Components Molecular weight inlet mass kg/hr

Ethanol 46.07 0.0001192745

H2O 18.01528 95.9686572668
Ethylene Glycol 62.07 4344.6315117479
Total 4440.6002882892
Inlet mole Kmole/hr inlet mass Fraction inlet mole fraction Top mass (kg/hr)
0.000002589 2.685999063605E-08 3.43718713214115E-08 0.0001192745
5.3270699799 0.0216116406 0.0707232568 95.8425224429
69.995674428 0.9783883326 0.9292767088 0.0003302318
75.3227469969 1 1 95.8429719492

4440.6002882892
Ethanol
A
B
C
Temp (K)
log(p1 sat)
P SAT bar
ALPHA 16

K1

Sum B.P
 Top mole (kmole/hr) Top mass fraction Top Mole fraction bottom mass (kg/hr)
0.000002589 1.24447811298429E-06 4.86644582114259E-07 1.28780645654748E-12
5.3200684332 0.99999531 0.9999995134 0.1261348239
0 3.44555044012278E-06 0 4344.6311815161
5.3200710222 1 1 4344.75731634

Ethanol Water Ethylene Glycol

4.92531 A 3.55959 A
1432.526 B 643.748 B
-61.819 C -198.043 C
462 Temp (K) 462 Temp (K)
1.3456148121 1.1207533713
22.1622991154 13.2054550514
28.5027355003 16.9834181252

Total Presuure (bar) 1.0132500000

21.8724886409 K2 13.0327708378 K3

1.0324578264 Sum D.P 1.2766272042

 bottom mole (kmole/hr) bottom mass fraction Bottom Mole fraction
2.79532549717274E-14 2.9640469254847E-16 3.99316979058276E-16
0.0070015467 2.90315004411578E-05 0.0001000183
69.9956691077 0.9999709685 0.9998999817
70.0026706544 1 1

Ethylene Glycol
4.97012
1914.951
-84.996
462
-0.1092717306
0.7775498992
1

0.7673820866
Bubbel point T (k) 462
Dew Point T(k) 470

Components relative volatility at B.P

Ethanol 26.27
H2O 15.711
Ethylene Glycol 1

Average realtive volatility 0.0612250633

xd L.K 0.99999531
xd H.k 3.44555044012278E-06
xw L.k 2.90315004411578E-05
xw H.k 0.9999709685
N min 8.2434245494
N min approx 9
F (kg/hr) 4440.6002882892
D (kg/hr) 95.8429719492
W (kg/hr) 4344.75731634

Components Alpha = relative volatility

Ethanol 24.1276438966
H2O 16.3331803394
Ethylene Glycol 1

column efficiency
Components
Ethanol
H2O
Ethylene Glycol

Mol avg
Efficiency
% Efficiency
 Temperature (K)
470.6831500459

relative volatility at D.P geometric mean

22.16 24.1276438966
16.98 16.3331803394
1 1

Average Cp (j/g)
avg heat of vaporization (j/g)
Tb
Ta
q

F (inlet Fraction) D (distillate Top fraction)

2.68599906360533E-08 1.24447811298429E-06
0.0216116406 0.99999531
0.9783883326 3.44555044012278E-06

column efficiency
Viscosity M avg V
0.01097 5.73331066651862E-05
0.0091 18.0151955078
0.024 0.0002138653

0.1639440408
76.1297396731
0.7612973967
Net Area
Net Area
Down Comer Area
Down Comer Area
Cross sectional Area (Top)
Cross sectional Area (Bottom)

Plate Design

Aa (Top) m2
Aa(bottom) m2
Ad/Ac*100 (top)
Ad/Ac*100 (Bottom)
Lw/Dc
lw (weir length) m
Ah
weir height mm
hole dia (mm)
 thickness (mm)

Mechanical Design (pa)

p 100000
Do (m) 0.1632147325
J 1
ts (m) 0.003
C 0
fas (pa) 5440491.08359916
fcs (pa) 10880982.1671983
Insulation thickness(m) 0.01
Dm (m) 0.1832147325
W ins (lb/ft) 23.8428423237
W ins (kg/m) 3.296391067
W in kg 12.5098040992
insulation weight stress (Pa) 7248.3509555484

Cd 0.005
density of air kg/m3 1.2754
wind velocity (m/sec) 28.8
A 3.83
Pw (Pa) 10.1290839552
 Pressure
1.0132500000

Cp(J/g.k) Heat of Vaporization (j/g) Inet Fraction Density kg/m3

4.9 474 2.685999064E-08 789
4.18 851 0.0216116406 997
1.8308361527 982.7613984211 0.9783883326 1110
1

1.8816055198
979.9138047745
462
470.6831500459
0.9833268365

0.85874
0.0166731635

F*Alpha D*Alpha ɸ
6.4806828913207E-07 3.002632475E-05 0.85874
0.3529868226 16.3331037363 0.85874
0.9783883326 3.44555044E-06 0.85874

Vmin
Lmin
Rmin
R
X
Y
N
N Approx
NR/NS
NS
density v 997.0001304958 NS approx
density L 1109.9967194405 NR
 for real Reflux kg/h kg/sec
F 4440.6002882892 1.2335000801
D 95.8429719492 0.0266230478
W 4344.75731634 1.2068770323
R 0.0721692694 0.000020047
Ln=RD 6.9169172651 0.0019213659
Lm=Ln+qF 4373.478351032 1.2148550975
Vn=Ln+D 102.7598892143 0.0285444137
Vm=Vn+(1-q)F 176.7987437366 0.0491107621

Avg. density of liquid (kg/m3) 1109.9967194405

Avg. density of distillate (kg/m3) 997.0001304958
Floding velocity Flv (top) 0.0710235202
Floding velocity Flv (bottom) 0.0426545568
Surface Tension (top) 70
Surface Tension (bottom) 110
K (top) 0.061
K(Bottom) 0.064
uf (top) 0.0044410286
uf (Bottom)) 0.0302996472
Un (top) m/s 0.0035528229
Un (bottom) m/s 0.0242397177
An (top) m2 0.0080584656
An (bottom) m2 0.0020321413
Ad (top) m2 0.0012087698
Ad (bottom) m2 0.0003048212
Ac (Top) m2 0.0092672355
Ac (Bottom) m2 0.0023369625
Dia (Top) m 0.1086526369
Dia (Bpttom) m 0.0545620956
Tray Spacing 0.3
Height m 3.795
0.1632147325

0.0068496958
0.0017273201
13.0434782609
13.0434782609
0.76
0.0414671927
0.0003082363
40
2.5
3
a*Dx/a-ɸ
1.290406E-06
1.055489141
2.439155E-05

101.1636775
5.320705589
0.055514823
0.072169269
0.015533412
0.075657545
11.82192405
12
11.57899342
0.953971403
1
11
m3/sec

0.000001731
0.001094467
2.86303E-05
4.925853E-05
 REBOILER DESIGN
Properties Units
Inner Tube inner radius meters 0.001
Flow Arrangement Counter Flow
Outer tube ID to Inner tube ID ratio 10.000
Tubes in Reboiler Coiled Tube
Heat Exchanger Length L meters 4.80
Heating media Flow Rate kg/hr 5000.00
Temperature of heating medium K 500.00
Overall Heat Transfer Coefficient UA W/K 103834.93
Area sq. meters 0.15072
Mass Velocity kg/m2.hr 33174.0976645435
Bubble Point K 462.00
Numer of Tubes Passes 1
Outer Diameter meters 0.01
Heat Transfer kJ/hr 594700
 CONDENSER DESIGN
Properties Units
Inner Tube inner radius meters 0.019
Flow Arrangement Counter Flow
Outer tube ID to Inner tube ID ratio 5.263
Tubes Coiled Tube
Heat Exchanger Length L meters 3.50
Coolant Flow Rate kg/hr 100.00
Outlet Temperature of Coolant K 278.27
Overall Heat Transfer Coefficient UA W/K 380.35
Outer Diameter meters 0.10
Dew Point K 470.00
Area sq. meters 1.099
Mass Velocity kg/m2.hr 90.991810737
Number of Tube Passes 1
Heat Transfer kJ/hr 80143.14
Components
H2O
Ethylene Glycol
Total

HF
Hv
HL

q
tan(o)
angle
R min
R

Top line

Red
green
purple
xw Approx

Number of ideal stages

F (kg/hr)
D (kg/hr)
W (kg/hr)
Ln (kg/hr)
Vn (kg/hr)
Lm (kg/hr)
Vm (kg/hr)
Net Area
Net Area
Down Comer Area
Down Comer Area
Cross sectional Area (Top)
Cross sectional Area (Bottom)

Plate Design

Aa (Top) m2
Aa(bottom) m2
Ad/Ac*100 (top)
Ad/Ac*100 (Bottom)
Lw/Dc
lw (weir length) m
Ah
weir height mm
hole dia
thickness
Inlet Fraction F Top Fraction Bottom Fraction Enthalpy (kj/kg)
0.0216116406 0.99999531 2.9031500441E-05 851.8624
0.9783883326 3.44555E-06 0.9999709685 982
0.9999999731 0.9999987555 1

979.18748659
851.8617882716
981.9962219102

0.9784166631
-45.3320387294
88.736
3.2475417263
4.2218042442
1.2

0.1915044511 1

0.8

0.6

distillate 0.4
Feed
q line 0.2
0 (so no line)
0
0 0.2 0.4 0.6 0.8 1 1.

4
4440.6002882892
95.8429719492
4344.75731634 m3/sec
404.6302657497 9.4451509279E-05
500.4732376988 0.0001394387
4749.3875820897 0.0011086339
596.316209648 0.0001661418

Avg. density of liquid (kg/m3) 1190

Avg. density of distillate (kg/m3) 997
Floding velocity Flv (top) 0.8832901894
Floding velocity Flv (bottom) 0.137171821
Surface Tension (top) 70
Surface Tension (bottom) 110
K (top) 0.061
K(Bottom) 0.064
uf (top) 0.0075853496
uf (Bottom)) 0.0395989424
Un (top) m/s 0.0060682796
Un (bottom) m/s 0.0316791539
An (top) m2 0.0229782851
An (bottom) m2 0.0052445156
Ad (top) m2 0.0034467428
Ad (bottom) m2 0.0007866773
Ac (Top) m2 0.0264250279
Ac (Bottom) m2 0.0060311929
Dia (Top) m 0.1834733112
Dia (Bpttom) m 0.0876529996
Tray Spacing 0.3
Height m 1.035

0.0044578383
0.1306232554
13.0434782609
14.4026549266
0.75
0.225
0.0002006027
40
2.5
3
 in vapor In liquid
0 0
0.002 0.23
0.003 0.31
0.01 0.4
0.02 0.54
0.06 0.73
0.13 0.85
0.22 0.9
0.3 0.93
0.47 0.97
1 1

0.8 1 1.2