IS 9103 : 1999

(Reaffirmed 2004)
Edition 2.2
(2007-08)

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Indian Standard
C ONCRETE ADMIXTURES SPE CIFI CATION
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( First Reuision )
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@ BIS 2008

BUREAU OF INDIAN STANDARDS

MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 11OOO2

Price Group 7
Cement and Concrete Sectional Committee, CED 2

FOREWORD

This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards, after the
draft fi.nalized by the Cement and Concrete Secbional Committee had been approved by the Civil
Engineering Division Council.
Admixtures are materials added to the concrete before or during its mixing, with a view to
modifying one or more of the properties of concrete in the plastic or hardened state. An important
feature of the majority of admixtures for concrete is that it is difficult to quantitatively evaluate
the behaviour of the concrete under various possible circumstances. Therefore, performance of an
admixture is evaluated by comparing the properties of concrete with the admixture under test
with those of concrete without any admixture or with a reference admixture. This standard lays
down the procedure for such a relative evaluation of admixtures for concrete.
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In recent time there has been a lot of development in the freld of admixtures. Superplasticizers,
both normal and retarding type, constitute a major group of admixtures used by site engineers
now. Superplasticizers help in lowering the water/cement ratio so as to contribute to the 7=
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enhancement of durability. In this first revision of the standard, frrst published in 1979, 11 v

requirements of superplasticizers in detail and methods of determination of flow of concrete of 72

high workability have been added.
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This standard also gives uniformity tests which demonstrate that a particular consignmenl is a.1 n
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similar to material that has previously been submitted to the acceptance test.
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The admixtures covered in this standard are intended mainly for modifuing a single property in
concrete, but some of the admixtures available in the market are ofben capable of modifuing more a-
than one property of the concrete. In addition, an admixture may be used to improve the desirable
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properties of concrete in more than one way. For example, water reducing admixtures ( see 3.4 ) z>
may be used to improve the workability of concrete with the same water and cement contents, to ?a
increase the compressive strength without changing the workability by reduction of the water
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content in the concrete mix or to effect saving in cement content by reduction in both the cement
and water contents in the mix while maintaining the same workability and compressive strength P31
as in the reference concrete. In such cases, the procedure of evaluation of the admixture may have 9x
to be appropriately chosen. This standard also provided for evaluation of admixtures for specific -c
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use with the materials and mix proportions to be used on the work.
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The performance of concrete admixtures including superplasticizers depend upon both the a
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admixtures and the cement and their compatibility, in addition to the concrete mix proportions and za
the environmental conditions in the field. Among the characteristics of the cement, which affect the o
performance of concrete admixtures including superplasticizers are the CBA, SO3 and alkalicontenls, -l
nature of sulphates, and the frneness. The ambient temperature and humidity conditions influence C
the performance of set-controlling admixtures and affect the retention of enhanced workability
(slump loss) when water-reducing admixtures and superplasticizers are used. While no
generalisation ofthese effects is possible, it is nevertheless necessary to evaluate concrete admixtures
for specific use with the concrete-making materials and mix proportions to be used on bhe work, under
fr.eld conditions. This standard also provides for such specifrc evaluation of an admixture, in addition
to the general evaluation for conformity to the requirements of this standard.
The requirements of integral waterproofrng admixtures are covered in IS 2645 : 1975
'Specification for integral cement waterproofrng compounds ( /irst revision)'.
This edition 2.2 incorporates Amendment No. 1 (January 2003) andAmendment No. 2 (August 2007).
Side bar indicates modifrcation of the text as the result of incorporation of the amendments.
For the purpose of deciding whether a particular requirement of this standard is complied with,
the frnal value, observed or calculated, expressing the result ofa test or analysis, shall be rounded
off in accordance with IS 2 : 1960 'Rules for rounding off numerical values (reuised )'- The number
of signifrcant places retained in the rounded off value should be the same as that of the specified
value in this standard.

Indian Stan dard
C ONCRETE ADMIXTURES
( First Reuision" )
1 SCOPE
1.1 This standard covers the chemical
and air-entraining admixtures including
superplasticizers, solid or liquid or emulsion, to
be added to cement concrete at the time of
mixing so as to achieve the desired property in
concrete, in the plastic or hardened state.
1.2 The different types of admixtures covered
in this standard are as follows:
a) Accelerating admixtures,
b) Retarding Admixtures,
c) Water-reducing admixtures,
d) Air-entraining admixtures, and
e) Superplasticizing admixtures.
1.3 The chloride content in the admixture shallbe
declared by the manufacturer. Superplasticizers
are expected to be chloride free.
1.3.1 Admixtures that contain relatively large
amounts of chloride may accelerate corrosion of
prestressing steel. Where corrosion of such
steel is of major concern, compliance with the
requirement of this specificalion does not
constitute assurance of acceptability of the
admixture for use in prestressed concrete. In
case of reinforced concrete, to minimize the
chances of deterioration of concrete, lhe total
chloride content in the concrete should be
limited as specified in IS 456.
2 NORMATIVE REFERENCES
The Indian Standards listed in Annex A
contain provisions which, through reference in
this bext, constitute provision of this standard.
At the time of publication the edibions indicated
were valid. All standards are subject to
revision, and parties to agreement based on
this standard are encouraged to investigate the
possibility of applying the most recenb edition
of the standards indicated in Annex A.
3 TERMINOLOGY
3.0 For the purpose of this standard, the
following defrnitions shall apply.
3.1 Adrnixtures
A material other than water, aggregates, and
hydraulic cement and additives like pozzolana
or slag and frbre reinforcement used as an
ingredient of concrete or mortar and added to
the batch immediately before or during its
mixing bo modifr one or more of the properties
ofconcrete in the plastic or hardened state.
IS 9103 : 1999
SPE CIFI CATI ON
-
3.2 Accelerating Adrnixture or Accelerator
An admixture when added to concrete, mortar
or grout, increases the rate of hydration of a
hydraulic cement, shortens the time of set, or
increases the rate of hardenins or strensth
development.
3.3Retarding Adrrrixture or Retarder
An admixture which delays the sehting of
cement paste, and hence of mixtures, such as \a
mortar or concrete containing cement. oc
3.4 Water Reducing Adrnixture or -an
Workability Aid :e
An admixture which either increases ;<
workability of freshly mixed mortar or concrete
without increasing water content or maintains rnx
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workability with a reduced amount of water. aE
3. 5 Air-Entrainin g Adrnixtures =r
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An admixture for concrete or mortar which
causes air to be incorporated in the form of
minute bubbles in the concrebe or mortar z>
during mixing, usually to increase workability
and resistance to freezing and bhawing and ?o
disruptive action of de-icing salts. =a
3. 6 Superplasticizing Adrnixtures O=
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An admixture for mortar or concrete which <F
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imparts very high workability or allows a large
decrease in water content for a given workability.
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3. 7 Retarding Superplasticizing Admixture zq
Superplasticizing admixture that imparts c
prolonged workabilily retention and retards --
settrng. 7
4 REQUIREMENTS FOR ADMD(TURES
Concrete made wibh admixtures when
compared with identical concrete made without
the admixture in accordance with 7 and 8 shall
conform lo the requirements appropriate to the
type of admixture given i.n Table 1A and Table
18, except in bhe case of air-enbraining
admixture. In the case of air-entraining
admixtures, a reference admixture of approved
quality shall be used in the control concrete to
entrain identical amount of air.
NOTE
-
Ifrequired by bhe purchaser, the concrete wilh
air-entraining admixture may be tested for resistance to
freezing and thawing in accordance with bhe procedure
given in Annex B, in such case the relativc durabi-lity
factor of the concrete with admirture under test shall be
not less bhan 80.
IS 9103 : 1999

Table 1A Physical Requireurents

( Clause 4)

SI Requirements Accele- Retarding Water Air-Entrain- Superplasticizing Test

No. rating Adrnixture Reducing ing Adrrixture Admixture(forWater- Ref
Admixture Admixture Reduced Concrete Mix)

Normal RetardingType
(r) (2) (3) (4) (D,l (6) (7) (8) (s)

r) Water content, 95 80 80 7.2.5

percent of control
sample, Mot
ri) Slump Not more than 15 mm 7.2.1
below that of the
control nix concrete

iii) Ti-me of setting, 7.2.3

allowable deviation \a
from control sanple
hours:
z=
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Initial =v
Max -3 +3 +l + 1.5 +4 t<
Min -1 +l +1 do
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+3 +l +1.5 +3 a:
Max -2 E:1
Min -1 -t a'
c=
rv) Compressive strength,
percent of control z>
sample, Min
1 day 140 ?o
3 days r25 90 ll0 90 L25 t25 E9
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7 days 100 90 1r0 90 L25 t25
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28 days 100 90 ll0 90 115 ll5 <F
6 months 90 90 100 90 100 100
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I year 90 90 100 90 100 100
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v) Flexural strength, 8.2.2 z
percent of control a
sample, Mirr

3 days 110 90 100 90 110 110

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7 days 100 90 100 90 100 100
28 days 90 90 100 90 100 100

vi) Length change, 8.2.3

percent increase over
control sample, Mox
28 days 0.010 0.010 0.010 0.010 0.010 0-010
6 months 0.0 r0 0.010 0-010 0.010 0.0r0 0.010
1 year 0.010 0.010 0.010 0.010 0.010 0.010

vii) !,lgsding, percent J 5 o J 5 5 7.2.4

increase over control
sample, Mo.r

ix) Air content (%) l5

Mo-x, over control
 IS 9103 : 1999

Table 18 Requirernents for High Workability Test Mix

( Clause 4)
Sl No. Requirements Type of Superplasticizing Admixture Test Reference
Normal Retarding Type
(2) (3) (4) (5)
l"low 5I0 mm - 620 mm 510 rnm - (i20 mm 72.1 1

Loss of workability on st:rnding At 45 min thc slump sh;rll be Ar 2 h lhc slump shlll be i2.1 2
not lcss th:rn that of control not less than thll ofcontrol
mrx concrete at 15 min mrx cuncretc ;rt 15 mrn
rir) lllinimurncompressive strength,
pcrccnt ofcontrol mix concrete
7 days 90 90
28 days 90 90
6 montbs 90 90
I year 90 90

5 METHOD OF SAMPLING OF 6.1.1 Materials for Tests for Specific Use \q

ADMD(TURE FOR TEST oc
When an admixture is required bo be tested for
5.1 Liquid Adrnixture a specifrc work, test samples shall be prepared -cn
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Liquid admixture shall be agitated thoroughly using materials proposed bo be used on the
immediately prior to sampling. Grab work. 5<
(individual) samples taken for testing shall 6.1.2 Materials for Tests for General Eualuatiotr. a9
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represent noh more than I 000 litres of of Admirture @a
admixture and shall have a volume of at least qE
one litre. A minimum of four grab samples shall When an admixture is required to be tested for
be taken. Composite samples shall be prepared general evaluation, the requirements of 6'

by thoroughly mixing the grab samples selected materials shall be as follows:

and the resultanb mixture sampled to provide a) Cement The cement shall be ordinary 2>
at least 4 litres for quality tests. Portland- cement conforming to IS 269 or
5.1.1 Admixture from bulk storage tanks shall IS 8112 or IS 12269. ?o
be sampled equally from the upper, b) Aggregate The coarse and hne aggre-
intermediate, and lower levels by means of gates shall- conform to the requirements -n
drain cocks in the sides of tanks or a weighed given in IS 383. While the hne aggregate >a
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sampling bottle fihted with a stopper bhat can shall conform to the grading of Zone II, <Fz
be removed after the bottle is lowered to the the coarse aggregate shall be graded -o
desired depth. aggregate of 20 mm nominal maximum a
size, with the gradings conforming to o
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5.2 Non-liquid Adrnixture IS 383 in bobh the cases. c
Grab samples taken for lests shall represent
not more than 2 tonnes of admixture and shall 6.2 Preparation of Concrete c=
weigh at least 1 kg. A minimum of 4 grab Except in the case of air-entraining
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6.2.1
samples shall be taken and composite sample
admixtures, the concrete mix shall be prepared
shall be prepared by thoroughly mixing the four
grab samples. The resultant mixture sampled both with and without admixture. the lalter
shall provide ah Ieast 2.5 kg from bhe composite
being treated as the reference or control
concrete mixture. In the case of air-entraining
sample. Grab samples shall be taken from admixtures, reference admixture shall be used
different locations well distributed throughout in control concrete (see 4).
[he quantity to be represented.
5.2.1 Samples of packed admixtures shall be 6.2.2 The admixture shall be used in
obtained in the same manner as described in accordancewith the recommendations of the
IS 3535. manufacturer. When an admixture is to be
tested specifrcally for air-entrainment, it shall
5.2.2 Samples shall be packed in moisture- be used in such a quantiby that it produces air
proof, airtight containers. conbent in the range of 3.5 to 7 percent.
6 PREPARATION OF TEST SAMPLES NOTE The manufacturer shall give detailed
-
instructions on bhe cotrect use of the :rdmixbure for bhe
6.1 Materials purpose indicated.
IS 9103 : 1999

6.2.3 Proportioning of Concrete of mixing, as the relative advantage of some water-

reducing admrxtures may decrease with time after
6.2.3.1 Proportioning concrete for tests fo, mD(rnE-
specific use 7.2.1.1The flow of freshly mixed
The concrete mix shall be proportioned to have superplasticized concrete of high workability
the cement content specified for the work and shall be determined accordins to the method
to meeb the stipulated workability and strength given in Annex C.
requirements. In case of air-entrained concrete, 7.2.L.2 Loss of worhability otr. stantding
the air content specified for the work shall be The slump of high workability concrete mixes
used. If the maximum size of coarse aggregate shall be determined at 45 min and at 2 h, using
is greater than 20 mm, the concrete mix shall normal type and retarding type
be wet-screened over 20 mm IS Sieve before superplasticizers, respectively after the
test. following operations.
6.2-3.2 Proportiotr,ittg concrete fo, tests fo, Aft,er mixing the concrete mixes shall be
general evaluation covered to prevent loss ofwater by evaporation
The concrete mix may be designed according to and kept at a temperature of 27 * 2"C and
any accepted method of mix design, to meet the relative humidity of 65 + 5 percent. At 45 min, ,aa
following requirements: the concrete shall be remixed by hand using a OC
shovel just enough to counteract any bleeding
a) The cement content of the mix shall be or segregation and slump of concrete shall be -an
307 + 3 kg/m3, determined. The tested concrete shall be v
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b) The concrete mix shall have a slump of 50 discarded and the remaining concrete shall be 72
+ l0 mm or a compaction factor of 0.85 to covered and tested at 2}:', after mixing by hand
0.90 to facilitate compaction by using a shovel. Q9
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hand-rodding, @q
7.2.2 Test for Air-content
a;
c) The concrete mix shall be compacted Air-content of freshly mixed concrete shall be
according to the requirements given in a-
determined by the pressure method given in
IS 516, and
IS 1199.
d) In case of air-entrained concrete an air 2>
content of6 percent shall be used. 7.2.3 Test for Time of Setting ^-
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Time of setting, initial and frnal, shall be
6.2.3.3 Samples shall be thoroughly mixed as determined as given in IS 8142.
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recommended by the manufacturer to ensure
uniformity before testing. 7.2.4 Test for Bleeding -ll
Bleeding shall be computed at a percentage of 2c
6.2.4 The concrete shall be made in a -C
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the net amount of mixing water in the concreie. 'z
mechanical power driven mixer in accordance The neb mixing water is the water in excess of r-
with the procedure specified in IS 516. that present as absorbed water in the O
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7SAMPLING AND TESTING OF FRESH aggregate. Absorbed water in the aggregate za
CONCRETE shall be determined as given in IS 2386 c
(Part 3). The test shall be carried out in j
T.l Sampling accordance with the details given in Annex D. C
7
Sampling of fresh
concrete shall be done 7.2.5 Test for Water Content
according to the requirements given in IS 1199. 7.2.5.L The water-cement ratio of bhe concrete
7.2 Methods of Tests shall be determined to the nearest 0.001, as
follows:
Samples of freshly mixed concrete from at least a) Net water content of the batch shall be
three separate batches for each condition of computed by determining the absorption
concrete shall be analysed for the tests water of aggregabe as given in IS 2386
described in 7.2.1 to 7.2.5. (Part 3).
7.2.t Test for Worhability b) Mass of cement per unit volume of
concrete shall be computed as given in
The workability of freshly mixed concrete in IS 1199. and
terms of slump or compaction factor shall be c) Water-cement ratio shall be determined
determined according to method given in by dividing the net mass of water by the
IS 1199. mass of cement in batch.
NOTE In some cases, it may also be worthwhile to
- the workability of fresh concrete not sooner
determine 7.2.5.2The relative water content for the
than 15 min and not laber bhan 20 min after complelion concrete containing admixture shall be
 IS 9103 : 1999
expressed as a percentage of the water content 9 UNIFORMITY TEST AND
of the reference concrete mixture. This shall be REQUIREMENTS
computed by dividing the average water Any batch of admixture shall have the same
content ofall batches ofconcrete by the average physical state and composition, as that of the
water content of the reference concrete and admixture tested for accepbance. To check this
multiplying the quotient by 100.
uniformity of composition, a representative
8 TESTING OF HARDENED CONCRETE sample of bhe batch shall be hested and shall
sabisfy hhe requirements given in Table 2.
8.1 Preparing Test Specirnens
10MARKING
The test specimens shall be prepared as given
in IS 516. 10.1 Each conbainer of admixture shall be
legibly marked with the following informabion:
8.2 Method of Testing
a) Identifrcation of the source of
Specimens for tests on hardened concrete shall manufacture,
be prepared from at least three separate b) Year and date of manufacture,
batches for concrete with and without the c) Type of admixture, thal is, whether
admixture. The specimen shall be analysed for accelerating, retarding, waber reducing,
the requirements described in 8.2.1 to E.2.3. air-entraining, normal superplasticizing \a
CC
8.2-l Test for Compressiue Strength or retarding superplasticizing,
d) Batch Number, and 1=
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At least three specimens shall be tested for e) Chloride ion content. :v
each type of concrebe and each age of testing. :<
Compressive strength shall be debermined as 10.2 Additional Inforrnation
given in IS 5f6. The following information shall be provided by av
cnT
8.2.2 Test for Flexural Strength the manufacturer in a printed form f!o
a) Physical state (that is, liquid or solid) and aE
At least bhree specimens shall be tested for colour; w<
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each type of concrete and each age of testing. a
Flexural sbrength shall be computed as given in b) Composition;
IS 516. i) Generic type of main active constibuenl(s), z>
=an
for example, lignosulphonate, organrc
8.2.3 Test fo, Length Change (Drying hydroxycarboxylic acid or carbohydrate; <:
Sh.rinhage) ii) Dry material content; 7a
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Changes in length on drying and wetting shall iii) Ash content;
be debermined as given in IS 1199. The iv) Relative density of liquid admixture; za
moist-curing period, including the period in v) Chloride ion conlent, expressed as a r--
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moulds shall be 14 davs. percenbage by mass of total admixture; z
-
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Table 2 Uniforrnity Tests and Requirernents a
c
( Clause I )
za
Sl No. Property Requirement Reference Test F
i
C
(1) (2) (3) (4)

r) Dry material conLent Annex E

a) For liquid admixture 0.91-rT<DMC< 105T,

b) For solid :rdmixture where
T manufacturcr's staLod valve, in percenb by mass
DMC - test results, in percent by mass
u) Ash content 0.95T<AC< 1.05T, do

where
T- manufacturer's state d v;rlve, in percent by mass
AC test results in perccnt by mass
rii) Relative density Within 0-02 of the valuc statcd by Lhc manufacturer do

iv) Chloride ion content Within l0 percent r.rf the value or wibhin 0.2 percent do
whichevcr is greatcr as stated by the manu{acturer
v) pH 6, Mitt do

NOTE Uniformity requirements frrr ash content is not applicable to accelerating admixturc which may contain more
than I -percent chloride content.
IS 9103 : 1999

c) The chloride ion content relative to the
cement mass contributed by the
recommended dosage or dosages expressed
as percentage by mass of chloride ion;
d) Recommended storage conditions,
maximum storage time before use and
necessary safety precautions, for
example, toxic or corrosive;
e) Any known incompatibility with other
admixture or with certain types of cement
etc;
f) The recommended dosage or dosages;
g) The effect of underdosage
overdosages; and
h) Expiry date.
10.3 Infonrration Concerning the
Adrnixture Acceptance Test
The following information shall be provided by
the manufacturer in a printed form, if
requested:
a) The source of cement (works of
manufacture) and aggregates (quarry or
pit or for material dredged from seas,
estuaries or river the locality);
b) The quantity of admixture used in the
test mix concretes:
c) The values of slump, w/c ratio and cement
content for each batch of the control and
test mix concrebes; and
d) The air content of each batch of the
control and test mix concrete.
11 BIS Certifrcation Marking
and The product may also be marked with Standard
Mark.
1l.l The use of Standard Mark is governed by
the provisions of Bureau of Indian Standards
Act, 1986 and the Rules and Regulations made
11a
thereunder. The details of conditions under OC
which the licence for the use of Standard Mark
may be granted to manufacturers or producers -cf,
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may be obtained from bhe Bureau of Indian
Standards. <- '(

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ANNEX A
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( Clause 2 )
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LIST OF REFERRED INDIAN STANDARDS 2c
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15 No. TitIe 15 No. TitIe c-
a
269: 1989 for 33 grade
Specifrcation 3b3b 1966 Methods of sampling hydraulic (]
ordinary Portland cement cement ( first reuision ) z
q
(fourth reuision ) o
383: 1970 Specifrcation for coarse and fine 6925 1973 Methods of test for -
aggregates from natural sources determination of water soluble
for concrete (second reuision ) chlorides in concrete
456: 1978 Code of practice for plain and admixtures
reinforced concrebe (third gllz 1989 for 43 grade
Specifrcation
reulslon
516: 1959
,
Method of test for strength of
ordinary Portland cement
(first reuision )
concrete
1199: 1959 Methods of sampling and gL42 r976 Methods of test for determining
analysis ofconcrete setting time of concrete
2386 Methods of test of aggregates penetration resistance
(Part 3) : 1963 for concrete : Part 3 Soecifrc
gravity, density, voids, 12269:1987 Specifrcation for 53 grade
absorption and bulking ordinary Portland cement
 IS 9103 : 1999

ANNEX B
( Note under Clause 4)
TEST FOR RESISTANCE OF CONCRETE AGAINST FREEZING AND THAWING
B-O TEST FOR RESISTANCE OF ru1 = fundamental bransverse frequency
CONCRETE AGAINST FREEZING AND ab zero cycle of freezing and
THAWING thawing; and
B-l The freezing and thawing cycle shall ru2 = fundamental bransverse frequency
consist of albernately lowering the temperature after C cycle of freezing and
<lf t,he specimens from 4 + l'C bo -18 + 2"C and thawing.
raising it from -18 + 2'C to 4 + l"C in not less The relative durabilitv factor shall be
lhan 2 h nor more than 5 h. The freezing and calculated as follows:
thawing can take place either in (i) water, or (ii)
freezing in air and thawing in water. DF (or DFt) = PN/300
B-2 The test for fundamental transverse RDF=DFIDF,xlOO
frequency shall be conducted on concrete prism where \q
specimens (100 mm x 100 mm x 400 mm or DF = durability factor of the concrebe oc
150 mm x 150 mm x 600 mm) or on concrebe containing the admixture under zl
cylinder specimens (150 mm in dia x 300 mm test, a.n
d-
length). The lest shall commence at the age of DFt = durability facbor of the concrete
l4 days (water-curing till then) by electro- containing the reference t<
r- tD
dynamic method in accordance with IS 516. admixture,
rnn
The relative dynamic modulus of elasticity P = relative dynamic modulus of @a
shall be calculated as follows: elasticity in percentage of the qP
dynamic modulus of elasticity at
P"= nr2lnr2 x loo zero cycle (values of P will be 60 or
=l
a-
greater), and
where :afl
N = number of cycles at which P z>
P. = .elative dynamic modulus of reaches 60 percent, or 300 if P ?-l
elasticity (percent), after C cycles does nob reach 60 percent prior to ?o
of freezing and thawing; the end of the best (300 cycles). =a
Fl-q
2c
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ANNEX C
c
=
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( Clause 7.2.7.1)

METHOD OF DETERMINATION OF FLOW OF CONCRETE OF HIGH WORKABILITY

C-0 This method covers determination of the Diameter of lhe base : 200a2mm
flow of fresh mixed superplasbicized concrete of Diameter of bop : 130*2mm
high workability. Height : 200*2mm
The slump cone shall be provided with two
C-l APPARATUS mebal foot pieces at the bottom and two handles
at the top.
C-1.1 The Slurnp Cone
C-1.2 TarnpingBar
The slump cone for receiving the freshly mixed The tamping bar shall be made of hardwood
concrete shall consist of a frustrum of cone of and having a 40 mm x 40 mm section of length
minimum thickness of 1.5 mm metal, wibh the 200 mm, with a circular section to form a
following internal dimensions: handle bo bhe bar.
IS 9103 : 1999

C-1.3 Flow Table Apparatus similar to that shown in Fig. 1A shall be

The flow table apparatus shall be constructed
in accordance with Fig. 1A and 18. FIow table
top shall be constructed from a flat metal plate
of minimum thickness 1.5 mm. The top shall
have a plan area of 700 mm x 700 mm and a
flabness of within 1.5 mm. The centre of the
table shall be scribed with a cross, the lines of
which run parallel to and out to the edges of the
plate, and with a central circle 200 mm in
diameter. The under surface of the plate shall
be reinforced in order to prevent distortion of
the flat surface. The front of the flow table top
shall be provided with a Mting handle as shown
in Fig. 1. The total mass of the flow table top
shall be 16 + I kg.
The flow table top shall be hinged to a base
frame using externally mounted hinges in such
a way that no aggregate can become trapped
easily between the hinges or hinged surfaces.
The front of the base frame shall extend a
provided on each side of the table so that the
lower front edge of the table can only be lifted
40+1mm.
The lower front edge of the flow table top shall
be provided with two hard rigid stops which
transfer the load to the base frame. The base
frame shall be so construc[ed thab this load is
then transferred directly to the surface on
which the flow table is placed so that there is
minimal tendance for the flow table top to
bounce when allowed to fall.
C-1.4 Accessory Apparatus
C-1.4.r Mould
The mould shall be made of a metal readily not
attacked by cement paste or liable to rust and of \a
minimum thickness 1.5 mm. The interior of the
mould shall be smooth and free from projections,
such as protruding rivets, and shall be free from -cn
dents. The mould shall be in the form of a hollow =v

minimum 120 mm beyond the flow table top in frustrum of a cone having the internal 3:
order to provide a top board. An upper stop dimensions as shown in Fis. 2. The base q9
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METAL PLATE @<
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EXTERNAL
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LIFTING HAN D LE

BOARD

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All dinensions in millimetres.
Frc. l FLow T.q.slo
 IS 9103 : 1999

AII dimcnsrons in mrllimetrcs.

Frc. 3 T,,urprNG BAR

All dimcnsrons in millimetres.

table-top and inner surface of the mould shall
Frc. 2 CoNcRETE MoULD be wiped with a damp cloth. The slump cone is
and the top shall be open and parallel to each placed centrally on the hable and to be held in
other and at right angles to the axis ofthe cone. position by standing on the bwo foot pieces. The
The mould shall be provided with two metal foot slump cone is to be hlled with concrete in bwo \a
pieces at the bottom and bwo handles above [hem. equal layers, each layer tamped lightly 10 cc
times with the wooden tamping bar. After 1=
C-1.4.2 Tamping Bar filling the mould, the concrebe is to be struck off -F
:v
The hamping bar shall be made of a suitable flush with the upper edge of the slump cone and
hardwood and having dimensions as shown rn the free area of bhe table-top cleaned off. f-E
Fie. 3. @9
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Half a minute after striking off the concrete, 6A
C-2 SAMPLING the cone shall be slowly raised vertically by the q*
C-2.1The sample of freshly mixed concrete handles. After this, the table-top raised by the
shall be obtained in accordance with the handle and allowed to fall 15 times in 15 s. The
=l
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provisions given in IS 1199. concrete spreads itself out. The diameter of the
concrebe spread shall then be measured in two 2>
C-3 PROCEDURE
directions, parallel to the table edges. The
The flow table shall be level and properly arithmetic mean of the two diamebers shall be <=
supported. Before commencing the test, the the measurement of flow in millimetres.
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ANNEX D -a
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METHOD OF TEST FOR BLEEDING OF CONCRETE
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D-0 This method covers determination of the D-1.2 Tamping Bar C

relabive quantity of mixing water that will

bleed from a sample of freshfu mixed concrete. The tamping bar shall be a round-ended
D-lAPPARATUS
D-l.1 Measure
A cylindrical container of approximabely 0.01 m3
capacity, having an inside diameter of 250 mm
and inside heighb of 280 mm. The container shall
be made of metal of minimum thickness of 4 mm
and shall be externally reinforced around bhe top
with metal band 38 mm wide and 4 mm thick.
The inside shall be smooth and free from
corrosion, coating, or lubricants. Suitable
handles should be provided, properly welded on
the outer surface of the container, on the
opposite sides in centre, so as to enable
Iifting/handling of the container with concrete.
steel
bar of 16 mm diameter and 600 mm lensth.
D-l.3 Pipette
A pipette for drawing off free water from the
surface of the test specimens.
D-1.4 Graduated Jar
A graduated jar of 100 cm3 capacity.
D-2 SAMPLING
The sample of freshly mixed concrete shall be
obtained in accordance with the provisions
given in IS 1199 except when small batches are
made under laboratory conditions.
IS 9103 : 1999

D-3 PROCEDURE and covered with a lid. Water accumulated at

D-3.1 Compacting the top shall be drawn off by means of a pipette,
at 10 min intervals during the frrst 40 min and
The container shall be filled with concrete as at 30 min intervals subsequently till bleeding
soon as practicable after mixing to a height of ceases. To facilitate collection of bleeding
250 + 3 mm. The concrete shall be frlled into the water, the specimen may be tilted by placing a
measure in layers approximately 50 mm deep 50-mm block under one side of the measure
and each layer shall be compacted by hand. during collection of water. The water shall be
D-3.1.1 Compactitr.g by Hand transferred to graduated jar and accumulated
When compacting by hand, tamping with the quantity of water shall be recorded after each
tamping bar shall be distributed in a uniform transfer-
manner over the cross-section of the measure. D-4 CALCUI.ATION
The number of strokes per layer required to Accumulated bleeding water expressed as a
produce the specifred condition will vary percentage of the net mixing water shall be
according to the type ofconcrete, but in no case calculated as follows:
shall the concrete be subjected to le-ss than 60
strokes per layer for the 0.01 m" measure. vw;<
Then, the top surface of the concrete shall be
Bleeding water percentage = 100
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-w" oc
levelled to a reasonably smooth surface by a
minimum amount of trowelling. zt-
where im- rri
D-3.2 The test specimen shall be kept at a
temperature of 27+2"C. Immediately after V* = total mass of the bleeding water, kg; 72
trowelling the surface of test specimens the w = net mass of water in the batch, kg;
time as well as the mass, of the cylinder and its W = total mass of the batch, kg; and rnn
contents shall be recorded. The container shall l!a
be kept on a level surface free from vibration s = the mass of sample, kg. a;
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( Clause IO.L ) r-C
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CIIARACTERISTIC PROPERTIES OF ADMD(TURE r-
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E-l DRY MATERIA], CONTENT temperature. Stopper the weighing bottle and z6
The dry material content in the liquid or weigh to nearest 0.001 g. Again place the bottle
non-liquid samples shall be determined and stopper in the oven for one hour and repeat
the drying and the weighing etc. The weight c
=
according to the following procedures.
should become constant.
E-1.1 Liquid Adrnixture
Calculation:
Place 25 to 30 g of preheated, completely dry
sand in a wide mouth glass weighing bottle (60
Find the weight of sample and the dried
residue.
mm dia, 30 mm height) provided with ground
glass stopper. Place the bottle with sand and Weight of bottle and sand = W's.
stopper in the electric oven and dry for 17 + Ll4 Weight of bottle, sand and = Wz
h at 105 + 2"C. (The period of drying may be sample
shortened if sand is already dry.) Transfer the
bottle with stopper to a desiccator and allow to Weight of sample = Wz- Wt
cool to room temperature and weigh nearest to Weight of bottle, sand and = V[/s
0.001 g. Remove the stopper and with the help dried residue
of a pipette evenly distribute 4 ml of the liquid
Weight of dried residue = Ws - Wt
over the sand. Insert the stopper and place the
bottle and stopper in the oven. Dry for 17 + ll4
h at 105 + 2'C. At the end of bhe drying period Percent residue on drvins = 5: 13 t roo
transfer to a desiccator, cool to room W, - W,

10
 IS 9103 : 1999

E-1.2 Non-Liquid Adrnixture Weight of crucible, lid and ash = Ws

Place about 3 g of the non-liquid sample into an
already weighed dried tared glass stoppered Ash content
weighing bottle to bhe nearest 0.001 g. Remove
bhe stopper and immediately place both stopper
and bottle in the drying oven. Dry for 17 + ll4h E.3 REI.ATIVE DENSITY OF LIQUID
at 105 r 2"C. At Lhe end of lhe drying period ADMD(TURE
transfer the bottle and stopper to a desiccator, E-3.1 Apparatus
cool ho room temperature, stopper the bottle
and weigh to nearest 0.001 g. Calculate as Following apparatus shall be used:
above in E-1.1. a) Constant temperature bath
b) Hydrometer, and
E-2 ASH CONTEI{T
c) Measuring cylinder.
The ash content which gives an indication of
Place about 400 ml of admixture in a 500-ml
inorganic constituents, is determined by graduated cylinder avoiding the formabion of
igniling the admixture at 600"C to remove any
air bubbles in the liquid. Allow bhe temperabure
organic material. Place, accurately weighed to
the nearest 0.00f g, about 1 g of the sample to a
of the liquid bo be 20 + 5"C. Hold the
temperature of the stem and insert ib into the \a
clean pre-ignited and accurately weighed silica cc
or porcelain crucible. Then place the crucible liquid in the cylinder. Insert the hydrometer
over a sbeam water bath or an air oven, at 90oC
into the cylinder in such a way that it floats -r
free and does not touch the side ofthe cylinder. :e
to remove the liquid portion by evaporation. Release the hydrometer when approximately in
Finally transfer bhe crucible with its solid ;<
contents to a muffle furnace at room the equilibrium position. When it has reached
the equilibrium read the scale at the bottom of
temperature and heab gradually so that the F',1 I
the meniscus for transparent liquids or where CDO
temperature reaches 300'C in t h and 600"C in
a further 2 to 3 h period. Maintain the the meniscus merges with the stem of the aP
hydromeber for opaque liquids to report the =,
w<
temperature of the furnace at 600 + 25"C for 16
relative density.
bo 24 h. Remove the crucible from the furnace,
cool, coveredwith its lid in the desiccator. After E-4 CHLORIDE ION CONCENTRATION z>
cooling for 30 min, weigh the crucible plus lid The chloride ion contenb in an admixture shall 7-
and contents to the nearest 0.001 g.
be determined as given in IS 6925. ?-
Calculate the ash content in the original mass =q
of the superplasticizer: E-5pH
Weight of crucible and lid = The hydrogen ion concentration represented by 2o
r-C
Wl
pH value of the liquid superplasticizer shall be <vz
Weight of crucible, lid and = Wz determined wibh the help of a suitable pH -
sample meter. a
a
c
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=
C
=

l1
IS 9103 : 1999

ANND( F
(Foreword)
COMMITTEE COMPOSITION
Cement and Concrete Sectional Committee, CED 2
Chairrnart
DR H. C. VISVESVARYA
Chandrika, 63-64 East Park Road, Malleswaram, Bangalore 560003

Members Represenlittg

SHRI H. BH T|.{OITARYA Orissa Cement Limited, New Delhi

SHRI G. R. BHARTIKAR B. G. Shirke & Co, Pune
DRA. K. CHATTE&IEE The Associated Cement Companies Ltd, Mumbai
SERr S. H- SUBR3MANIAN ( Allernate)
CHIEF ENGINEER (DESIGN) Central Public Works Department, New Delhi
SU?ERINTENDING ENGINEER (S&S) ( AITeTnaIe ) 41r,
CHIEF ENGINEER, NAVAGAM DAM Sardar Sarovar Nirman Nigam Ltd, Gandhinagar
( AIIeTnaIe)
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SUPERINTENDING ENGINEER, QCC rtrt
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CHTEF E NGINEER (RESEARCH-cUM-DIREcToR) Irrigation and Power Research Institute, Amritsar
RESEARCH OFF'ICER CONCRETE TECHNOLOGY ( AITeTn,aIe \
72
DIREcToR A. P. Engineering Research Laboratories, Hytlerabad a9
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JOINT DIREcToR ( Altenr,ate) <c
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DrREcroR (CMDD) (N&W) Central Water Commission, New Delhi
DEpuTy DIRECToR (CMDD) (NW&S) (Alternote) 8o
SHRI K. H. GANGWAI Hyderabad Industries Ltd, Hyderabad
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SHRI V. PATTABHI ( Altern ate )

SHRI V. K. GHANEIiAR Structural Engineering Research Centre (CSIR), Ghaziabad

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SHRI S. GoPINATH The India Cements Ltd, Chennar
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SHRr R. T.ALtrLAKARAN ( Altentale )
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SHRI S. K- GUITA THAKURTA Gannon Dunkerley & Co Ltd, Mumbai -c
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SIiRI S. P. SANKARANARAY.{NAN ( AlterDote
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)

SHRI N. S. BHAL Central Building Research Institute (CSIR), Roorkee

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DR IRSHAD MAsooD ( Allernate ) za
DR IRSHA.D MAsooD Cement Corporation of India, New Delhi
SIrRI N. C. JttN ( ALtentate )
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JOINT DIRECTOR STANDARDS (B&S) (CB-I) Research, Designs and Standards Organization (Ministry of
Railways), Lucknow
JoINr DIRECToR STANDARDS (B&S) (CB-II) ( Altertnte)
SHRI N. G. JoSHI Indian Hume Pipes Co Ltd, Mumbai
SHRI P. D. KELKAR (Alternale)
SHRI D. K. KANUNGo National Test House, Calcutta
SHRI B. R. MEENA ( Alternale )

SHRI P. KRISHNAMT]RTHY Larsen and Toubro Limited, Mumbai

SHRI S. CHAIGAV !&"trr'{ ( Alter nale )

DRA. G. MA-DHAV.{ RAo Structural Engineering Research Centre (CSIR), Chennar

SHRI K. Ma,r,tr ( Alterrwte)
CIL{RMAN-oL\4-I\I4NAGING DrREcroR Hospital Services Consultancy Corporation (India) Ltd, New Delhi
SHRI J. SARUP ( Alternale )

( Conlhtued on page 13 )

L2
 IS 9103 : 1999
( Con linued frotn poge 12 )

Mentbers Represen lin g

SHRI PRAFUU-A KUNL{R Ministry of Transport, Department of Surface Transport, Roads
Wing, New Delhi
SHRI P. P. NAIR ( Allerrrole )
I[ r.]M R],1 R S Ec RI:T.,\RY Centr;rl Board of Irrig;rtion :rnd Power, Ncw Dclhi
DIRr.rcroR (CIVIL) ( ALternale)
S]IRI SIIDE.SII DIIINLAN, CE Engineer-in-Ohiefs Branch, Army Hc:rdqulrtcrs, Ncw Dclhr
SlrRr DrNEsrr STKAND, ADDrTroNAr, CE ( AlLe.nnte )
SIIRI Y R. PIIULL Centr:rl Road Rescarch lnstitute (CSIR). New l)elhi
SHRI S. S. SEEHRA ( Alternate )
SHRI Y- R. PITUI Indian Roads Congress, New l)elhi
SHRI A. K. SHARMA (Alternate)
DR C. R,{JKUMAR National Council for Cement and Building Materials, Ncw Delhi
DR K. MOI{AN ( Alternate)
SHRI G. RAMDAS f)irectorate General ofSupplies and Disposals, New Delhi \q
OC
SrIRr R. C. SHART,L,\ (Altertnte)
SITR] S, A. REDDI Gammon India [.td, Mumbai -cn
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REPRESENTATryE Builder's Association of India, Munb:ri
SHRI J. S. SANGANERIA Geological Survey of India, Calcutta
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SI{RI L. N. AcARwAr, ( Allerrtate) Q9
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SHRI S. R. SI'RI Central Soil and Materials Research Station, New Delhi
SHRr N. CHANDRdSEK,\IAN ( Alternate )
SUPERINTENDING ENGINEER (DESIGN) Public Works Department, Government of Tamil Nadu, Chennai a'
ExBcurrvE ENGINEER (S. M. R. DrusIoN) ( tllternate)
SURI A. K, CTi-A-DHA Hindust:rn Prefab Ltd, New Delhi z>
SItRr J. R. Str( Alternate)
DR H C. V]SVESV,ARAY^{ The Instilution of E n gineers (India), Calcutt:r zo
SHRI D- C CHATUR\tsDr(Allernute) -ll
SHRr VrNoD KtrNr,AR, Direcbr Gener:rl, BIS ( Ex-officio Metnber ) >e
Dircctor (Civ Engg) -C
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Mernber-Secrelary r-
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SIIRI J. K, PRASAD a
Additional f)irector (Civ Engg), BIS o
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Concrete Subcommittee, CED 2: 2 :'1
C
7
Conuener

DRA. K. MULUCK Nalional Council for Ccment;rnd Building Materials, New Delhi
Members
SHRI C] R. AUMCHANDANI Sbup Consultants Ltd, Mumbai
SrrRr S. RANGA-RqJN.] ( AltentoLe)
DR P C. CHowD}tARY Torsteel Rcsearch Foundation in India, Calcutta
DR C. S. VISHWANATH (Allernale)
SHRI J P, DESAI (iujarat Ambuja Cement Ltd, Ahmedabad
SHRI B. K. JAGETIA ( Allernale )
DrREcroR Central Soil Materials Research Station, New Delhi
SHRI N. CHANDR ASEKARAN ( Altern ate )
JOINT DIRECTOR ST.{NDARDS (B&SYCB.II Research, Designs and Standards Organizalion, Lucknow
JoINT DIREcToR STANJTJARDS (B&S)/CB-I ( Alternate )

( Cotilirr,ued ott poge l,l )

r3
IS 9103 : 1999
( Continued. lrorn page 13 )

Mernbers Representing

SUPERIT.TTENDING ENGINEER (DESIGNS) Central Public Works Department, New Delhi

SHRI V. K. GHANEK.AR Structural Engineering Research Cen tre, Ghaziabad

SHRI D. S. PR.\I<-ASH R.ro ( -llkrtnte)
SIIRI S. K. GUHA THAKURT.{ (]annon Dunkerley and Co Ltd, Mumbai
SERI S. P. SANKARA,\ARAY.ANAN (, IIeTncIe )
SHRr J. S. HrNGo&AN'r Associated Consulting Services, Mumbai
SIrRI A. P. REMEDIoS ( Altentate )
SHRI I,ALIT KUMAR JAIN In personal capacity (Consulting Slruclural Engineer 36, Old
Sneh Nagar, Wardha Road, Nagpur 'l4OO I 5 )

SHRI M. P. JAISINGH Central Building Research Institute (CSIR), Roorkee

SHRI B. ILaMESWAM RAo ( Alternate )
CHrEF ENGTNEER & JorNT SECRET^{RY Public Works Department, Mumbai \a
ST'PERIN.TENDING ENGINEER ( AITeTn.ate )
oc
PROF S. KRISHNAMooRTEY Indian Institute of Technology, New Delhi 7=
-tn
SHRI K. K. NAYAR ( Alternale )
--
DR S. C. MAII.I National Council for Cement and Building Materials, New Delhi 72
MANAGING DIRxcToR Hindustan Prefab Ltd, New Delhi aa
rf,^
SHRI M. KUNDU (Alrerru,e tt6
) <c
SHRI M. K. MUKIIER,IEE Ministry of Transport (Roads Wing), New Delhi oP
SmJ N. K. SINHA ( Alternate )
;<
SHRI B. V. B. PAL The Associated Cement Co Ltd, Mumbai
SmJ M. G. DANDAV.ATE ( Altemale )
z>
SHRI A. B. PHA.DKE The Hindustan Construction Co Ltd, Mumbai
SmJ D. M. SAVLB, (Alternate)
?o
arl 70
SHRI Y. R. PHUI,L Central Road Research Institute, New Delhi - lr1

SHRI S. S. SEEHRA ( Allernatel ) 2a

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SHRI SATENDER KUMAR (AILeTnaTeII)
SHRI A. S. PMSAD RAo Structural Engineering Research Centre (CSIR), Chennar r-
a
SHRI K. M.wI ( Allerrr.ole o
) o
K. L. PRUTHI National Building and Construction Corporation Lbd, New Delhi
zO
SHRI
o
SHRI J. R. GABRIEL ( Alterrnte)
SHRI B. D. RAJLATKER Nuclear Power Corporation, Mumbai c=
SHRI U. S. P. VERIVLA (Altennte) =
SHRI HANUT,GNTIIA RAO A. P. Engineering Reserch Laboratories, Hyderabad
SHRI G. RAMAKRISHNEN ( AITeTnaTe)
SHRI S. A. REDDI Gamnon India Ltd, Munbar
DR N. V. NAYAK ( Alterlale )
SHRI S. C, SAWHNSY Engineers India Ltd, New Delhi
SHRI R. P. MEmorRA (AlLernate)
SHRI J. R. SHARMA Army Headquarters, Engineer-in-Chiefs Branch, New Delhi
SITRI SURINDER NIOHIN ( Altertt ate )
PRoF M. S. SHETTY Indian Concrete Institute, Chennai
SHRI B. T. UNwAu,A In personal capacity (15/9, Rustorn Baug, Victoria Road,
Mutnbai 400027)
DIREcToR (C&NIDD) Central Water Commission, New Delhi
DEpr-rry DIRECToR (C&MDD) ( Altern ate )

t4
Bureau of Indian Standards
BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote
harmonious development of the activities of standarrlization, marking and quality cerffication of goods and
attending to connected matters in the country.

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Amendments are issued bo standards as the need arises on the basis of comments. Standards are also
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referring bo bhe labest issue of 'BIS Catalogue' and 'Standards : Monthly Additions'.
This Indian Standard has been develooed from Doc : No. CED 2 (5421\
cc
Amendments Issued Since Publication
-|n
Amend No. Date of Issue ;v
-<
Amd. No. 1 January 2003
aa
Amd. No. 1 August 2007
CEO

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BUREAU OF INDIAN STANDARDS zq
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Headquarters:
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Manak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002. Telegrams: Manaksanstha 7
Telephones: 323 0r 31, 323 33 75, 323 94 02 (Common co all offices)

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