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SYNOPSIS
This paper presents the mix proportioning of High Strength Concrete (HSC) of M85 grade with
60 MPa in 7 days. M55 (the maximum possible grade that can be designed) grade as per IS
10262: 2009 limiting maximum cement content to 450 kg/m3 of concrete was designed. Trials
adopting various mineral additives like silica fume and fly ash at various percentage levels such
as 2.5%, 5%, 10%, 15%, 20% etc.,. Were mixed and tested. Chemical admixtures like super
plasticizer and rapid hardening solution were also adopted in combination with mineral
admixtures at various dosages starting from 0.6% to 1.5% by weight of cement. The target
strength of 85 MPa in 28 days and 60 MPa in 7 days was achieved with w/c 0.34, cement content
438 kg/m3, 2.5% Silica fume and 1.2% of super plasticizer. Workability of fresh concrete and
other mechanical properties for hardened concrete were determined for 3, 7, 14, 28 days of
curing in potable water. Rapid chloride penetration test (RCPT) value was determined after 28
and 90 days to establish the durability of this mix. The results indicate that the early strength is
low for higher percentage replacement of additives. However, the performance of the mix
designed was satisfactory in terms of mechanical properties.
KEYWORDS: High Strength Concrete, High Early Strength Concrete, Cement Replacement,
SYNOPSIS: This paper presents the mix proportioning of High Strength Concrete (HSC) of
M85 grade with 60 MPa in 7 days. M55 (the maximum possible grade that can be designed)
grade as per IS 10262: 2009 limiting maximum cement content to 450 kg/m3 of concrete was
designed. Trials adopting various mineral additives like silica fume and fly ash at various
percentage levels such as 2.5%, 5%, 10%, 15%, 20% etc.,. Were mixed and tested. Chemical
admixtures like super plasticizer and rapid hardening solution were also adopted in combination
with mineral admixtures at various dosages starting from 0.6% to 1.5% by weight of cement. The
target strength of 85 MPa in 28 days and 60 MPa in 7 days was achieved with w/c 0.34, cement
content 438 kg/m3, 2.5% Silica fume and 1.2% of super plasticizer. Workability of fresh concrete
and other mechanical properties for hardened concrete were determined for 3, 7, 14, 28 days of
curing in potable water. Rapid chloride penetration test (RCPT) value was determined after 28
and 90 days to establish the durability of this mix. The results indicate that the early strength is
low for higher percentage replacement of additives. However, the performance of the mix
1
Professor of Civil Engineering, MVGR College of Engineering, Vizianagaram - 535 005, (A.P), India.
markandeyaraju@gmail.com
P.G student in Structural Engineering, MVGR College of Engineering, Vizianagaram - 535 005, (A.P), India.
shivab.145@gmail.com
KEYWORDS: High Strength Concrete, High Early Strength Concrete, Cement Replacement,
1. INTRODUCTION
1.1 GENERAL
Increasing progress in the applications of prestressed concrete in the construction industry has
generated interest in the High Strength Concrete (HSC). Successive increase in compressive
strengths of concrete over the past few decades resulted in changing definitions to high strength
concrete. ACI committee 363 defines HSC as “The concrete with specified compressive strength
equal to or greater than 40 MPa”. High strength concretes made by adding pozzolana like flyash;
blast furnace slag and silica fume are order of the day in the economic and environmental
perspectives. Blending pozzolana also makes concrete durable by reducing the permeability. The
only way to have low volume of pores is to ensure that the mix contains particles graded down to the
finest size. This is usually achieved by the use of pozzolana which fills the space between the cement
particles and aggregates. The mix must be sufficiently workable for the solids to be dispersed in such
a manner that dense packing is achieved. This also requires deflocculation of cement particles which
can be achieved by the use of suitable super plasticizer at a required dosage. The super plasticizer
must be compatible with the cement. Hence, low permeability and dense concrete result in durable
concrete. In the present investigations, mix design for HSC was carried out by using mineral and
chemical admixtures. The RCPT on High Strength Concrete was also carried out.
2. LITERATURE REVIEW
D. Karthik and J. Doraikkannan1 have conducted Experimental Investigation on silica fume and steel
slag in concrete. Ashfi Rahman and Harjinder Singh2 have studied the Effect of Mineral Admixtures
on Characteristics of High Strength Concrete. Harjinder Singh and Shikha Bansal3 performed studies
on Effect of Silica Fume on the Strength of Cement Mortar. It is reported that the compressive
strength of mortar improves when a part of cement/sand is replaced by certain percentage of silica
fume. Dr. Engr. Gana and Engr. Okoye4 presented a case study on Relevance of High Performance
advantages for Kurdistan Region, Iraq. Abudel Salam6 has studied effect of steel fiber and silica
fume on hardened concrete compressive and flexural strength. In this paper an attempt is made at
300°C to present the results of an experimental investigation carried out on fiber reinforced concrete.
Damgir et al., 7 presented a case study of split tensile strength of fiber reinforced concrete using silica
fume and steel fibers. Sesha phani et al.,8 conducted studies on effect of mineral admixtures on
durability properties of High Strength Self Compacting Concrete (HSSCC). Shanmugapriya and
Uma 9 carried out experimental Investigation on Silica Fume as Partial Replacement of Cement in
High Performance Concrete. Shanmugapriya and Uma10 have carried out experimental investigations
to assess the suitability of silica fume in high performance concrete. Vijaya Kishore11 studied the
performance of Ultra Strength Concrete. Faseyemi Victor Ajileye12 reported investigations on Micro
experimental investigation on High Performance Concrete using Silica Fume and Superplasticizer.
Sreenivasulu and Srinivasa Rao14 presented a case study on design of M100 grade concrete. Shankar
and Khadiranaikar 15 have studied RCPT on Geopolymer concrete. It is reported that as the grade of
concrete increases, the RCPT charges decreases. Chandramouli et al.,16 examined RCPT for
durability studies on glass fiber reinforced concrete. Yaqub and Imran Bukhari17 performed studies
on Effect of Size of Coarse Aggregate on Compressive Strength of High Strength Concrete. This
paper describes the influence of aggregate size on compressive strength of high strength concrete.
3. EXPERIMENTAL PROGRAM
3.1.1 Cement: Ordinary Portland cement of 53 grade conforming to Indian standard IS 12269: 1987
was used for the present experimental investigation. Various properties of cement were determined
3.1.2 Fine Aggregate: Natural River Sand conforming to IS 383: 1987 and IS 10262: 2009 was
used. The results of various tests on fine aggregate are given in Table 2.
3.1.3 Coarse Aggregate: Crushed granite course aggregate conforming to IS 383: 1987 was used.
3.1.4 Fly Ash: Fly ash confirming to IS 3812: 1981 of Indian standard was used as pozzolana
admixture. Fly ash was obtained from NTPC Paravada, Visakhapatnam, Andhra Pradesh,
INDIA.
3.1.5 Silica Fume: Commercially available Silica fume was procured and used in the experimental
investigation from Industrial area, Autonagar, Gajuwaka, Visakhapatnam. Physical and Chemical
Chemicals is used. The super-plasticizers used for the study conform to IS 9103: 1999. The
3.1.7 Potable Water: Ordinary potable tap water available in laboratory was used for mixing
properties of ingredients they can be proportioned to obtain the maximum strength. This chapter
presents mix design of M55 grade concrete with different cement contents and w/c ratios as
shown in below table. Although all mix designs were presented here, the minimum with a
cement content of 450 kg/m3 and w/c ratios of 0.28, 0.3, 0.34 and 0.4 were designed and tested
for 7 days. Maximum strength was achieved at w/c ratio of 0.34, keeping it constant cement
content was increased to 500, 550 and 600 kg/m3 and mixes were designed and tested. The mix
design calculations that were performed for conducting this study are presented in Table 6. Both
Percentage of silica fume and Fly-Ash were taken by Cement Weight and replaced in both fine
aggregate and cement. The dosage of Super plasticizer is X lt for 100 kg of Cement, Where X =
0.25, 0.5, 0.75, 1, 1.5 and 2 lt. The dosage of Rapid hardening Solution is 6 lt for 100 kg of
Cement and it is replaced by Water. It is assumed that maximum cement content would result in
maximum strength and hence fine aggregate and cement was replaced with mineral admixtures.
[1] From Table 7, the percentage of Fly-Ash is replaced in Fine aggregate, we can see that the
maximum early strength of 53.35 MPa is reached at 5% of fly-ash and the maximum density
[2] From Table 8, Silica fume is replaced in Fine aggregate, we can see the maximum early
strength of 52.3 MPa is reached at 2.5% of silica fume (by weight of cement) and the
[3] From Table 9, to study the effect of Superplasticizer and determine its optimum dosage,
different percentages were considered for w/c of 0.34, we have known that the maximum
early strength of 52.5 MPa attained at 0.25 dosages and maximum density of 2497 kg/m3 at
0.5 dosages.
[4] From above Table 10, the percentage of Silica fume is replaced in Fine aggregate and the
results were shown with the combination of super plasticizer. we can see that the maximum
early strength of 51.75 MPa at 2.5% of silica fume and maximum density of 2390 kg/m3 at
[5] From Table 11, the dosage of Rapid Harding Solution (R.H.S) was used for different levels
i.e., 5 lt, 5.5 lt, 6lt for 100 kg cement. We can see that dosage of 6 lt for 100 kg cement was
[6] From Table 12, combination of R.H.S and Fly Ash were used at different cement contents. It
shows that the maximum strength and density was achieved at 600 kg/m3 of cement content
[7] From Table 13, combination of R.H.S and Silica Fume were used at different cement
contents. It shows that the maximum strength and density was achieved at 550 kg/m 3 of
[8] From Table 14, combination of R.H.S, Silica Fume, Superplasticizer and Fly Ash were used
at different cement contents. Flyash and silica fume was replaced in cement content; R.H.S
was replaced in water content. The results shows that the target strength of 60 MPa in 7 days
was achieved with w/c 0.34, cement content 438 kg/m3, 2.5% Silica fume and 1.2% of super
plasticizer. So this mix is finalized for further work and the mix proportions for finalized
The mix design was carried out as per IS 10262: 2009 and IS 456: 2000 and the mix proportions
for concrete of M85grade were achieved after a number of trial mixes. Identification mix proportions
and quantity of materials of concrete mixture are given in Table 8. For M85 grade concrete the
trials were carried out to improve strength and durability of the fresh concrete.
3.4 Workability
The workability tests were conducted on fresh concrete of finalized mixture and the values are given in
Table 16. It shows that the workability for this mixture is low.
The sizes of various specimens were adopted as per IS 516: 1959. Specimens were de-moulded
in 20 hours and cured as the top surface of the concrete in the mould was hard enough by then.
Spreading wet gunny bags over the mould for the 1st 20 hours after the casting was carried out for
Concrete cylindrical specimens are used to determine Split tensile strength of concrete and were
tested as per IS 516: 1959 and IS 5816: 1999. The split tensile strength of concrete at curing
Flexural strength of concrete was determined by two points loading as per IS 516 (1959). The
flexural strength of concrete at curing periods of 7, 14 and 28 days are presented in Table 17.
A typical stress and strain curve of concrete in compression is shown in Figure 1. The relation is
fairly linear in the initial stages but subsequently becomes non-linear reaching a maximum value
and then a descending portion is obtained before concrete finally fails. The curve is usually
obtained by testing a cylinder with a height-to-lateral dimension ratio of at least 2 (150 mm x
300 mm), the test being conducted under uniform rate of strain. If a uniform rate of strain is
adopted, it will not be possible to obtain the descending portion of stress and strain curve beyond
For reinforced concrete structures, one of the major forms of environmental attack is chloride
ingress, which leads to corrosion of the reinforcing steel and a subsequent reduction in the
strength, serviceability, and aesthetics of the structure. A common method of preventing such
deterioration is to prevent chlorides from penetrating the structure to the level of the reinforcing
steel bar by using relatively impenetrable concrete. The ability of chloride ions to penetrate the
concrete must then be known for design as well as quality control purposes. One of the tests to
know this is RCPT (Rapid Chloride Permeability Test) conducted as per ASTM C 1202 (94).
RCPT is based on the principle that negatively charged chloride ions are attracted to a positive
electrode and consists of measuring the total charge passed through a sample over the six hours
test duration when a direct current potential difference of 60V is applied across the end of the
samples. The quality of material is quantitatively assessed based on the total charge passed
during the test, which is considered to be the measure of the chloride permeability of concrete.
Test results for the resistance to penetration of chloride ions into concrete of 28 and 90 days
after casting, measured in terms of the electric charges passed through the specimens in
Coulombs for M85 grade concrete. It is observed that most of the chloride ion permeability
values fall in the range of low (1000-2000 Coulombs) category. The charge passed through the
M85 grade concrete mixtures are 1840 Coulombs at the age of 28 days and 1120 coulombs at
1. The target strength of 60 MPa in 7 days was achieved with addition of 2.5% micro silica and
1.2% super plasticizer (Conplast SP430) by using cement content of 438.75 kg/m3.
2. It is observed by trail mixes, the admixtures gave more strength and workability to the
concrete. Fly ash dosage of 5-10% by weight of cement shows better results than higher
percentages of fly ash. Super plasticizer Conplast SP430 dosage of 0.9-1.2% shows better
values. Silica fume dosage of less than 5% by weight of cement shows better results than
3. 60 MPa of compressive strength of concrete in 7 days was achieved by use of optimum % (i.e.
2.5%) of silica fume which fills the space between the cement particles and between the
aggregates and the cement particles. However, 88 MPa in 28 days was achieved. So it was
4. Water cement ratio of less than or equal to 0.30 did not yield higher strengths, may be because
5. The split tensile and flexural strength of M85 concrete was increased by age of concrete and
the resultant values are more when compared with the theoretical value 0.7 fck. The flexural
strength results of M85 concrete were more when compare with split tensile strength results
of concrete. However, the performance of the mix designed was satisfactory in terms of
mechanical properties split tensile strength, flexural strength and modulus of elasticity.
6. It is observed that most of the chloride ion permeability values fall in the range of low (1000-
The authors thank to Y. Mahendra, G. Arun Kumar, B. Pallavi, Ch. Snehal and P. Venkatesh,
under graduate students of Civil Engineering, MVGRCE, Vizianagaram for their help in
experimental work.
7. REFERENCES
1. Karthik. D and Doraikkannan. J., “Experimental Investigation of silica fume and steel slag in
3. Harjinder Singh and Shikha Bansal., “Effect of Silica Fume on the Strength of Cement
4. Engr. Gana and Engr. Okoye., “Relevance of High Performance Concrete Applications in
Science, Technology and Innovation (IRJESTI), (ISSN2315-5663) Vol. 4(1) pp. 19-24,
January 2015
advantages for Kurdistan Region, Iraq”, International Journal of Scientific and Engineering
7. Damgir. R. M., “Split Tensile Strength of Fiber Reinforced Concrete Using Silica Fume and
Natural Sand in high performance concrete with silica fume”, International Journal of
11. Vijaya Kishore. K., “Ultra Strength Concrete” International Journal of Emerging trends in
12. Faseyemi Victor Ajileye., “Investigations on Micro Silica (Silica Fume) As Partial Cement
13. Vinayagam. P., “Experimental Investigation on High Performance Concrete Using Silica
Engg. and Appl. Sciences, 2012, Research Paper: Sreenivasulu and Srinivasa Rao, 2012:
Pp.183-185
16. Chandramouli., “RCPT Durability Studies on Glass Fiber Reinforced Concrete”, Journal of
17. Yaqub. M and Imran Bukhari., “Effect of Size of Coarse Aggregate on Compressive Strength
of High Strength Concrete”, 31st Conference on our world in concrete and structures: 16 - 17
18. Sidhu. D. S., “Early Age Behavior of Silica Fume Concrete”, 26th Conference on our world
in concrete and structures: 27 - 28 August 2001, Singapore, Article Online Id: 100026071.
19. IS 383: 1987 Specification for coarse and fine aggregate from natural sources for concrete,
8th Reprint October 1991, Bureau of Indian Standards, and New Delhi.
20. IS 456: 2000 Code of practice for plain and reinforced concrete, 4th Revision, Bureau of
21. IS 516: 1959 Methods of test for strength of concrete, Amendment No. 2, Reprint 1993,
22. IS 5816: 1999 Splitting Tensile Strength of Concrete–Method of Test, Bureau of Indian
23. IS 10262: 2009 Concrete Mix Proportioning Guidelines, Bureau of Indian Standards, New
Delhi.
24. IS 12269: 1987 Specification for 53 grade ordinary Portland cement, Bureau of Indian
25. ASTM C 1202, Electrical Indication of Concrete’s Ability to Resist Chloride Ion Penetration,
Annual Book of American society for Testing Materails, Vol. C04.02, 1993.
7. TABLES AND FIGURES
Values 0.36 95.5 0.35 0.61 0.41 0.12 2.15 0.50 100
Not
Slight/ Not
Result Liquid Brown 7-8 >100°c Applicabl Soluble
Faint Applicable
e
Table 6 Mix Proportions for Mix Designs
Table 7 Fly- Ash Results (by weight of cement) (W/C = 0.34, Cement = 450 kg)
11.25
1 1015.29 874.36 153 2285 33.15
(2.5%)
33.75
2 992.79 874.36 153 2379 49.0
(7.5%)
45
3 981.54 874.36 153 2369 47.9
(10%)
22.5
4 1004.04 874.36 153 2407 53.35
(5%)
67.5
5 959.04 874.36 153 2369 43.32
(15%)
Table 8 Silica Fume Results (by wt of cement) (W/C = 0.40, Cement = 450 kg)
112.5
1 874.71 840.83 180 2381 38.95
(25%)
11.25
6 975.96 840.83 180 2473 52.3
(2.5%)
1.125 (0.25%
2 1026.54 871.7 153 2471 52.5
D)
Compr
Super
Fine Coarse Silica strength
Sl. W/C Water plasticizer Density
aggregate aggregate fume (MPa) for
3
No Ratio (lt) (lt) (kg/m )
(kg) (kg) (kg) 7-days
45 2.25 (0.5%
2 0.34 981.54 874.36 153 2340 38.35
(10%) D)
45
1 450 981.54 874.36 126 27 2320 43.85
(10%)
30
2 600 852.90 751.95 168 36 2576 53.8
(5%)
27.5
3 550 902.65 792.45 154 33 2513 46.5
(5%)
25
4 500 954.83 834.62 140 30 2542 43.1
(5%)
Table 13 Silica Fume +Rapid Hardening Solution Results (W/C = 0.34)
27.5
1 550 902.65 792.45 154 33 2504 53.75
(5%)
25
2 500 954.83 834.62 140 30 2560 51.05
(5%)
22.5
3 450 1004.04 874.36 126 27 2370 49.1
(5%)
Table 14 Silica Fume + Fly Ash + SP + Rapid Hardening Solution Results
(15cm*15cm*15cmsize)
Comp
Wat Fly
Sl. W/C Cement FA CA SF SP R.H.S Density strength
er Ash
No Ratio (kg) (kg) (kg) (kg) lt (lt) Kg/M3 (MPa)
(lt) (kg)
for 7days
22.5
1 0.34 427.5 1026.4 874.2 153 0 (0%) 0 0 8370 52.7
(5%)
11.2 0 1.2
2 0.34 438.1 1026.4 874.2 153 0 8150 61.3
(2.5%) (0%) %
22.5
3 0.34 427.5 1026.4 874.2 126 0 (0%) 0 27 7640 49.7
(5%)
11.2 0
4 0.34 438.7 1026.4 874.2 126 0 27 7700 41.15
(2.5%) (0%)
12.5 0 1.1
5 0.34 487.0 979.83 834.6 140 30 8313 48.7
(2.5%) (0%) %
0 1.2
6 0.34 500.0 979.83 834.6 140 0 (0%) 30 8382 45.15
(0%) %
25 1.0
7 0.34 475.0 979.83 834.6 140 0 (0%) 30 8240 50.95
(5%) %
0 1.2
8 0.34 500.0 979.83 834.6 140 0 (0%) 30 8410 49.8
(0%) %
Table 15 Mix Proportions for Finalized Mixture
50
40
Stress (N/mm2)
30
20
10
0
0 0.0005 0.001 0.0015 0.002 0.0025 0.003 0.0035 0.004 0.0045 0.005
Strain
2000
1500
RCPT
1000
VALUE
(Coulombs)
500
0
28 DAYS 90 DAYS
AGE (Days)