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Copyright© 2018 ASTM International, West Conshohocken, PA . All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed,
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Table of Contents
Program Report Cycle Information..............................................................................................................................3
How to Use This Program Report ...............................................................................................................................4
Revision 3 Issued July 9, 2018 ....................................................................................................................................4
Overview .....................................................................................................................................................................4
Data Preparation........................................................................................................................................................8
A copy of the data entry worksheet for this cycle is available under Documents at ptp2.astm.org.
Contact Information
Authorized By: Amy Meacock
Address: ASTM International
100 Barr Harbor Drive
West Conshohocken, PA
19428-2959
Email: ptp@astm.org
Phone: 1-610-832-9585
Fax 1-610-832-9668
Sample Information
Identification: Dissolved Gas Analysis(DGA) DGA1808
Source: Confidential, donated
Preparation, Distribution: Doble Engineering Company, 85 Walnut Street, Watertown, MA
United States 02472
Phone: 6173932981
Distribution Dates: Week of August 10, 2018
Homogeneity Confirmed prior to distribution and by analysis of returned data.
Stability: Sample packaged and sealed to ensure stability during
shipment. Once received, sample stability is the responsibility of
the recipient.
Report Information
Result Submission Due Date: October 5, 2018
Data Analysis & Reporting: ASTM International PTP Office
Report Issue Date: November 9, 2018
Overview
The Program Report shows results for all participating laboratories. It is similar to the
Laboratory Report, but without reference to a specific laboratory. The intent of the Program
Report is to assess the performance of a method, rather than a specific lab. The Program
report is directed to PTP program managers, to the subcommittees responsible either for the
test methods or for the product’s specifications, and to laboratories desiring to investigate
overall test method performance.
Numeric Methods
Average column—Consider cases where the Average for any test method is
unusual for the product.
Precision Performance column—Consider any test method where the “These
Data R” is considered “Worse” than the “ASTM R.”
Normal column—Consider possible impact on identified outliers for any test
method where the Anderson-Darling Statistic indicates non-normality.
Non-Numeric Methods
This agreement is presented to participants on screen prior to their clicking on the “accept”
link to submit payment for services.
“You agree the data generated as a result of the proficiency testing services and provided to
ASTM is confidential information and you further agree not to disclose or provide this data to
anyone else without ASTM's written consent. You also acknowledge and agree that the
report generated as a result of this proficiency testing program will be copyrighted by ASTM
International. You may however share data with an accreditation body for auditing purposes
only. You hereby assign to ASTM any rights you may have in data you provide to ASTM
International by clicking on the link.”
Numeric Methods
Non-Numeric Methods
For each method, the summary table appears first, followed by the Results Table and
historic Z-scores, the Data Distribution chart (Q-Q plot), and the Histogram. There is one set
of these tables and plots for each numeric test method. All results reported by participating
laboratories are included in the summary tables. All results except for non-conforming results
and those rejected as GESD outliers are then used for calculations and generating statistics.
Z-Score results from a Comparison Lab will be included when available.
Program Numeric Method Summary Table (one for each Test Method)
The Program Numeric Method Summary Table is a summary of the statistics generated for
that specific test method. No specific laboratory’s result is highlighted. If there are
“comparison labs,” their results, Z-Scores and notes are shown. If there are no comparison
labs, as is most often the case, then that portion of the table is omitted.
Program Numeric Results Table and Z-Scores (one for each Test Method)
Each laboratory is identified by a randomly selected code with the same laboratory code
applying throughout the entire report. This table shows performance statistics for all of the
methods in a specific PT program on a single or consecutive pages. Program Report –
Results Summary Table includes results from all participating laboratories. All results except
for GESD outliers and non-conforming results are then used for calculations and generating
statistics.
This table shows historic Z-Scores for all laboratories for each test method. This table
shows, for each laboratory: a randomized Lab Code, test result, deviation, Z-score, notes,
historic Z-scores from the six most recent cycles, count, average Z-score, and standard
deviation for the Z-scores collected for each laboratory. The pooled standard deviation
across all laboratory Z-scores is also provided.
The graphic is plotted above a horizontal line scaling the range of results. An individual plot
is comprised of a rectangle (“box”) with the left end at the first quartile and the right end at
the third quartile. The height of the rectangle is chosen so as to produce a pleasing picture,
but it is usually substantially less than the width. The rectangle is divided by a vertical line
segment at the median of the distribution. A line segment which is an extension of the
horizontal bisector of the rectangle (a “whisker”) extends from the left end of the rectangle
down to the value of the smallest observed result that is no more than 1.5 interquartile
ranges less than the first quartile. A similar line extends from the right end of the rectangle
to the value of the greatest observed result that is no more than 1.5 interquartile ranges
more than the third quartile. The extreme ends of the two rays are capped with a small,
unobtrusive T. Finally, for any result smaller than the first quartile minus 1.5 interquartile
ranges, a marker is plotted on an invisible extension of the left whisker, and all results larger
than 1.5 interquartile ranges plus the third quartile are plotted beyond the end of the right
whisker.
Non-Conforming results will be listed in the respective Program Numeric Results Table along
with a NCR in the Notes column.
For non-numeric methods, the method generally provides – or one can infer – a list of all
possible valid results. Any submitted result that is not on such a list is non-conforming.
Standard Deviation, s
srepro, and srepeat are the corresponding reproducibility standard deviation and the
repeatability standard deviation as calculated using the proficiency testing data.
sASTM R and sASTM r when needed are determined from the corresponding ASTM
reproducibility (R) and ASTM repeatability (r) as:
Where:
ni is the number of Z-scores listed for a given laboratory
si is the corresponding standard deviation for those Z-scores
k is the number of laboratories with historic Z-scores
Reproducibility, R
ASTM R – Extracted from or calculated using equations in the referenced ASTM Test
Method. Reported to the resolution given in the method or to the same resolution as the
reproducibility standard deviation.
These Data R – Calculated using the reproducibility standard deviation, srepro, determined for
These Data as per the following equation:
Repeatability, r
ASTM r – Extracted from or calculated using equations in the referenced ASTM Test
Method. Reported to the resolution given in the method or to the same resolution as the
repeatability standard deviation.
These Data r – Calculated using the repeatability standard deviation, srepeat, determined for
These Data as per the following equation
As with the t-test, the risk of Type I error is held to 5% only if the distributions are nearly
normal. This statistical test evaluates whether or not the PT precision is better than,
consistent with or worse than the ASTM precision in accord with the following table
Normal?
The following conclusions are made regarding the normalcy of the “These Data” distribution
based on the Anderson-Darling Statistic:
Unique Results
Number of unique non-numeric results reported by all laboratories submitting results
Mode
The mode is the most frequently occurring non-numeric result.
Modal
Frequency of Mode divided by n and expressed as a percent. (Resolution = 0.1 %.)
NSP - No Statistics Performed: < 6 results submitted, or mixed data set with > 18%
non-numeric results, or statistics not calculated as per program review.
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -3.1 -0.91 NDS NDS NDS 1 -0.91
0021 7 0.9 0.26 0.74 0.68 0.66 4 0.59 0.22
0030 7 0.9 0.26 NDS 0.75 0.82 3 0.61 0.31
0041 7.9 1.8 0.52 0.74 0.39 0.66 4 0.58 0.15
0068 7 0.9 0.26 NDS NDS NDS 1 0.26
0090 5 -1.1 -0.32 NDS 0.61 NDS 2 0.15 0.66
0097 7 0.9 0.26 NDS NDS NDS 1 0.26
0103 4 -2.1 -0.61 0.74 -0.29 -0.77 4 -0.23 0.68
0105 5 -1.1 -0.32 0.26 0.32 -0.30 4 -0.01 0.35
0110 1.346275 -4.753725 -1.39 -2.05 NDS NDS 2 -1.72 0.47
0113 15 8.9 2.60 3 NDS -0.29 NDS 2 1.16 2.04
0123 4 -2.1 -0.61 -0.22 -1.44 -0.14 4 -0.60 0.59
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 173 -640.2 -1.77 NDS NDS NDS 1 -1.77
0021 1189 375.8 1.04 0.12 0.59 0.50 4 0.56 0.38
0030 1130 316.8 0.88 NDS 0.70 0.54 3 0.71 0.17
0041 1220 406.8 1.13 0.63 0.29 0.98 4 0.76 0.38
0068 978 164.8 0.46 NDS NDS NDS 1 0.46
0090 1007 193.8 0.54 NDS 0.38 NDS 2 0.46 0.11
0097 392 -421.2 -1.17 NDS NDS NDS 1 -1.17
0103 659 -154.2 -0.43 1.88 0.21 -0.07 4 0.40 1.02
0105 795 -18.2 -0.05 -1.11 1.73 0.86 4 0.36 1.22
0110 266.143405 -547.056595 -1.51 -0.68 NDS NDS 2 -1.10 0.59
0113 987 173.8 0.48 NDS -0.44 NDS 2 0.02 0.65
0123 962 148.8 0.41 -0.53 -0.95 -0.41 4 -0.37 0.57
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 18 -15 -1.28 NDS NDS NDS 1 -1.28
0021 38 5 0.44 0.79 1.59 0.10 4 0.73 0.64
0030 29 -4 -0.33 NDS 0.34 -0.46 3 -0.15 0.43
0041 43 10 0.86 0.79 0.54 0.04 4 0.56 0.37
0068 30 -3 -0.25 NDS NDS NDS 1 -0.25
0090 14 -19 -1.62 NDS -1.38 NDS 2 -1.50 0.17
0097 37 4 0.35 NDS NDS NDS 1 0.35
0103 50 17 1.46 0.29 0.25 -0.98 4 0.26 1
0105 27 -6 -0.51 0.66 1.30 0.07 4 0.38 0.78
0110 49.86342 16.86342 1.45 8.48R NDS NDS 1 1.45
0113 37 4 0.35 NDS -0.71 NDS 2 -0.18 0.75
0123 22 -11 -0.93 -1.45 -1.29 -0.98 4 -1.16 0.25
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -12 -1.62 NDS NDS NDS 1 -1.62
0021 17 2 0.27 -0.68 0.53 0.33 4 0.11 0.54
0030 20 5 0.68 NDS 0.86 0.90 3 0.81 0.12
0041 20.4 5.4 0.73 1.06 1.00 0.65 4 0.86 0.2
0068 21 6 0.81 NDS NDS NDS 1 0.81
0090 11 -4 -0.54 NDS 0.86 NDS 2 0.16 0.99
0097 20 5 0.68 NDS NDS NDS 1 0.68
0103 9 -6 -0.81 1.06 -0.28 -0.75 4 -0.20 0.87
0105 16 1 0.14 0.48 1.00 0.74 4 0.59 0.37
0110 1.33104 -13.66896 -1.84 -8.92R NDS NDS 1 -1.84
0113 25 10 1.35 NDS 0.72 NDS 2 1.04 0.45
0123 16 1 0.14 -1.26 -1.38 -0.19 4 -0.67 0.76
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 3 -12.3 -1.62 NDS NDS NDS 1 -1.62
0021 18 2.7 0.36 0.38 0.73 0.73 4 0.55 0.21
0030 22 6.7 0.88 NDS 1.02 0.68 3 0.86 0.17
0041 20.5 5.2 0.68 0.56 0.73 0.72 4 0.67 0.08
0068 22 6.7 0.88 NDS NDS NDS 1 0.88
0090 10 -5.3 -0.70 NDS 0.67 NDS 2 -0.02 0.97
0097 19 3.7 0.49 NDS NDS NDS 1 0.49
0103 10 -5.3 -0.70 0.90 -0.19 -0.72 4 -0.18 0.76
0105 16 0.7 0.09 0.38 0.96 1.01 4 0.61 0.45
0110 2.20919 -13.09081 -1.73 -2.14 NDS NDS 2 -1.94 0.29
0113 26 10.7 1.41 NDS 0.73 NDS 2 1.07 0.48
0123 15 -0.3 -0.04 -0.13 -1.29 -0.02 4 -0.37 0.62
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 5 -17.5 -1.41 NDS NDS NDS 1 -1.41
0021 31 8.5 0.68 0.76 1.19 1.20 4 0.96 0.28
0030 28 5.5 0.44 NDS 0.63 0.49 3 0.52 0.1
0041 36 13.5 1.09 0.10 -0.14 1.36 4 0.60 0.73
0068 20 -2.5 -0.20 NDS NDS NDS 1 -0.20
0090 14 -8.5 -0.68 NDS -1.05 NDS 2 -0.87 0.26
0097 22 -0.5 -0.04 NDS NDS NDS 1 -0.04
0103 16 -6.5 -0.52 0.76 0.42 -2.33 4 -0.42 1.39
0105 25 2.5 0.20 0.98 0.21 0.26 4 0.41 0.38
0110 0 -22.5 -1.81 -1.39 NDS NDS 2 -1.60 0.3
0113 43 20.5 1.65 NDS 1.33 NDS 2 1.49 0.23
0123 30 7.5 0.60 0.17 -1.97 -0.38 4 -0.40 1.12
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 5 -112.2 -6.99 R NDS NDS NDS 0
0021 141 23.8 1.48 0.82 1.40 1.13 4 1.21 0.3
0030 129 11.8 0.74 NDS 0.75 0.46 3 0.65 0.16
0041 137 19.8 1.23 0.33 0.46 0.78 4 0.70 0.4
0068 119 1.8 0.11 NDS NDS NDS 1 0.11
0090 89 -28.2 -1.76 NDS 0.11 NDS 2 -0.83 1.32
0097 121 3.8 0.24 NDS NDS NDS 1 0.24
0103 99 -18.2 -1.13 0.95 0.31 -0.59 4 -0.12 0.93
0105 112 -5.2 -0.32 0.19 0.90 0.90 4 0.42 0.59
0110 17.419935 -99.780065 -6.22 R -2.06 NDS NDS 1 -2.06
0113 114 -3.2 -0.20 NDS -0.44 NDS 2 -0.32 0.17
0123 111 -6.2 -0.39 -0.12 -0.98 0.47 4 -0.26 0.6
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 21576 -22,168.9 -0.78 2 NDS NDS NDS 1 -0.78
0021 76798 33,053.1 1.16 2 -0.53 0.08 0.63 4 0.34 0.73
0030 61100 17,355.1 0.61 2 NDS 36.15R 0.61 2 0.61 0
0041 70500 26,755.1 0.94 2 1.49 -0.38 1.72 4 0.94 0.94
0068 5666 -38,078.9 -1.34 2 NDS NDS NDS 1 -1.34
0090 61026 17,281.1 0.61 2 NDS 0.23 NDS 2 0.42 0.27
0097 58 -43,686.9 -1.53 2 NDS NDS NDS 1 -1.53
0103 53968 10,223.1 0.36 1.03 0.02 -0.87 4 0.14 0.79
0105 55282 11,537.1 0.40 -0.92 1.76 0.93 4 0.54 1.12
0110 46.18743561 -43,698.7125644 -1.53 2 18.32R NDS NDS 1 -1.53
0113 54588 10,843.1 0.38 NDS -0.30 NDS 2 0.04 0.48
0123 64330 20,585.1 0.72 2 -0.42 -0.40 0.29 4 0.05 0.56
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0018 6708 -15,302.4 -1.31 NDS NDS NDS 1 -1.31
0021 26961 4,950.6 0.42 -0.73 -0.22 -0.34 4 -0.22 0.48
0030 27500 5,489.6 0.47 NDS 28.23R 0.11 2 0.29 0.25
0041 32000 9,989.6 0.86 1.46 -0.24 1.05 4 0.78 0.73
0068 2376 -19,634.4 -1.68 NDS NDS NDS 1 -1.68
0090 27093 5,082.6 0.44 NDS 0.07 NDS 2 0.26 0.26
0097 26588 4,577.6 0.39 NDS NDS NDS 1 0.39
0103 28935 6,924.6 0.59 0.64 0.83 -0.78 4 0.32 0.74
0105 26167 4,156.6 0.36 -1.23 1.40 0.92 4 0.36 1.14
0110 18.31860898 -21,992.081391 -1.88 16.96R NDS NDS 1 -1.88
0113 31770 9,759.6 0.84 NDS -0.18 NDS 2 0.33 0.72
0123 28008 5,997.6 0.51 0.37 -1.14 0.15 4 -0.03 0.76
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0068 0 $ NDS NDS NDS 0
0110 1.44970 $ $ NDS NDS 0
Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0068 0 $ NDS NDS NDS 0
0110 1.44970 $ $ NDS NDS 0
Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 6 -1.3 -1.80 -0.85 -0.97 NDS 3 -1.21 0.52
0044 7 -0.3 -0.46 0.06 1.81 -5.56R 3 0.47 1.19
0052 8 0.7 0.88 -0.40 0.21 -1.39 4 -0.18 0.96
0067 8 0.7 0.88 -0.85 -1.03 -1.39 4 -0.60 1.01
0069 7.4 0.1 0.08 0.78 0.57 0.28 4 0.43 0.31
0093 27 19.7 26.36 R 1.87 -1.15 -6.39R 2 0.36 2.14
0120 7 -0.3 -0.46 0.06 NDS NDS 2 -0.20 0.37
0121 8 0.7 0.88 1.87 NDS NDS 2 1.38 0.7
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 885 -208.6 -0.73 -0.99 -1.58 NDS 3 -1.10 0.44
0044 1165 71.4 0.25 0.45 0.98 -1.63 4 0.01 1.14
0052 962 -131.6 -0.46 -0.30 0.23 -0.81 4 -0.34 0.43
0067 1140 46.4 0.16 -0.60 -0.67 -0.45 4 -0.39 0.38
0069 969 -124.6 -0.44 0.56 0.50 0.26 4 0.22 0.46
0093 1201 107.4 0.38 -2.26 0.37 0.64 4 -0.22 1.37
0120 742 -351.6 -1.23 0.50 NDS NDS 2 -0.37 1.22
0121 1685 591.4 2.08 3 6.47R NDS NDS 1 2.08
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 50 11.2 0.58 -1.47 1.59 NDS 3 0.23 1.56
0044 24 -14.8 -0.77 -0.05 0.29 -1.27 4 -0.45 0.7
0052 37 -1.8 -0.10 -0.36 0.08 -1.39 4 -0.44 0.66
0067 16 -22.8 -1.18 -0.72 -0.13 -0.04 4 -0.52 0.53
0069 26.7 -12.1 -0.63 0.97 0.76 1.13 4 0.56 0.81
0093 48 9.2 0.48 -1.07 0.18 -0.79 4 -0.30 0.75
0120 32 -6.8 -0.35 1.37 NDS NDS 2 0.51 1.22
0121 77 38.2 1.98 6.48R NDS NDS 1 1.98
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 17 -2.7 -0.60 -0.68 -1.25 NDS 3 -0.84 0.35
0044 15 -4.7 -1.05 -0.68 -0.26 -1.18 4 -0.79 0.41
0052 21 1.3 0.29 1.43 1.18 0.18 4 0.77 0.63
0067 19.0 -0.7 -0.16 -0.42 -0.33 -0.11 4 -0.26 0.14
0069 19 -0.7 -0.16 1.35 0.07 0.79 4 0.51 0.69
0093 98 78.3 17.40 R 8.83R -0.92 -1.62 2 -1.27 0.49
0120 18 -1.7 -0.38 0.38 NDS NDS 2 0.00 0.54
0121 29 9.3 2.06 3 8.04R NDS NDS 1 2.06
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 39 20.3 7.07 R 1.82 -1.30 NDS 2 0.26 2.21
0044 15 -3.7 -1.28 -0.98 0.01 -1.59 4 -0.96 0.69
0052 22 3.3 1.16 0.22 1.09 0.37 4 0.71 0.48
0067 17 -1.7 -0.58 -1.11 -0.53 -0.08 4 -0.58 0.42
0069 19 0.3 0.12 0.41 0.24 0.53 4 0.33 0.18
0093 43 24.3 8.46 R -0.45 -0.92 -1.76 3 -1.04 0.66
0120 17 -1.7 -0.58 -0.18 NDS NDS 2 -0.38 0.28
0121 22 3.3 1.16 1.95 NDS NDS 2 1.56 0.56
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 52 8.5 0.25 $ $ NDS 1 0.25
0044 22 -21.5 -0.64 -0.83 -1.64 0.62 4 -0.62 0.93
0052 9 -34.5 -1.02 -0.61 -0.65 0.59 4 -0.42 0.7
0067 23.0 -20.5 -0.61 -0.30 -0.09 -0.92 4 -0.48 0.36
0069 53.8 10.3 0.30 1.12 0.62 0.68 4 0.68 0.34
0093 34 -9.5 -0.28 0.24 1.82 -2.18 4 -0.10 1.65
0120 <13 $ NCR $ NDS NDS 0
0121 111 67.5 1.99 2.37 NDS NDS 2 2.18 0.27
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 153 22.5 1.19 0.97 -0.57 NDS 3 0.53 0.96
0044 119 -11.5 -0.61 -0.60 0.06 0.17 4 -0.25 0.42
0052 125 -5.5 -0.29 0.22 0.26 -0.04 4 0.04 0.26
0067 119 -11.5 -0.61 -0.79 -0.76 -0.78 4 -0.74 0.08
0069 117 -13.5 -0.72 1.36 1.23 1.10 4 0.74 0.98
0093 144 13.5 0.72 -1.95 -0.23 -2.30 4 -0.94 1.43
0120 108 -22.5 -1.19 -0.20 NDS NDS 2 -0.70 0.7
0121 159 28.5 1.51 5.46R NDS NDS 1 1.51
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 66703 8,320 0.92 0.47 -1.17 NDS 3 0.07 1.1
0044 45409 -12,974 -1.44 -0.65 -1.56 -0.79 4 -1.11 0.46
0052 61732 3,349 0.37 -0.79 0.57 0.54 4 0.17 0.65
0067 57300 -1,083 -0.12 -0.07 -0.36 -0.32 4 -0.22 0.14
0069 60729 2,346 0.26 -0.53 1.37 2.12 4 0.81 1.17
0093 70852 12,469 1.38 -0.67 1.47 -1.63 4 0.14 1.54
0120 58535 152 0.02 0.58 NDS NDS 2 0.30 0.4
0121 45804 -12,579 -1.40 2.03 NDS NDS 2 0.32 2.43
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0023 32073 6,637.2 1.34 0.50 -1.13 NDS 3 0.24 1.26
0044 16840 -8,595.8 -1.73 -0.77 -1.38 -0.61 4 -1.12 0.52
0052 27245 1,809.2 0.36 -0.37 0.92 -0.28 4 0.16 0.6
0067 25900 464.2 0.09 0.26 0.15 0.12 4 0.16 0.07
0069 29954 4,518.2 0.91 -0.16 1.96 1.58 4 1.07 0.93
0093 20655 -4,780.8 -0.96 -0.47 0.18 -0.67 4 -0.48 0.48
0120 27372 1,936.2 0.39 0.79 NDS NDS 2 0.59 0.28
0121 23447 -1,988.8 -0.40 2.64 NDS NDS 2 1.12 2.15
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0044 4.4 $ $ $ NDS 0
0121 0 $ $ NDS NDS 0
Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0044 0 $ $ $ NDS 0
0121 45 $ $ NDS NDS 0
Pooled StdDev of Z: 0
Legend
NDS No Data Submitted
NCR Non Conforming Results
1 Test result outside ± 3 sigma range for These Data
2 Test result outside ± 3 sigma range for ASTM Reproducibility
3 Z-Score outside range of -2 to 2
# Z-Score > 90
$ Z-Score not calculated
R Rejected by GESD
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 7 0.2 0.10 0.25 0.25 0.29 4 0.22 0.08
0002 5.29 -1.51 -0.74 NDS -0.81 NDS 2 -0.78 0.05
0004 4.3 -2.5 -1.22 -0.52 -1.00 0.15 4 -0.65 0.61
0005 16 9.2 4.52 R 0.25 0.49 NDS 2 0.37 0.17
0007 5.8 -1 -0.49 -0.06 3.65 0.74 4 0.96 1.86
0008 6 -0.8 -0.39 -0.14 0.30 0.42 4 0.05 0.38
0009 8 1.2 0.59 -0.52 -0.37 -1.62 4 -0.48 0.91
0011 7 0.2 0.10 0.63 0.11 0.02 4 0.22 0.28
0012 7 0.2 0.10 0.25 1.36 0.29 4 0.50 0.58
0013 7 0.2 0.10 -0.91 0.73 -0.80 4 -0.22 0.78
0014 8 1.2 0.59 1.02 0.54 NDS 3 0.72 0.26
0015 8 1.2 0.59 1.02 NDS 0.15 3 0.59 0.44
0016 8 1.2 0.59 -0.14 1.46 -0.39 4 0.38 0.83
0017 7.3 0.5 0.25 -0.10 0.38 -0.12 4 0.10 0.25
0022 7 0.2 0.10 0.63 0.78 0.07 4 0.40 0.36
0024 6.4 -0.4 -0.19 NDS -0.61 -0.67 3 -0.49 0.26
0025 4 -2.8 -1.37 NDS -0.04 4.11R 2 -0.71 0.94
0026 12.69556 5.89556 2.90 3 2.94 2.07 NDS 3 2.64 0.49
0028 6 -0.8 -0.39 0.25 0.78 0.56 4 0.30 0.51
0029 7 0.2 0.10 -0.14 0.11 0.15 4 0.06 0.13
0031 7 0.2 0.10 NDS -1.00 NDS 2 -0.45 0.78
0032 6 -0.8 -0.39 -0.52 NDS NDS 2 -0.46 0.09
0034 8 1.2 0.59 0.84 NDS NDS 2 0.72 0.18
0035 1.45 -5.35 -2.62 3 -0.85 -1.15 -1.11 4 -1.43 0.8
0036 5 -1.8 -0.88 NDS NDS NDS 1 -0.88
0038 8.8 2 0.99 NDS 0.70 NDS 2 0.85 0.21
0039 7.2 0.4 0.20 1.40 0.59 NDS 3 0.73 0.61
0040 5 -1.8 -0.88 -0.14 0.11 # 3 -0.30 0.51
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 1051 -45 -0.19 0.20 1.74 0.26 4 0.50 0.85
0002 702.97 -393.03 -1.66 NDS -1.01 NDS 2 -1.34 0.46
0004 471.6 -624.4 -2.63 3 -1.89 -1.31 -2.13 4 -1.99 0.55
0005 998 -98 -0.41 -0.31 -0.84 NDS 3 -0.52 0.28
0007 1294.8 198.8 0.84 0.91 1.10 0.14 4 0.75 0.42
0008 1004 -92 -0.39 -0.39 -0.26 -0.26 4 -0.33 0.08
0009 1183 87 0.37 -0.03 -0.11 -0.94 4 -0.18 0.55
0011 1053 -43 -0.18 0.16 -0.04 -0.02 4 -0.02 0.14
0012 1430 334 1.41 2.31 1.30 0.61 4 1.41 0.7
0013 1150 54 0.23 0.18 0.56 -0.68 4 0.07 0.53
0014 1068 -28 -0.12 1.23 -0.47 NDS 3 0.21 0.9
0015 1315 219 0.92 0.65 NDS 0.11 3 0.56 0.41
0016 1099 3 0.01 -0.15 0.49 -0.70 4 -0.09 0.49
0017 798.5 -297.5 -1.25 0.00 0.64 0.43 4 -0.05 0.85
0022 1101 5 0.02 -0.01 1.43 -0.01 4 0.36 0.72
0024 823 -273 -1.15 NDS -1.00 -0.61 3 -0.92 0.28
0025 1080 -16 -0.07 NDS -0.06 -0.09 3 -0.07 0.02
0026 1294.79768 198.79768 0.84 0.53 0.36 NDS 3 0.58 0.24
0028 1010 -86 -0.36 0.28 -0.29 -0.10 4 -0.12 0.29
0029 1113 17 0.07 -0.29 -0.16 -0.03 4 -0.10 0.16
0031 1202 106 0.45 NDS -0.78 NDS 2 -0.17 0.87
0032 700 -396 -1.67 0.35 NDS NDS 2 -0.66 1.43
0034 1298 202 0.85 1.15 NDS NDS 2 1.00 0.21
0035 877.45 -218.55 -0.92 -1.33 -0.38 -1.16 4 -0.95 0.41
0036 1836 740 3.12 1,3 NDS NDS NDS 1 3.12
0038 1415.2 319.2 1.34 NDS 1.19 NDS 2 1.27 0.11
0039 1011 -85 -0.36 0.61 -0.37 NDS 3 -0.04 0.56
0040 973 -123 -0.52 -1.91 0.15 0.42 4 -0.47 1.04
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 23 -14.8 -1.02 -0.34 -0.11 0.10 4 -0.34 0.49
0002 23.23 -14.57 -1.01 NDS -0.21 NDS 2 -0.61 0.57
0004 17.2 -20.6 -1.42 -0.46 -0.81 1.74 4 -0.24 1.38
0005 28 -9.8 -0.68 -0.67 -0.61 NDS 3 -0.65 0.04
0007 62.9 25.1 1.73 1.84 0.61 0.50 4 1.17 0.71
0008 39 1.2 0.08 -0.42 -0.01 -0.81 4 -0.29 0.41
0009 26 -11.8 -0.81 -0.46 -0.51 -0.27 4 -0.51 0.22
0011 34 -3.8 -0.26 0.19 0.14 0.13 4 0.05 0.21
0012 72 34.2 2.36 3 4.68R 0.65 0.00 3 1.00 1.22
0013 45 7.2 0.50 1.17 2.30 -0.14 4 0.96 1.04
0014 29 -8.8 -0.61 0.80 0.85 NDS 3 0.35 0.83
0015 175 137.2 9.47 R -0.50 NDS -0.30 2 -0.40 0.14
0016 45 7.2 0.50 0.92 2.05 -0.30 4 0.79 0.98
0017 71.5 33.7 2.33 3 -0.95 0.48 -0.10 4 0.44 1.39
0022 28 -9.8 -0.68 0.19 0.45 0.78 4 0.19 0.63
0024 30.3 -7.5 -0.52 NDS -0.51 -0.61 3 -0.55 0.06
0025 40 2.2 0.15 NDS 0.35 1.94 3 0.81 0.98
0026 44.60403 6.80403 0.47 0.07 -0.20 NDS 3 0.11 0.34
0028 61 23.2 1.60 3.21 1.70 0.40 4 1.73 1.15
0029 29 -8.8 -0.61 -0.63 0.09 -0.67 4 -0.46 0.36
0031 24 -13.8 -0.95 NDS -1.46 NDS 2 -1.21 0.36
0032 29 -8.8 -0.61 -0.63 NDS NDS 2 -0.62 0.01
0034 38 0.2 0.01 -0.29 NDS NDS 2 -0.14 0.21
0035 9.46 -28.34 -1.96 -0.44 -1.79 1.02 4 -0.79 1.39
0036 73 35.2 2.43 3 NDS NDS NDS 1 2.43
0038 35.4 -2.4 -0.17 NDS 1.20 NDS 2 0.52 0.97
0039 27.8 -10 -0.69 0.03 -0.01 NDS 3 -0.22 0.4
0040 40 2.2 0.15 -0.26 1.05 1.84 4 0.70 0.94
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 18 -2.3 -0.77 -0.14 -0.19 -0.27 4 -0.34 0.29
0002 13.55 -6.75 -2.30 3 NDS -1.77 NDS 2 -2.04 0.37
0004 14.5 -5.8 -1.97 -0.14 -1.70 1.46 4 -0.59 1.59
0005 23 2.7 0.94 0.33 -1.17 NDS 3 0.03 1.09
0007 18.7 -1.6 -0.53 0.52 0.44 -0.66 4 -0.06 0.62
0008 19 -1.3 -0.43 -0.37 -0.57 0.45 4 -0.23 0.46
0009 20 -0.3 -0.09 -1.08 -0.26 -1.78 4 -0.80 0.78
0011 21 0.7 0.25 0.57 0.49 0.25 4 0.39 0.16
0012 22 1.7 0.60 0.80 1.77 1.44 4 1.15 0.55
0013 23 2.7 0.94 -0.37 0.19 -0.20 4 0.14 0.58
0014 24 3.7 1.28 1.28 1.32 NDS 3 1.29 0.02
0015 23 2.7 0.94 0.10 NDS 0.47 3 0.50 0.42
0016 18 -2.3 -0.77 -0.85 0.57 -0.48 4 -0.38 0.65
0017 19.7 -0.6 -0.19 0.92 0.81 0.07 4 0.40 0.55
0022 19 -1.3 -0.43 0.10 0.57 -0.04 4 0.05 0.41
0024 18.4 -1.9 -0.64 NDS -1.02 -0.41 3 -0.69 0.31
0025 19 -1.3 -0.43 NDS -1.09 2.44 3 0.31 1.88
0026 21.11083 0.81083 0.29 0.57 0.42 NDS 3 0.43 0.14
0028 18 -2.3 -0.77 1.51 0.41 0.56 4 0.43 0.94
0029 20 -0.3 -0.09 -0.61 -0.34 0.18 4 -0.22 0.34
0031 20 -0.3 -0.09 NDS -1.70 NDS 2 -0.90 1.14
0032 17 -3.3 -1.12 -0.37 NDS NDS 2 -0.75 0.53
0034 23 2.7 0.94 1.09 NDS NDS 2 1.02 0.11
0035 18.38 -1.92 -0.64 -0.96 -1.10 -0.21 4 -0.73 0.4
0036 17 -3.3 -1.12 NDS NDS NDS 1 -1.12
0038 23.1 2.8 0.97 NDS 1.70 NDS 2 1.34 0.52
0039 19.7 -0.6 -0.19 1.04 -0.19 NDS 3 0.22 0.71
0040 19 -1.3 -0.43 -2.02 0.26 -5.76R 3 -0.73 1.17
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 17 -2.6 -0.90 -0.10 -0.17 -0.20 4 -0.34 0.37
0002 13.00 -6.6 -2.28 3 NDS -1.74 NDS 2 -2.01 0.38
0004 14.0 -5.6 -1.93 -0.31 -1.74 1.34 4 -0.66 1.52
0005 23 3.4 1.16 -0.10 -1.00 NDS 3 0.02 1.08
0007 18.5 -1.1 -0.39 0.06 0.15 -0.57 4 -0.19 0.35
0008 16 -3.6 -1.24 0.34 -1.16 0.17 4 -0.47 0.84
0009 22 2.4 0.82 -0.10 0.07 -1.77 4 -0.25 1.09
0011 20 0.4 0.13 0.55 0.73 0.21 4 0.41 0.28
0012 21 1.4 0.47 0.55 1.22 1.26 4 0.88 0.42
0013 18 -1.6 -0.56 -1.18 1.63 -0.03 4 -0.04 1.21
0014 22 2.4 0.82 1.42 0.81 NDS 3 1.02 0.35
0015 22 2.4 0.82 0.34 NDS 0.57 3 0.58 0.24
0016 17 -2.6 -0.90 -0.53 2.29 -0.59 4 0.07 1.49
0017 19.8 0.2 0.06 0.18 0.45 0.18 4 0.22 0.17
0022 18 -1.6 -0.56 -0.10 0.32 -0.14 4 -0.12 0.36
0024 17.5 -2.1 -0.73 NDS -1.00 -0.42 3 -0.72 0.29
0025 20 0.4 0.13 NDS -0.67 3.06 3 0.84 1.96
0026 23.61748 4.01748 1.37 0.77 0.32 NDS 3 0.82 0.53
0028 16 -3.6 -1.24 0.34 0.32 -0.20 4 -0.20 0.74
0029 19 -0.6 -0.21 -0.96 -0.50 0.02 4 -0.41 0.42
0031 21 1.4 0.47 NDS -1.65 NDS 2 -0.59 1.5
0032 17 -2.6 -0.90 0.12 NDS NDS 2 -0.39 0.72
0034 21 1.4 0.47 0.69 NDS NDS 2 0.58 0.16
0035 17.66 -1.94 -0.67 -1.13 0.23 -0.15 4 -0.43 0.59
0036 15 -4.6 -1.59 NDS NDS NDS 1 -1.59
0038 22.7 3.1 1.06 NDS 1.23 NDS 2 1.15 0.12
0039 20 0.4 0.13 1.20 -0.34 NDS 3 0.33 0.79
0040 17 -2.6 -0.90 -0.31 -0.17 0.83 4 -0.14 0.72
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 22 -3.2 -0.48 -0.70 -0.36 -0.13 4 -0.42 0.24
0002 17.43 -7.77 -1.17 NDS -0.82 NDS 2 -1.00 0.25
0004 19.9 -5.3 -0.80 -0.40 -0.97 1.18 4 -0.25 0.98
0005 48 22.8 3.45 1,3 -0.40 1.10 NDS 3 1.38 1.94
0007 30.6 5.4 0.82 -0.01 0.73 0.39 4 0.48 0.38
0008 27 1.8 0.28 1.95 -0.13 -0.71 4 0.35 1.14
0009 22 -3.2 -0.48 -0.55 -0.36 -1.37 4 -0.69 0.46
0011 29 3.8 0.58 0.77 0.10 0.18 4 0.41 0.32
0012 31 5.8 0.88 -0.11 1.33 -0.39 4 0.43 0.81
0013 24 -1.2 -0.18 -0.26 1.87 -1.68 4 -0.06 1.46
0014 28 2.8 0.43 0.77 0.33 NDS 3 0.51 0.23
0015 32 6.8 1.03 1.36 NDS 0.03 3 0.81 0.69
0016 22 -3.2 -0.48 -0.11 1.71 -1.19 4 -0.02 1.24
0017 27.3 2.1 0.32 -3.34 -0.38 -0.60 4 -1.00 1.61
0022 25 -0.2 -0.03 -0.11 0.41 0.12 4 0.10 0.23
0024 26.4 1.2 0.19 NDS -0.44 -0.34 3 -0.20 0.34
0025 38 12.8 1.94 NDS 0.26 0.60 3 0.93 0.89
0026 27.39197 2.19197 0.34 0.48 -0.30 NDS 3 0.17 0.42
0028 23 -2.2 -0.33 -0.11 1.71 -0.98 4 0.07 1.15
0029 25 -0.2 -0.03 -0.40 -0.36 -0.36 4 -0.29 0.17
0031 24 -1.2 -0.18 NDS -1.05 NDS 2 -0.62 0.62
0032 27 1.8 0.28 0.18 NDS NDS 2 0.23 0.07
0034 34 8.8 1.34 -0.18 NDS NDS 2 0.58 1.07
0035 25.19 -0.01 0.00 -0.32 -0.67 -0.08 4 -0.27 0.3
0036 32 6.8 1.03 NDS NDS NDS 1 1.03
0038 31.1 5.9 0.90 NDS 0.85 NDS 2 0.88 0.04
0039 25.8 0.6 0.10 0.48 -0.05 NDS 3 0.18 0.27
0040 27 1.8 0.28 0.04 0.49 1.73 4 0.64 0.75
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 102 -17.6 -0.76 0.25 0.16 0.26 4 -0.02 0.49
0002 84.96 -34.64 -1.50 NDS -0.76 NDS 2 -1.13 0.52
0004 93.2 -26.4 -1.14 0.01 -1.01 1.30 4 -0.21 1.13
0005 116 -3.6 -0.15 -0.97 -0.71 NDS 3 -0.61 0.42
0007 126.3 6.7 0.29 0.21 0.32 -0.25 4 0.14 0.27
0008 127 7.4 0.32 1.25 0.41 0.69 4 0.67 0.42
0009 118 -1.6 -0.07 -0.62 -0.18 -1.65 4 -0.63 0.72
0011 130 10.4 0.45 0.74 0.55 0.40 4 0.54 0.15
0012 146 26.4 1.14 1.02 1.14 1.20 4 1.13 0.08
0013 122 2.4 0.10 -0.50 1.82 -0.28 4 0.29 1.05
0014 119 -0.6 -0.03 1.18 0.41 NDS 3 0.52 0.61
0015 151 31.4 1.36 0.90 NDS 0.79 3 1.02 0.3
0016 117 -2.6 -0.11 -0.29 1.77 -0.31 4 0.27 1.01
0017 132.9 13.3 0.58 -4.78R 0.93 0.75 3 0.75 0.18
0022 115 -4.6 -0.20 0.60 0.70 0.23 4 0.33 0.41
0024 105.3 -14.3 -0.62 NDS -0.62 -0.48 3 -0.57 0.08
0025 107 -12.6 -0.54 NDS -0.67 1.28 3 0.02 1.09
0026 136.95882 17.35882 0.75 0.06 -0.04 NDS 3 0.26 0.43
0028 106 -13.6 -0.59 -0.52 0.41 -0.36 4 -0.27 0.46
0029 125 5.4 0.23 -0.52 -0.03 0.33 4 0.00 0.38
0031 98 -21.6 -0.93 NDS -1.69 NDS 2 -1.31 0.54
0032 100 -19.6 -0.85 0.27 NDS NDS 2 -0.29 0.79
0034 147 27.4 1.18 1.67 NDS NDS 2 1.43 0.35
0035 110.24 -9.36 -0.40 -1.08 -0.36 -0.54 4 -0.60 0.33
0036 99 -20.6 -0.89 NDS NDS NDS 1 -0.89
0038 151.5 31.9 1.38 NDS 0.95 NDS 2 1.17 0.3
0039 129 9.4 0.41 1.67 0.16 NDS 3 0.75 0.81
0040 125 5.4 0.23 0.27 0.99 1.48 4 0.74 0.6
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 44749 -12,379.3 -1.01 -0.38 -0.30 0.08 4 -0.40 0.45
0002 47356 -9,772.3 -0.80 NDS 0.16 NDS 2 -0.32 0.68
0004 42874.1 -14,254.2 -1.16 -0.07 0.43 1.13 4 0.08 0.96
0005 61989 4,860.7 0.40 1.07 0.05 NDS 3 0.51 0.52
0007 51410 -5,718.3 -0.47 0.51 0.32 1.33 4 0.42 0.74
0008 70714 13,585.7 1.11 -0.90 0.83 0.93 4 0.49 0.94
0009 53319 -3,809.3 -0.31 0.38 -0.91 -1.75 4 -0.65 0.9
0011 65467 8,338.7 0.68 -0.62 0.12 0.23 4 0.10 0.54
0012 68973 11,844.7 0.97 1.85 3.21 1.53 4 1.89 0.95
0013 52524 -4,604.3 -0.38 -0.14 0.24 -1.03 4 -0.33 0.53
0014 61992 4,863.7 0.40 -0.75 0.10 NDS 3 -0.08 0.6
0015 78709 21,580.7 1.76 -0.53 NDS 1.32 3 0.85 1.22
0016 45655 -11,473.3 -0.94 -0.04 0.27 -0.65 4 -0.34 0.55
0017 57853 724.7 0.06 2.52 0.81 -0.36 4 0.76 1.27
0022 54374 -2,754.3 -0.22 -0.94 0.41 0.03 4 -0.18 0.57
0024 39431 -17,697.3 -1.44 NDS -2.12 -1.60 3 -1.72 0.36
0025 58398 1,269.7 0.10 NDS 1.01 -1.16 3 -0.02 1.09
0026 58307.9 1,179.6 0.10 -2.13 -0.19 NDS 3 -0.74 1.21
0028 45412 -11,716.3 -0.96 -0.16 0.05 -0.35 4 -0.36 0.44
0029 58820 1,691.7 0.14 0.13 -0.40 -0.42 4 -0.14 0.31
0031 42308 -14,820.3 -1.21 NDS -1.83 NDS 2 -1.52 0.44
0032 51004 -6,124.3 -0.50 -0.47 NDS NDS 2 -0.49 0.02
0034 71650 14,521.7 1.18 1.72 NDS NDS 2 1.45 0.38
0035 43971.31 -13,156.99 -1.07 0.09 -0.90 -1.03 4 -0.73 0.55
0036 59400 2,271.7 0.19 NDS NDS NDS 1 0.19
0038 72473.2 15,344.9 1.25 NDS 5.01R NDS 1 1.25
0039 62531 5,402.7 0.44 -0.88 0.20 NDS 3 -0.08 0.7
0040 66022 8,893.7 0.73 0.38 1.81 1.30 4 1.06 0.63
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 20192 -4,441.6 -0.73 -0.08 0.52 0.26 4 -0.01 0.54
0002 21085 -3,548.6 -0.58 NDS 0.37 NDS 2 -0.11 0.67
0004 17134.3 -7,499.3 -1.24 -0.11 0.52 0.76 4 -0.02 0.89
0005 24798 164.4 0.03 1.16 -0.07 NDS 3 0.37 0.68
0007 22601 -2,032.6 -0.33 0.18 0.29 0.81 4 0.24 0.47
0008 29755 5,121.4 0.84 -0.65 0.94 0.78 4 0.48 0.75
0009 26411 1,777.4 0.29 0.62 -0.28 -1.28 4 -0.16 0.83
0011 28476 3,842.4 0.63 -0.51 0.38 0.23 4 0.18 0.49
0012 27538 2,904.4 0.48 1.31 1.22 1.16 4 1.04 0.38
0013 22069 -2,564.6 -0.42 -0.23 -0.04 -0.09 4 -0.20 0.17
0014 27718 3,084.4 0.51 -0.63 0.68 NDS 3 0.19 0.71
0015 30740 6,106.4 1.01 -0.37 NDS 1.32 3 0.65 0.9
0016 21712 -2,921.6 -0.48 0.17 0.29 0.00 4 -0.01 0.34
0017 15371 -9,262.6 -1.53 2.09 -0.08 -0.09 4 0.10 1.49
0022 24578 -55.6 -0.01 -0.69 -1.51 0.30 4 -0.48 0.8
0024 18434 -6,199.6 -1.02 NDS -1.60 -1.17 3 -1.26 0.3
0025 26136 1,502.4 0.25 NDS 0.89 -0.08 3 0.35 0.49
0026 29460.8 4,827.2 0.80 -2.45 0.37 NDS 3 -0.43 1.77
0028 20058 -4,575.6 -0.75 0.00 0.02 -0.38 4 -0.28 0.36
0029 28526 3,892.4 0.64 0.19 0.48 0.10 4 0.35 0.25
0031 15908 -8,725.6 -1.44 NDS -2.07 NDS 2 -1.76 0.45
0032 24253 -380.6 -0.06 -0.38 NDS NDS 2 -0.22 0.23
0034 31654 7,020.4 1.16 2.05 NDS NDS 2 1.61 0.63
0035 18852.62 -5,780.98 -0.95 0.06 -1.57 -0.33 4 -0.70 0.72
0036 25000 366.4 0.06 NDS NDS NDS 1 0.06
0038 29417.1 4,783.5 0.79 NDS NDS NDS 1 0.79
0039 28727 4,093.4 0.67 -0.48 0.88 NDS 3 0.36 0.73
0040 26708 2,074.4 0.34 0.27 1.63 0.47 4 0.68 0.64
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0007 0 -2 -0.60 -0.57 0.83 -0.71 4 -0.26 0.73
0013 11 9 2.70 3 1.57 -0.78 2.04 4 1.38 1.51
0016 6 4 1.20 1.57 -0.78 1.85 4 0.96 1.19
0017 27.9 25.9 7.76 R 2.46 -0.78 1.17 3 0.95 1.63
0026 0 -2 -0.60 NDS -0.78 NDS 2 -0.69 0.13
0043 0.75 -1.25 -0.38 -0.43 NDS NDS 2 -0.41 0.04
0051 0 -2 -0.60 -0.57 -0.78 0.70 4 -0.31 0.68
0057 0 -2 -0.60 NDS NDS NDS 1 -0.60
0060 3 1 0.30 -0.57 -0.78 -0.71 4 -0.44 0.5
0061 0 -2 -0.60 -0.57 1.01 NDS 3 -0.05 0.92
0064 19.2 17.2 5.15 R NDS -0.78 NDS 1 -0.78
0068 0 -2 -0.60 NDS NDS NDS 1 -0.60
0076 0.2 -1.8 -0.54 NDS 1.01 NDS 2 0.24 1.1
0085 9 7 2.10 3 1.78 NDS 0.83 3 1.57 0.66
0087 0.28 -1.72 -0.52 -0.57 NDS NDS 2 -0.55 0.04
0089 0.00 -2 -0.60 -0.57 NDS NDS 2 -0.59 0.02
0096 0 -2 -0.60 -0.57 NDS NDS 2 -0.59 0.02
0099 5.8 3.8 1.14 NDS NDS NDS 1 1.14
0107 1 -1 -0.30 -0.36 1.90 -0.69 4 0.14 1.19
0108 0.18897 -1.81103 -0.55 -0.57 7.24R -0.71 3 -0.61 0.09
0117 0 -2 -0.60 -0.57 -0.78 -0.71 4 -0.67 0.1
0121 0 -2 -0.60 -0.14 NDS NDS 2 -0.37 0.33
0127 5 3 0.90 NDS NDS NDS 1 0.90
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0007 29.7 7.6 0.55 0.52 2.29 0.57 4 0.98 0.87
0043 36.7 14.6 1.06 0.72 NDS NDS 2 0.89 0.24
0051 0 -22.1 -1.60 -1.36 -0.63 -0.80 4 -1.10 0.46
0057 15.1 -7 -0.51 NDS NDS NDS 1 -0.51
0060 25 2.9 0.21 0.52 -0.63 0.98 4 0.27 0.68
0061 28 5.9 0.43 0.40 1.31 NDS 3 0.71 0.52
0063 27 4.9 0.36 0.40 NDS NDS 2 0.38 0.03
0064 19.2 -2.9 -0.21 NDS -0.63 NDS 2 -0.42 0.3
0068 0 -22.1 -1.60 NDS NDS NDS 1 -1.60
0076 28.1 6 0.44 NDS -0.63 NDS 2 -0.10 0.76
0087 30.08 7.98 0.58 0.58 NDS NDS 2 0.58 0
0089 23 0.9 0.07 -0.07 NDS NDS 2 0.00 0.1
0096 30 7.9 0.57 0.34 NDS NDS 2 0.46 0.16
0099 0 -22.1 -1.60 NDS NDS NDS 1 -1.60
0107 33 10.9 0.79 0.76 1.31 1.00 4 0.97 0.25
0108 26.76 4.66 0.34 -0.33 12.99R -0.73 3 -0.24 0.54
0117 0 -22.1 -1.60 -0.33 -0.63 -0.72 4 -0.82 0.55
0121 46 23.9 1.74 -0.51 NDS NDS 2 0.62 1.59
StdDev
Lab Code DGA1808 Result Dev Z 1808 Notes 1802 1708 1702 Z Count Avg Z
Z-Score
0001 9.6 -0.4 -0.11 0.13 2.08 NDS 3 0.70 1.2
0005 34 24 6.40 R -0.91 -0.68 NDS 2 -0.80 0.16
0008 7 -3 -0.80 NDS -0.27 NDS 2 -0.54 0.37
0011 7 -3 -0.80 -1.20 -0.27 NDS 3 -0.76 0.47
0012 7 -3 -0.80 -0.01 0.33 NDS 3 -0.16 0.58
0013 15 5 1.33 1.47 1.94 NDS 3 1.58 0.32
0015 9 -1 -0.27 0.28 NDS NDS 2 0.01 0.39
0016 15 5 1.33 0.58 1.54 NDS 3 1.15 0.5
0017 7.0 -3 -0.80 -0.31 -1.58 NDS 3 -0.90 0.64
0021 6 -4 -1.07 -1.20 NDS NDS 2 -1.14 0.09
0026 15.30 5.3 1.41 5.93R NDS NDS 1 1.41
0029 3 -7 -1.87 -0.61 -2.89 NDS 3 -1.79 1.14
0032 8 -2 -0.53 NDS NDS NDS 1 -0.53
0035 4.7 -5.3 -1.41 3.25 NDS NDS 2 0.92 3.3
0040 8 -2 -0.53 2.36 -1.48 NDS 3 0.12 2
0041 7 -3 -0.80 -1.20 -0.27 NDS 3 -0.76 0.47
0042 8 -2 -0.53 -0.91 -0.27 NDS 3 -0.57 0.32
0043 8 -2 -0.53 NDS NDS NDS 1 -0.53
0047 14 4 1.07 0.28 0.13 NDS 3 0.49 0.51
0049 10 0 0.00 -0.01 0.13 NDS 3 0.04 0.08
0051 10 0 0.00 NDS NDS NDS 1 0.00
0052 15 5 1.33 -0.01 NDS NDS 2 0.66 0.95
0054 8 -2 -0.53 -0.67 0.94 NDS 3 -0.09 0.89
0056 10 0 0.00 -1.20 -0.68 NDS 3 -0.63 0.6
0059 12.0 2 0.53 NDS NDS NDS 1 0.53
0061 21 11 2.93 3 NDS 0.13 NDS 2 1.53 1.98
0065 9 -1 -0.27 6.52R 3.15 NDS 2 1.44 2.42
0066 3 -7 -1.87 -1.50 -1.28 NDS 3 -1.55 0.3
Lab - 0001
General Comments Nothing abnormal to report
Lab - 0002
General Comments We observed air bubble in the sample syringe when received (slightly
less than 1 ml)
PTP Response: As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.
Lab - 0013
General Comments Sample Number No 211781
Lab - 0035
General Comments We thank you for your efforts
Lab - 0038
General Comments The document pouch was not fully sealed down, but the paperwork did
not come out in transit.
Lab - 0052
General Comments Gas bubble was present in the syringe. PTP Response: As long as the
air bubbles weren't larger than 10ml, it's always ok to agitate the sample
back and forth and continue with testing.
Lab - 0059
General Comments There are bubbles in the sample。PTP Response: AS long as the air
bubbles weren't larger than 10ml; it's always ok to agitate the sample
back and forth and continue with testing.
Lab - 0061
General Comments The sample contained a large bubble. PTP Response: As long as the air
bubbles weren't larger than 10ml, it's always ok to agitate the sample
back and forth and continue with testing.
Lab - 0066
General Comments Moisture - automated method
Lab - 0067
Lab - 0069
General Comments All OK
Lab - 0070
General Comments no comment
Lab - 0071
General Comments Not sure why two lab results for Hydrogen and Co are different.
Lab - 0073
General Comments A bubble of approximately 1 ml or more was present in the syringe. It
could not be dissolved completely. A small bubble persisted. In an effort
to completely dissolve the bubble, the continuous pressure applied by
hand on the plunger allowed for traces of oil to leak past the plunger.
PTP Response; As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.
Lab - 0076
General Comments The sample was received in order by Witbank Lab Syringe no.:31405 ,
DGA1808
Lab - 0077
General Comments Syringe contained 0.5ml bubble.
PTP Response: As long as the air bubbles weren't larger than 10ml, it's
always ok to agitate the sample back and forth and continue with testing.
Lab - 0092
General Comments Box arrived very quickly and in good state.
Lab - 0101
General Comments The syringe number for JHB LAB is 31001
Lab - 0125
General Comments Good morning, we have had problems with the contact address, we hope
that the same will not happen for the next evaluation
PTP Response: ASTM PTP will contact you to verify all shipping
information.