broek, David, 1987, Elementary Engineering Fracture Mechanics, Martinus
Mechanical Engineering and Applied Mechanics Department Nijhoff Publishers, Boston, MA, p. 79.
at the University of Rhode Island for his help and guidance Dieter, George, E., 1986, Mechanical Metallurgy, Third Edition, McGraw-
during this research. Appreciation is also extended to Frank Hill Book Company, New York, NY, pp. 73-74, 139.
Liotine, Andrew Moniz, Charles Clarke, Benjamin Brewer, Hutchinson, J. W., 1968, "Plastic Stress and Strain Fields at a Crack Tip,"

Journal of Electronic Packaging JUNE 1992, Vol. 114/237

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Journal of Mechanics and Physics of Solids, Vol. 16, Pergamon Press, pp. 337- lations for 63-37 Sn-Pb Solder," ASME Winter Annual Meeting, Paper 91-
347. WA/EEP-21.
Lau, J., Harkings, G., Rice, D., and Krai, J., 1987, "Thermal Fatigue Re- Ramberg, Walter and Osgood, William R., 1943, "Description of Stress-
liability of SMT Packages and Interconnections," 1987 IEEE International Re- Strain Curves by Three Parameters," Technical Notes National Advisory Com-
liability Physics Symposium. mittee for Aeronautics No. 902, Washington, D.C.
Nigam, Himanshu, 1988, Experimental Studies in Dynamic and Elastic-Plastic Rice, J. R., 1968, "A Path Independent Integral and the Approximate Analysis
Fracture, Ph.D. Dissertation, University of Rhode Island, Kingston, RI. of Strain Concentration by Notches and Cracks," ASME Journal of Applied
Rafanelli, Anthony, J., 1989, "Tensile Testing of 63-37 tin-Lead (Sn-Pb) Mechanics, Vol. 35, June, 1968.
Solder at Room Temperature," Raytheon Company Industrial Engineering Rice, J. R., and Rosengren, G. F., 1968, "Plane Strain Deformation Near a
Council Journal, Raytheon Company, Lexington, MA. Crack Tip in a Power Law Hardening Material," Journal of Mechanics and
Rafanelli, Anthony, J., 1991, "Ramberg-Osgood and HRR Power Law Re- Physics of Solids, Vol. 16, Pergamon Press, pp. 1-12.

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