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Petrophysical Measurements From Drill

Cuttings: An Added Value for the


Reservoir Characterization Process
P. Egermann, N. Doerler, M. Fleury, J. Behot, F. Deflandre, and R. Lenormand, Inst. Français du Pétrole (IFP)

Summary Indirect Permeability-Evaluation Methods From Cuttings.


The permeability is derived using empirical correlations with prop-
Permeability and porosity are necessary for reservoir characteriza-
tion, and cuttings can provide quick information using dedicated erties related to pore-size distribution, pore connectivity, or the
measurement techniques. In this paper, we present the first appli- spatial correlation between the pores. These parameters are evalu-
cations of these techniques on real reservoir characterization cases ated from capillary properties (mercury porosimetry) by NMR or
and the comparisons with logs and core data. image analysis.
The method of permeability measurement from cuttings is Several approaches have been proposed to derive permeability
based on a pressure pulse applied to a cell filled initially with from mercury porosimetry curves (Purcell 1949; Thomeer 1960,
cuttings saturated with viscous fluid in the presence of trapped gas. 1983; Swanson 1981; Katz and Thompson 1986). Kamath (1992)
The permeability is derived from the transient response of the oil performed a comparison between these methods and concluded
invasion into the cuttings by using a numerical approximation of a that the best result is obtained with new correlations based on the
mathematical model. The porosity of dry drill cuttings is measured Swanson characteristic length. In addition, Kamath and Swanson
using the routine helium technique. These methods were tested and each reported a possible use of mercury porosimetry curves ob-
validated by using various samples of crushed rock of known tained from cuttings.
permeability and porosity. Both measurement techniques are fast, Many papers have been published on permeability evaluation
require light conditioning, are applicable over a large range of from NMR measurements, but very few refer to its application on
permeability, and need only 1 mL of sieved rock to be carried out. cuttings. A major effort was conducted by Chevron, which resulted
In this paper, we present a field application of an integrated in prototype equipment fitted for rig conditions (Nigh and Taylor
drill cuttings measurement program [permeability, porosity, 1985). The cuttings are first prepared (cleaned and dried) and
nuclear magnetic resonance (NMR) T2 distribution] on a carbonate placed in a portable NMR tool. The porosity is derived from the
reservoir. Various drilling conditions [including water-based mud measured volume of water, and permeability is evaluated from the
(WBM) and oil-based mud (OBM)] and lithologies have been whole T2 relaxation signal using the Timur law (Timur 1968).
investigated to develop the different techniques that are presented Recently, this approach has been subject to further developments
in the paper. The question of whether measurements on cuttings (Mirotchnik et al. 2004).
are representative of the native reservoir is of primary importance A thin section also can be obtained from cuttings to evaluate
and was checked by comparing the consistency of the porosity the porosity and the permeability using image analysis. The po-
measurements obtained from cuttings with other data (cores or rosity corresponds to the fraction of voids, whereas the permeabil-
logs). The overall results demonstrate the added value of k and ␾ ity is derived from an empirical law (Coskun and Wardlaw 1993;
measurements from cuttings in addition to the data that are com- Ioannidis et al. 1996) or from Carman-Kozeny type laws (Fens
monly collected. et al. 1998).
Direct Permeability-Evaluation Methods From Cuttings. Few
methods exist to measure permeability directly from cuttings. San-
Petrophysical Methods in the Reservoir tarelli et al. (1998) proposed imbedding cuttings into disks of
Characterization Process acrylic resin. The disks are surfaced and mounted in a core holder
The early determination of rock petrophysical properties is one of to measure permeability under constant-flow or transient-flow
the main concerns during the reservoir characterization process conditions. Another method, which is based on gas pressure dif-
because it directly impacts the hydrocarbon in place (porosity, fusion, was proposed by Luffel (1993). Cleaned and dried cuttings
saturation) and the well deliverability (permeability). If these prop- are placed in a cell at atmospheric pressure. The cell is then placed
erties are available during the drilling process, they also can be in communication with another cell under pressure, and the de-
used for drilling steering. Logs generally provide a good estimate crease of the pressure in the latter is interpreted in terms of per-
of porosity and saturation along the well, but permeability is more meability. The principle is similar to well testing, using gas instead
difficult to obtain because this parameter refers to conductance of of liquids. However, because of the low viscosity of gases, this
the reservoir rock to flow. method can be used only on very-low-permeability rocks.
Recently, we presented an original method to measure the per-
Routine Cuttings Analysis. Cuttings are used routinely by mud meability directly from drill cuttings (Egermann et al. 2005). The
loggers to build the “master log,” in which the geological descrip- proposed method does not require specific conditioning, is easy to
tion of the drilled formation is reported. Hydrocarbon indices also apply, and provides results consistent with core analysis and with
are determined from cuttings to identify the reservoir rock. Al- typical ranges of reservoir permeability.
though cuttings rock material is coming directly from the reservoir, In this paper, we present how to integrate these direct petro-
few applications of permeability characterization are reported in physical measurements from samples of drill cuttings with other
the literature. The published works can be divided into two cat- data (e.g., logs, core) obtained during the reservoir characterization
egories: direct and indirect evaluations. process. In the first part of the paper, we recall the principles of our
permeability-measurement technique and the latest improvements
that were introduced to allow the measurement on small volumes
of cuttings (on the order of 1 mL). Then, some results related to the
Copyright © 2006 Society of Petroleum Engineers
porosity measurement from cuttings using existing techniques are
This paper (SPE 88684) was first presented at the 2004 Abu Dhabi International Petroleum shown. The general approach to integrate the measurements from
Exhibition and Conference, Abu Dhabi, 10–13 October, and revised for publication. Original
manuscript received for review 7 December 2004. Revised manuscript received 17 May
cuttings with other available data is then described and applied to
2006. Paper peer approved 30 May 2006. a real case in the last section. The results confirm the added value

302 August 2006 SPE Reservoir Evaluation & Engineering


of the measurements from cuttings provided that they are repre-
sentative of the native reservoir.

Petrophysics From Drill Cuttings


Permeability-Measurement Technique. Principle of the
Method. The main issue in determining permeability from cuttings
is to establish flow into the rock itself rather than in intercuttings
space. The originality of the proposed method is to achieve an
effective flow inside the cuttings by compression of residual gas
that they contain. Viscous oil is used as displacing fluid to decrease
the pressure-diffusion kinetics into the rock. It enables measure-
ment of permeability values corresponding to reservoir rocks,
which are not accessible from the gas pressure test (Luffel 1993).
The method has been tested and validated with an experimental
prototype and interpretation software to derive permeability values
from the experimental data (Egermann et al. 2005).
Fig. 1—Experimental apparatus working with small volumes of
Dealing With Small Volumes of Cuttings. The original appa-
cuttings.
ratus described in the previous section enabled us to develop the
method but required a significant volume of cuttings (50 mL). It
appeared from our first measurements on real cuttings that this
volume should be significantly reduced for several reasons: the prototype apparatus, the cuttings cell was pressurized to 10 bar
• The available volume and number of drill cuttings at the using a large volume of nitrogen in the pressurized cell. Now, we
wellhead in the desirable range of size (2 to 3 mm) can vary widely use a nitrogen volume of the same order as the trapped gas to
according to the nature of the rock, the drill bit, and the type of compress in the cuttings cell (Fig. 1). It pressurizes the cuttings in
well (vertical, slanted, or horizontal). Therefore, only a few mil- two steps. Initially, the pressure in the cuttings quickly reaches 10
liliters of cuttings are often retrieved from the well over several bar (the initial pressure in the nitrogen) owing to the instantaneous
meters of drilled reservoir. compression of the intercuttings space filled with liquid. Then, the
• The raw cuttings coming out from the well need to be cleaned pressure decreases and finally stabilizes with the pressure diffusion
from the mud. This operation may be time consuming depending inside the cuttings, which compresses the trapped gas inside.
on the mud type. Whereas water-based mud cuttings require only Therefore, this procedure
a simplified cleaning procedure with synthetic brine, oil-based • Still enables us to pressurize the cuttings with viscous oil.
mud cuttings need the use of solvents to remove the oil phase from • Permits easier calculation of the volume of oil injected from
the pore space. Because of the simplicity of the technique, it is our the volume of the gas cap, which is a direct function of the re-
experience that the time spent to clean the cuttings thoroughly can corded pressure (Boyle’s law).
be as long as the time spent to run the measurement itself. A • Simplifies the apparatus because only one absolute pressure
reduction of the cuttings volume is then important to reduce the gauge is needed to evaluate the volume of oil injected as a function
costs associated with the measurement. of time.
• A mixing of several lithologies is sometimes observed after • Makes the interpretation process easier to handle because the
the cleaning process. This can result from the presence of lamina- pressure variation at the edge of the cuttings is recorded.
tions, mixing, or patchy lithology. A sorting process is then needed • Requires smaller volumes of cuttings for measurements; con-
before measurement. Such sorting cannot be handled on large sequently, only 1 mL is necessary with the new procedure.
volumes of cuttings. Fig. 2 illustrates the cumulative oil injected as a function of
• The technique also has a wide field of application on sets of time using the new apparatus. It is now possible to work with a
old cuttings, although the available volumes are often very limited. smaller volume of oil injected on the order of 0.03 cm3, which is
The main emphasis of the present approach was the develop- two orders of magnitude lower than what was required in the
ment of a new system with improved accuracy and flexibility and previous apparatus.
less sensitivity to the ambient conditions (mainly the temperature Fig. 3 shows the good agreement between the core permeability
that affected the calibration of the previous system, which was and the cuttings permeability obtained from crushed core samples
based on the measurement of pressure drop in a capillary tube). In (size 2–3 mm) using the new apparatus.

Fig. 2—Experimental results with 1-cm3 cuttings.

August 2006 SPE Reservoir Evaluation & Engineering 303


Fig. 4—Principle of the powder pycnometer.

fully to remove all brine located in the intercuttings space; other-


wise, this would have led to erroneous evaluation of porosity and
incorrect values of the T2 peak. This was achieved by capillary
desorption using a semipermeable membrane.
Fig. 3—Comparison between core and cuttings permeability Before the measurement, the total volume of the cuttings is
with small volumes of cuttings. measured with the powder pycnometer for porosity assessment.
Then, the saturated cuttings are introduced in the NMR tool, and
both the volume of brine contained in the rock and the T2 distri-
Porosity-Measurement Technique. We followed an approach bution are obtained. The volume of brine corresponds to the pore
similar to that reported by Meazza et al. (1996) to measure the volume, leading to the determination of porosity using the total
porosity and the grain density (Marsala et al. 1997). We followed volume method. The T2 distribution obtained from cuttings is very
the classical methods of standard core analysis. The solid volume similar to the one obtained from a core (Fig. 6). This feature is
was determined using the gas expansion method. The grain density particularly interesting for permeability estimates from T2, as
is then obtained from the weight of the dry cuttings. The total pointed out by Mirotchnik et al. (2004).
volume of the cuttings was measured with a powder pycnometer Fig. 7 illustrates the variability of the T2 distribution obtained
(Micromeretics). The principle of the method relies on the use of from a set of cuttings samples that corresponds to different lithol-
a size-calibrated powder, which can occupy all the space between ogies and permeabilities. It demonstrates that such measurements
the cuttings (Fig. 4). The volume of powder is first measured for on cuttings
calibration. Then, the cuttings are introduced into the piston, and • Can give a fast evaluation of key features of the rock.
the total volume is deduced by difference with the preliminary • Can provide a useful link between the direct permeability
calibration test. For 2- to 3-mm cuttings, the apparatus needs ac- measurements made from cuttings and NMR logs of the reservoir.
curate calibration with nonporous rocks of similar shape and size Bringing these data together can improve calibration and confi-
to provide consistent results. The cuttings porosity is then derived dence in terms of permeability prediction from NMR.
from the associated solid volume obtained with helium.
This approach was tested with measurements on crushed core Integration of Cuttings Measurements
cuttings. The good agreement obtained with the core porosity val- Representativity Issue. From the moment the cuttings are gener-
ues confirmed the results found by Meazza et al. (1996). All the ated downhole by the drilling tool until the moment at which they
measurements made from the cuttings fall within a 2-porosity-unit are collected at the shakers, the representativity of the cuttings with
(P.U.) error bar (Fig. 5). respect to the native reservoir can be lost for several reasons:
• The lag-time calculation is of primary importance to identify
NMR Measurement From Cuttings. The NMR technique can which reservoir levels the cuttings are coming from. This calcu-
provide both a porosity measurement and the main value of T2, lation is often considered to be accurate for vertical wells (on the
which is widely used for log interpretation for permeability esti-
mation. The cuttings were saturated with 20 g/L NaCl brine before
the NMR measurement. The cuttings samples were prepared care-

Fig. 5—Comparison between core and cuttings porosity. Fig. 6—T2 distribution on core and cuttings.

304 August 2006 SPE Reservoir Evaluation & Engineering


were subjected to an ultrasonic apparatus. The bottom picture
shows the surface of the cuttings after this cleaning process. The
quartz grains that constitute the sandstone can be clearly identified,
and some open pores even appear visible.

Integration With Other Data. The integration of the cutting mea-


surements must be done with the help of all the other reservoir data
that are available. This is very similar to the quick-look approach
used to interpret the logs. Every log brings one piece of the infor-
mation to evaluate the consistency and representativity of the data.
For example, because porosity is a petrophysical property, which
is well-determined from logs in most cases, it can be used to check
the cuttings representativity.
Several other examples have been encountered. The cuttings
porosity log can exhibit the same shape as the traditional porosity
log but with a systematic shift. Here, it means that the lag-time
calculation needs to be revisited. If the porosity values differ sig-
nificantly from the logs, then the grain density can be very helpful
Fig. 7—T2 distribution obtained on eight different cuttings to identify if the differences result from insufficient cleaning (po-
rock samples. rosity and grain density are different) or from the interpretation of
the logs. The rock description also can identify possible problems
order of a meter) but can lead to significant errors in deviated and related to the mixing of cuttings coming from several locations
horizontal wells. within the reservoir (mixing during the drilling operation).
• Depending on the nature of the rock (e.g., vuggy and uncon- When the representativity control is successful, then the per-
solidated rocks) and the type of drilling bit (PDC is very destruc- meability measurements are conducted. It is possible to use these
tive), the cuttings retrieved from the well may not constitute a direct measurements with other available data to identify the best pay
representative elementary volume of the native rock. For these intervals to draw a permeability/porosity correlation according to the
reasons, 2- to 3-mm cuttings are recommended. This, however, rock types or improve the log calibration. Fig. 9 shows the general
does not ensure that the representativity issue is respected. workflow, which takes into account the cuttings measurements in
• The raw cuttings are dirty because they have been contami- the calibration of the coefficients for NMR permeability prediction.
nated by the drilling mud. The deposition of mud solid particles
Field Application
can modify the rock structure and the petrophysical properties. The
presence of remaining fluids can also lead to erroneous results. The following field example concerns a carbonate reservoir drilled
Therefore, a cleaning procedure tailored to the drilling-mud type with a WBM. A light cleaning procedure without solvents was
(OBM or WBM) must be conducted to restore the native properties used to condition the cuttings. Porosity data obtained from cuttings
of the rock. measurements are compared with NMR log data in Fig. 10 for two
The efficiency of the cleaning procedure that has been devel- different wells. A very good consistency was found in the two
oped through our experiences with field cuttings is shown in cases; therefore, the cuttings were considered representative of the
Fig. 8. The top picture shows an example of the cuttings as re- native reservoir.
ceived in the laboratory from the field. The presence of a shell of The NMR coefficients calibration approach for permeability
fine solid particules surrounding the rock can be observed easily prediction was validated with a series of cores from this reservoir.
under the microscope. In this case, the cuttings were cleaned with Eight samples belonging to the same rock type were taken from
fresh synthetic reservoir brine and solvents. Then, the cuttings cored intervals. The permeability, porosity, and NMR were first
measured on the cores. Then, each core was crushed, and the same
type of measurements were conducted on the cuttings. All the
results are gathered in Table 1.
The Kenyon expression was used to determine the permeability
value from NMR, as suggested by Fleury (2001).

k = C T 2a peak ␾b. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . (1)


The default parameters recommended for carbonate rock are
C⳱0.1, a⳱2, and b⳱4. The results obtained using these param-

Fig. 8—Cleaning process. Fig. 9—Calibration of coefficients for NMR permeability prediction.

August 2006 SPE Reservoir Evaluation & Engineering 305


Fig. 10—Porosity logs from NMR and cuttings.

eters are gathered in Table 1 and plotted in Fig. 11. It can be wells, such as completion design optimization, permeability/
observed that the standard deviation from the core permeability is porosity correlation, and log calibration. This last point is particu-
on the order of one decade, which is not satisfactory in the context larly interesting in carbonate reservoirs for which NMR perme-
of the reservoir characterization process. ability predictions are uncertain when standard calibration coeffi-
The parameters were then optimized using both the T2 peak and cients are used.
the direct measurement obtained from cuttings. The following val-
Nomenclature
ues were determined: C⳱0.0086, a⳱1.15, and b⳱1.57.
The results obtained with the new parametrization show an ⳱ coefficients of Kenyon’s law a, b, C
improved agreement with the core measurements. The standard k ⳱ permeability
deviation decreases approximately to 0.25 decade (Fig. 12), com- ␾ ⳱ porosity
pared to one decade with the default parameters. T2 ⳱ transverse NMR relaxation time
The optimized expression then can be applied to the whole log
Acknowledgments
NMR data set, where direct measurements on core or cuttings are
not available. Because the reservoir rocks frequently are divided The authors want to thank IFP for permission to publish these results.
into rock types, the calibration process has to be repeated for each References
of them to obtain accurate NMR permeability prediction over the Coskun, S.B. and Wardlaw N.C. 1993. Estimation of Permeability From
entire reservoir section. Image Analysis of Reservoir Sandstones. J. of Petroleum Science and
Engineering 10 (1): 1–16.
Conclusions Egermann, P., Lenormand, R., Longeron, D., and Zarcone, C. 2005. A Fast
In this paper, we have illustrated the application of a new perme- and Direct Method of Permeability Measurements on Drill Cuttings.
ability-measurement technique on real cuttings and demonstrated SPEREE 8 (4): 269–275. SPE-77563-PA.
their added value in terms of petrophysical characterization. The Fens, T.W., Kraaijveld, M.A., Riepe, L. et al. 1998. Archie’s Dream:
different types of measurements that are performed on the cuttings Petrophysics From Sidewall Sample and Cuttings. Paper presented at
(permeability, porosity, and NMR) enable assessment of the rep- the Soc. of Core Analysts Intl. Symposium, The Hague, 14–16 Sep-
resentativity of the cuttings with respect to the native reservoir and tember.
bring added value to other existing data. Fleury, M. 2001. Validity of permeability prediction from NMR measure-
Therefore, the proposed approach for reservoir characterization ment. Paper presented at the GERM Annual Meeting, La Pommeray,
with cuttings has many practical applications on new or existing France, 14–18 May.

306 August 2006 SPE Reservoir Evaluation & Engineering


Fig. 11—NMR permeability prediction using default coefficients. Fig. 12—NMR permeability prediction using coefficients opti-
mized with cuttings permeability.
Ioannidis, M.A., Kwiecien, M.J., and Chatzis, I. 1996. Statistical Analysis
of the Porous Microstructure as a Method for Estimating Reservoir Timur, A. 1968. An Investigation of Permeability, Porosity and Residual
Permeability. J. of Petroleum Science and Engineering 16 (4): 251– Water Saturation Relationships. Paper presented at the SPWLA Annual
261. Logging Symposium, New Orleans, 23–26 June.
Kamath, J. 1992. Evaluation of Accuracy of Estimating Air Permeability
From Mercury-Injection Data. SPEFE 7 (4): 304–310; Trans., AIME,
293. SPE-18181-PA. SI Metric Conversion Factors
Katz, A.J. and Thompson, A.H. 1986. Quantitative Prediction of Perme-
in.3 × 1.638 706 E+01 ⳱ cm3
ability in Porous Rock. Physical Review 34: 8179–8181.
Luffel, D.L. 1993. Devonian Shale Matrix Permeability Successfully Mea-
sured on Cores and Drill Cuttings. Gas Shales Technology Review Patrick Egermann is a research petroleum engineer with the
8 (2): 46–55. Inst. Français du Pétrole (IFP), currently working on multiphase-
Marsala, A.F., Meazza, O., and Rossi, E. 1997. Petrophysical Character- flow and gas-injection processes, including CO 2 . e-mail:
ization of Reservoir Rocks by Measurements on Cuttings. Paper pre- patrick.egermann@ifp.fr. Egermann holds MS degrees in reser-
sented at the Offshore Mediterranean Conference and Exhibition, voir engineering (from the IFP school) and hydraulic/fluid me-
chanics (from ENSEEIHT) and a PhD degree in earth sciences
Ravenne, Italy.
and environment from the U. of Toulouse. Françoise Deflandre
Meazza, O., Della Martera, M., and Lyne, A. 1996. Porosity From Cut- is a research engineer with IFP and is involved mainly in labo-
tings: Options and Answers. Paper SCA 9606 presented at the Soc. of ratory studies focusing on NMR and resistivity measurements
Core Analysts Symposium, Montpellier, France, 8–10 September. and interpretations. Marc Fleury holds an engineering degree
Mirotchnik, K., Ktyuchkov, S., and Strack, K. 2004. A Novel Method To in physics from the Ecole Polytechnique de Lausanne (Switzer-
Determine NMR Petrophysical Parameters From Drill Cuttings. Paper land) and a PhD degree in fluid mechanics from the Fourier U.
presented at the SPWLA 45th Annual Logging Symposium, The Neth- of Grenoble (France). Before joining the Inst. Français du Pé-
erlands, 6–9 June. trole (IFP) in 1992, Fleury worked in the field of physical ocean-
Nigh, E. and Taylor, M. 1985. Wellsite Determination of Porosity and ography at the Johns Hopkins U. in Baltimore, Maryland, and at
the U. of Victoria, Canada, studying turbulent mixing and
Permeability Using Drilling Cuttings. Paper presented at the 10th For-
double diffusive instability. He is now working as a senior petro-
mation Evaluation Symposium of the Canadian Well-Log Soc. physicist in special core analysis; his main interest is in electric
Purcell, W.R. 1949. Capillary Pressures—Their Measurement Using Mer- and NMR properties of porous media. Roland Lenormand
cury and the Calculation of Permeability Therefrom. Trans., AIME worked in academic research at the CNRS in Toulouse
186: 39–48. (France) for 10 years; his research was on the theory of mul-
Santarelli, F.J., Marsala, A.F., Brignoli, M., Rossi, E., and Bona, N. 1998. tiphase flow in porous media, focusing on the use of network
Formation Evaluation From Logging on Cuttings. SPEREE 1 (3): 238– modeling and percolation theory. e-mail: roland.lenormand@
244. SPE-36851-PA. ifp.fr. Afterward, he joined Schlumberger in Ridgefield and
Swanson, B.F. 1981. A Simple Correlation Between Permeabilities and Dowell Schlumberger in France, where he worked on carbon-
ate acidizing. Lenormand joined the reservoir department of
Mercury Capillary Pressures. JPT 33 (12): 2498–2504. SPE-8234-PA.
IFP in 1988 and has been involved in various experimental and
Thomeer, J.H.M. 1960. Introduction of a Pore Geometrical Factor Defined simulation aspects of petrophysics. His area of expertise also
by the Capillary Pressure Curve. Trans., AIME 219: 354–358. includes heavy oils and upscaling. Lenormand holds a PhD
Thomeer, J.H.M. 1983. Air Permeability as a Function of Three Pore- degree in theoretical physics from the U. of Paris. Bios for
Network Parameters. SPEJ 23 (2): 809–814. SPE-10922-PA. N. Doerler and J. Behot were not available.

August 2006 SPE Reservoir Evaluation & Engineering 307

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