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WELDING RESEARCH
SUPPLEMENT TO THE WELDING JOURNAL, DECEMBER 2017
Sponsored by the American Welding Society and the Welding Research Council

Repairing Ultrasonic Welded


Carbon Fiber­Reinforced Nylon 66 Composite
Application of a second ultrasonic vibration not only restored
joint strength but also decreased the scatter in weld strength

BY L. LU, Q. ZHI, Y.-H. GAO, Z.-X. LIU, AND P.-C. WANG

in lightweight vehicle structures (Refs.


ABSTRACT 18–23). Despite these advantages, the
use of ultrasonic welding in vehicle
In this study, a method for repairing partially welded carbon fiber­reinforced nylon 66
structural applications has been limit-
composite joints with ultrasonic welding was developed. The method included position­
ing the ultrasonic horn and anvil proximate the weld, and applying an ultrasonic vibration ed, partly because of concerns regard-
at substantially the same location on the existing welds fabricated by introducing a sepa­ ing weld quality inspection and weld
ration of 0.7 mm (0.03 in.) between 4­mm­ (0.16­in.­) thick carbon fiber­reinforced nylon repair.
66 workpieces. Welding tests were performed and the welded joints were quasi­static It has been shown that alignment
tested and analyzed. It was found that the separation between the workpieces and leveling of a welding fixture, a
influenced the contact between them, and consequently resulted in variations in weld welding horn, and the workpieces dur-
area and weld strength. The welds were repaired by applying the second ultrasonic vibra­ ing ultrasonic welding are critical for
tion with the proper energy intensity under the same horn pressure. The application of a formation of an ultrasonic weld (Ref.
second ultrasonic vibration not only restored the joint strength but also decreased the 24). When the warped workpiece is
scatter in strength of the welds. Microstructure analyses of the repaired welds revealed
positioned near a second workpiece
the main mechanism for repairing the ultrasonic welds was the increase in weld area
caused by melting of the materials at the periphery of the existing weld between the for joining, a separation is present be-
workpieces. The application of the repair method would reduce the potential need to tween the workpieces. The space be-
scrap the particular component assembly. tween the workpieces can lead to im-
proper weld formation. Therefore,
there is an urgent need to develop a
KEYWORDS method to inspect the weld quality
and repair the partially joined (or
• Carbon Fiber­Reinforced Nylon 66 Composite • Ultrasonic Weld • Flawed Joint flawed) welds in ultrasonic welding of
• Repair • Repair Mechanism
thermoplastic composites.
Weld quality can be confirmed off-
Introduction ing the composite parts (Refs. 6–11), line from the production operation by
there is a need to understand the join- periodically removing the workpieces
Ever-increasing fuel economy, envi- ing of carbon fiber thermoplastic com- from the operation and physically ex-
ronmental, and mechanical perform- posite for automotive applications. amining and testing a number of weld
ance requirements in the automotive Various joining techniques such as nuggets. Nevertheless, it would be
industry make the high strength-to- adhesive bonding, mechanical fasten- preferable to have an on-line process
weight ratio associated with carbon ing, and fusion welding are available that could be performed during the
fiber/nylon composite attractive (Refs. for joining thermoplastics (Refs. 12, welding operation to assess welding
1–4). They offer greater strength and 13). Among all of these methods, ul- conditions and weld nugget quality
better structural crashworthiness trasonic welding is particularly prom- and size. Many studies (Refs. 25–28)
when compared with other lightweight ising (Refs. 14–17). Ultrasonic welded have reported that the weld quality
materials (e.g., aluminum and magne- thermoplastic composite is known to could be reflected by various signals
sium) (Ref. 5). While a great deal of ef- have good stiffness and strength (i.e., ultrasonic wave and process sig-
fort has been focused on developing (Refs. 14, 15), providing a potentially natures, power, meltdown, etc.).
the carbon fiber composites and mold- wide range of applications, especially Among these techniques, an in-situ

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WELDING RESEARCH

monitoring method through power


and displacement data was particular- A
ly promising (Ref. 26). Based on this
concept, an on-line method of moni-
toring the target horn displacement
and welding time of stable phase of
melt film has been developed for weld
quality inspection (Ref. 29). The pur-
pose of the present study was to devel-
op a method for repairing the flawed
joints. We first conducted tests to
study the correlation between the
weld area and strength of the welded
4-mm- (0.16-in.-) thick carbon fiber-
reinforced nylon 66 composite. Then,
the partially welded joints were fabri-
cated by introducing a separation of
0.7 mm (0.03 in.) between two work-
pieces. A second ultrasonic vibration
was applied to repair the welds and the
repair mechanism was examined. Fi-
nally, the criterion used for the devel-
opment for repairing the ultrasonic B
welded carbon fiber thermoplastic
composite and significance of the re-
pair method for vehicle structural as-
sembly were discussed.

Experimental Procedure
Materials
Commercial nylon 66 and carbon
fiber (24K, T300 type, Toray Carbon
Magic Co. Ltd.) with a length of 2 mm
(0.08 in.) were selected for this study.
Per the manufacturer’s data sheet, the
material properties of these materials
are given in Table 1.

Injection Molding Carbon Fiber­


Reinforced Nylon 66 Composite
Fig. 1 — A — Schematic; B — photo of the specific equipment and setup for ultrasonic
Carbon fibers were first cleaned welding of injection­molded carbon fiber­reinforced nylon 66 composite.
with a concentrated solution of nitric
acid and then surface pretreated using the carbon fiber-reinforced nylon 66 hopper while carbon fibers were added
8% diglycidyl ether of bisphenol solu- composite. to the second hopper. Nylon 66 was
tion in acetone. Both nylon 66 and A twin-screw extruder with two fully melted before the carbon fibers
pretreated carbon fibers were dried at separate inlets was used to mold car- were added to minimize the carbon
80°C (176°F) under vacuum condition bon fiber-reinforced nylon 66 compos- fiber from fracturing during com-
for 3 h before being used to fabricate ite. Nylon 66 was added to the first pounding. Carbon fiber-reinforced ny-

Table 1 — Material Properties of Nylon 66 and Carbon Fiber

Specific Gravity Tensile Strength Elastic Modulus


(g/cm3) (lb/in.3) (MPa) (lb/in.2) (GPa) (lb/in.2)

Nylon 66 1.14 4.1 × 10–2 80 1.16 × 104 3 4.35 × 105


Carbon Fiber 1.76 6.4 × 10–2 3454 5 × 105 231 3.4 × 107

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WELDING RESEARCH

lon 66 composite with 30% mass car-


bon fiber was fabricated. The process-
ing temperature was 270~280°C
(518~536°F) and the screw speed was
180 rpm. After fully mixing nylon 66
with carbon fibers in a twin-screw ex-
truder, carbon fiber-reinforced nylon
66 composite was processed into the
pellets with a length of 2 mm (i.e.,
0.08 in.). The pellet was then fed into
the injection extruder to mold into the
coupons with the dimensions of 132
mm × 38 mm × 4.0 mm (i.e., 5.2 in. ×
1.5 in. × 0.16 in.). The mechanical
Fig. 2 — Schematic of a single lap­shear specimen. properties of the injection molded car-
bon fiber-reinforced nylon 66 compos-
ite were measured and the results are
A shown in Table 2.

Ultrasonic Welding Process


The ultrasonic welding process was
performed using a KZH-2026 multi-
function UW machine (Ref. 30) with a
nominal power of 2.6 kW and a nominal
frequency of 20 kHz. The output ampli-
tude of the transducer used in this
study was 25 m (9.8 × 10–4 in.), which
B was designed to be fixed and cannot be
adjusted during the welding process.
The gain ratios of the booster and the
horn were 1:1.2 and 1:1.5, respectively.
The amplitude of the assembled stack
was obtained by using a displacement
sensor that was integrated in the weld-
ing machine.
The welding setup used in this study
is schematically shown in Fig. 1. The
C piezoelectric converter converted the
electrical signal into mechanical vibra-
tions. To transfer the ultrasonic waves
to the workpieces, the transducer was
connected to the horn, which was
placed perpendicularly in contact with
the workpieces to be welded. The sup-
port frame of the transducer-booster-
horn system was attached to a pneu-
matic piston that provided vertical
Fig. 3A — Schematic for the mimic of 0.7 mm (0.03 in.) separation at the faying inter­ movement along with the static force
face; B — a discrepant weld; C — repairing the ultrasonic welded carbon fiber­reinforced (i.e., horn pressure) applied through the
nylon 66 composite. horn to the workpieces. The machine
was also equipped with a data acquisi-

Table 2 — Mechanical Properties of Injection­Molded 4­mm­ (i.e., 0.16­in.­) Thick Carbon Fiber­Reinforced Nylon 66 Composite Coupons
with 30% Mass Carbon Fiber

Tensile Strength Elastic Modulus


(MPa) (lb/in.2) (MPa) (lb/in.2)

99.2 ± 3 (1.4 ± 0.4) × 104 8936 ± 421 (1.3 ± 0.6) × 106

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Fig. 5 — Effects of welding time and horn pressure on the strength


of ultrasonic welded 4­mm­ (0.16­in.­) thick carbon fiber­reinforced
nylon 66 composite with 30% mass carbon fiber.
Fig. 4 — Schematic of sample preparation for examining the
microstructure of the ultrasonic welded 4­mm­ (0.16­in.­)
thick injection molded carbon fiber­reinforced nylon 66 com­
posite as fabricated.

tion system, which combined with the figuration shown


pressure sensor, horn-displacement in Fig. 2 was se-
sensor, and timer, were integrated in lected in this
the controller of the UW machine. The study. There was
horn pressure, weld energy, and dis- no energy direc-
placement of the horn were recorded tor introduced
online in a personal computer as a on the work-
function of time by the data acquisi- pieces. All speci-
tion system. The final horn displace- mens were weld-
ment, weld energy, welding time, horn ed in energy
pressure, hold time, and delay time mode using a
were also displayed in the control panel KZH-2026 multi-
during the ultrasonic welding process. function ultra-
To avoid the coupons’ motion during sonic welding Fig. 6 — Correlation between the joint strength and weld area of ul­
welding, the coupons were fixed with a machine (Ref. trasonic welded 4­mm­ (0.16­in.­) thick lapped carbon fiber­reinforced
fixture as shown in Fig. 1. 30) with a nomi- nylon 66 composite with 30% mass carbon fibers made with a welding
The machine includes three welding nal power of 2.6 time of 2.1 s and a horn pressure of 0.15 MPa (21.76 lb/in.2).
modes, energy, time, and collapse mode. kW and a fre-
The value of the weld energy for the en- quency of 20 kHz. The values of the ul- the faying surface prior to welding —
ergy mode, the welding time for the trasonic energy, horn pressure, and hold Fig. 3A. Ultrasonic welds, shown in
time mode, and the horn displacement time were preset prior to welding and Fig. 3B, were fabricated with a weld
for the horn-displacement mode are then ultrasonic welding was performed time of 2.1 s, a horn pressure of 0.15
preset prior to welding to control the using nominal power. When the weld MPa (21.76 lb/in.2) and a hold time of
welding process. The workpieces were time or weld energy approached the 3.0 s. To repair the undersized or
then welded using nominal power of the preset values, the ultrasonic wave oscil- flawed welds, a second vibration with
machine. When the weld energy, weld lation was stopped and the coupons various energy intensities were ap-
time, or horn-displacement reached the were held for 3.0 s to solidify the molten plied to the existing flawed welds us-
preset values for the selected weld material. All specimens were welded us- ing the same horn pressure [0.15 MPa
mode, the ultrasonic wave oscillation ing 7075 aluminum horn with a diame- (21.76 lb/in.2)], referring to Fig. 3C.
was stopped. Therefore, the weld quali- ter of 18 mm (0.71 in.).
ty was controlled by the preset values in Quasi­Static Test
each selected welding mode. Repairing Ultrasonic Welds
Quasi-static tests were performed by
Sample Fabrication To mimic the tolerance resulting loading each specimen to failure in an
from part distortion, a separation of MTS 810 tensile tester according to
The single lap-shear specimen con- 0.7 mm (0.03 in.) was introduced at ASTM D1002-2001. To minimize the

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Fig. 7 — Effect of separation between the workpieces on the


strength of the ultrasonic welded 4­mm­ (0.16­in.­) thick lapped
carbon fiber­reinforced nylon 66 composite with 30% mass carbon Fig. 8 — Effect of repair energy on the strength of the ultrasonic
fiber made at a welding time of 2.1 s and a horn pressure of 0.15 welded 4­mm­ (0.16­in.­) thick carbon fiber­reinforced nylon 66
MPa (21.76 lb/in.2). composite with 30% mass fiber.

A B C D

Fig. 9 — Failure modes of repaired ultrasonic welded joints: A — Schematic of a loaded joint; B — interfacial failure mode for a repaired
partially bonded weld; C — failure through the upper workpiece; D — failure through the lower workpiece for the nominal weld.

bending stresses inherent in the testing load to the overlap area of the weld [950 lon 66 composite has poor transmis-
of single-lap weld specimens, filler mm2 (1.47 in.2)]. Three replicates were sion, it is difficult to examine the weld
plates shown in Fig. 2 were attached to performed, and the average joint microstructure using polarization mi-
both ends of the specimen using mask- strengths were reported. croscopy (Ref. 31). To assess the char-
ing tape to accommodate the sample acteristics of the weld microstructure
offset. Load vs. displacement results of the ultrasonic welded joints, the
were obtained, as the specimens were Examinations of Weld specimens were prepared following the
loaded at a stroke rate of 2.0 mm/min Microstructure illustrations shown in Fig. 4. As
(0.08 in./min). The strength of the joint shown, the joints were notched from
was evaluated by the ratio of the peak Because carbon fiber-reinforced ny- the central position of the weld. Then,

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A B

C D

Fig. 10 — Appearances of the welded 4­mm­ (0.16­in.­) thick


E carbon fiber­reinforced nylon 66 composite with a separation of
0.7 mm (0.03 in.) between the workpieces before and after re­
pair with the repair energy of the following: A — 2 kJ; B — 3 kJ;
C — 4 kJ; D — 5 kJ; E — 6 kJ.

Results and the joint strength increased with in-


creasing the welding time and horn
Discussion pressure. The results indicated that in-
creasing the welding time and horn
Ultrasonic Weld­ pressure resulted in an increase in
welding energy. However, excessive
ing Carbon Fiber welding time and horn pressure did
Composite not always increase the joint strength.
When the welding time exceeded 2.1 s
To develop the and the horn pressure was above 0.15
welding process MPa (21.76 lb/in.2), the strength of
the prenotched specimens were im- window, 4-mm- the joints decreased slightly. Referring
mersed in liquid nitrogen for 10 min (0.16-in.-) thick carbon fiber-rein- to Fig. 5, although significant scatter
to embrittle the nylon 66. Finally, the forced nylon 66 composite with 30% in joint strength was observed, there
embrittled specimens were broken off mass fiber without energy director appeared an optimum welding combi-
from the notched site. To characterize were welded using various combina- nation (i.e., a weld time of 2.1 s and a
the weld microstructure, the broken tions of welding time and horn pres- horn pressure of 0.15 MPa (21.76
specimens were sputter-coated with sure. The welded joints were quasi- lb/in.2) to obtain the optimal joint
gold for 50 s and then examined with a static tested. Figure 5 shows the ef- strength.
scanning electron microscope fects of welding time and horn pres- To understand the cause of signifi-
(JSM6700F). sure on the joint strength. As shown, cant scatter in joint strength, the frac-

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A B

E
Fig. 11 — A — Schematic of weld growth; B — weld area of a
discrepant weld, effect of repair energy on the weld area of the
ultrasonic weld repaired with an energy of the following: C — 3
kJ; D — 4 kJ; E — 5 kJ; F — 6 kJ.

ture surfaces of the ultrasonic welded workpieces. This


joints were visually examined and the distortion could af-
results revealed the variation in weld fect the surface
area at the faying surface was likely contacts between
the culprit. To validate this observa- the horn/anvil-to-
tion further, the weld areas for all ul- workpiece, and F
trasonic welded joints made with a consequently pro-
welding time of 2.1 s and a horn pres- duced the separa-
sure of 0.15 MPa (21.76 lb/in.2) were tion between the
measured. Figure 6 shows the correla- workpieces. This
tion between the joint strength and could affect the
weld area. Referring to Fig. 6, the vari- heat generation
ation in weld area in the range of 180 and lead to the
to 400 mm2 (0.28 to 0.62 in.2) resulted variation in weld
in a fluctuation of the joint strength area. To validate
from 5.05 to 6 MPa (732.4 to 870.2 this speculation, expected the scatter in the weld quali-
lb/in.2). By examining the tested speci- the workpieces with the separations in ty was inevitable. Therefore, there is
mens, it was noted that the scatter in the range of 0.5 to 2.0 mm (0.02 to an urgent need to develop a method to
the weld area likely resulted from the 0.08 in.) at the faying surface, refer- inspect the weld quality and repair the
variations in the material properties ring to Fig. 3A, were welded, and the welds in ultrasonic welding of thermo-
and inconsistent surface contacts be- results of quasi-static tests are shown plastic composites.
tween the workpieces during the ultra- in Fig. 7. As shown, the separation be-
sonic welding process. tween the workpieces had a significant Repairing Ultrasonic Welded
In an attempt to check the dimen- influence on the strength of the weld-
sional quality of the workpieces, the ed joints. Examining the fractured Carbon Fiber­Reinforced Nylon
dimensions and surface quality of specimens revealed the separation be- 66 Composite
the injection molded carbon fiber- tween the workpieces reduced the
reinforced nylon 66 composite weld area, and thus resulted in lower A method for inspection of weld
coupons were examined. The results joint strength degradation. Since the quality using horn displacement and
revealed that beside the part distor- variations in the material property duration at the stable phase of melt
tion, there were some variations in and part dimension for the injection- film during the ultrasonic welding
thickness and surface roughness of the molded composites are common, it is process was developed in a previous

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Fig. 13 — A — Schematic of an undersized weld; B — cross section of


Fig. 12 — Effect of repair energy on the weld area in ultrasonic the discrepant joint and regions examined by SEM for the repaired ul­
welded 4­mm­ (0.16­in.­) thick carbon fiber­reinforced nylon trasonic welded 4­mm­ (0.16­in.­) thick carbon fiber­reinforced nylon
66 composite with 30% mass fiber. 66 composite.

A B

D
C

Fig. 14 — Effect of repair energy on the microstructures at region 1 of the repaired ultrasonic welded carbon fiber­reinforced nylon 66
composite with 0.7 mm (0.03 in.) separation between the workpieces: A — 3 kJ; B — 4 kJ; C — 5 kJ; D — 6 kJ.

study (Ref. 29). Once the discrepant were positioned to proximate the pair energy exceeded 5.0 kJ, it not
(or flawed) weld was identified, the de- weld, and an ultrasonic vibration was only increased the joint strength but
gree of the undersized welds could be applied at substantially the same loca- also reduced the scatter in joint
estimated based on the measurements tion on the existing weld using the strength. These results suggest that by
on the production line. Then, repair- same weld horn and horn pressure. applying the proper weld energy, it is
ing the discrepant or flawed welds Repaired ultrasonic welds were then feasible to repair the discrepant ultra-
could be made on or off the produc- quasi-static tested, and the results are sonic welded joints with the second ul-
tion line. shown in Fig. 8. For the purpose of trasonic pulse.
In this study, a second ultrasonic vi- comparison, the strengths of the nom- Referring to Fig. 8, the increase in
bration was applied to repair the dis- inal welds are also included in Fig. 8. joint strength with a repair energy of 5
crepant welds that had a separation of As shown, little improvement in joint kJ implied that the second ultrasonic vi-
0.7 mm (0.03 in.) between the work- strength was observed when the repair bration likely resulted in an increase in
pieces. The ultrasonic horn and anvil energy was less than 4.0 kJ. As the re- weld area by melting of the workpieces

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A B

Fig. 15 — Effect of repair energy on the porous zone at region 2 of


the repaired ultrasonic welded carbon fiber­reinforced nylon 66
composite with 0.7­mm (0.03­in.) separation between workpieces:
A — 3 kJ; B — 4 kJ; C — 5 kJ; D — 6 kJ.

at the faying surface (Refs. 32, 33). To Repair Mechanism to 5 kJ, the flash between the work-
validate this assessment, we examined pieces increased significantly. These
the failure modes of the tested speci- These results show the applied sec- results inferred that the applied sec-
mens, and the results are shown in Fig. ond vibration with the proper weld en- ond vibration melted the materials be-
9. Referring to Fig. 9, the results clearly ergy repaired the welds. In order to de- tween the workpieces.
revealed that the failure modes of the termine the correlation between the Referring to Fig. 11B, the melting
ultrasonic welds depended upon the energy required and degree of the un- materials occurred at a few spots and
weld area. While the partially bonded dersized weld, the tests were per- along the edge of the overlap at the
joints, having the weld area < 360 mm2 formed to understand the repair faying surface for a partially bonded
(0.56 in.2), failed interfacially (shown in mechanism. weld. This irregular weld clearly indi-
Fig. 9B), the fully bonded joints frac- Figures 10 and 11 present the ef- cated the workpieces were not in inti-
tured at the workpieces, referring to Fig. fect of repair energy on the weld ap- mate contact during ultrasonic weld-
9C and D. These results suggested the pearances and growth of the repaired ing. As the second vibration was ap-
weld area of the ultrasonic welded joints welds, respectively. Referring to Fig. plied to a partially bonded weld, the
affected the stress states of the joints. 10, while the weld indentation on the melting occurred at the periphery of
Referring to Figs. 8 and 9, it clearly upper workpiece deepened with an in- the undersized weld and grew with an
demonstrated the restoration in crease in repair energy, the flash be- increase in weld energy, and the weld
strength primarily resulted from an in- tween the workpieces changed little geometry changed from an irregular
crease in weld area of the welds caused when the repair energy was less than 5 shape to a more or less round shape,
by the second ultrasonic pulse. kJ. As the repair energy was increased referring to Fig. 11C–F. Figure 12

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C
Fig. 16 — Effect of repair energy on the thickness of upper porous
zone at region 2.

shows the effect of repair energy on the decrease in the D


the weld area of the repaired joints. As porous zone of the
shown, the joints repaired with an en- upper workpiece.
ergy of 5 kJ had a comparable weld The porous zone in
area to that of the fully bonded weld, the melt was
and these results explained the find- thinned out for the E
ings shown in Fig. 8 where the welds weld repaired with
repaired with an energy of 5 kJ had a energy less than 5
comparable strength to that of the ful- kJ. As the repair en-
ly bonded welds. Combining the re- ergy exceeded 5 kJ,
sults in Figs. 8, 11, and 12, it can be the melt at region 2 Fig. 17 — Effect of repair energy on the weld indentation of the
concluded the repair mechanism was was remelted and repaired ultrasonic welded carbon fiber­reinforced nylon 66
the melting of the carbon fiber com- thickened. From the composite: A — Schematic of a weld indentation; B — 3 kJ; C —
posite at the periphery of the existing above analyses, it 4 kJ; D — 5 kJ; E — 6 kJ.
discrepant weld. The increase in the can be concluded
weld area caused by merging the new that the increase in
melt with the existing discrepant weld the weld area result-
was mainly the reason for restoring ing from the second
the weld quality. ultrasonic vibration
Figure 13 shows the cross section was indeed the re-
of a partially bonded weld and an off- pair mechanism of
center undersized weld with a size of the ultrasonic
14 mm (0.55 in.) was observed. To welds.
progressively examine the change in
microstructures of the welds, two re- Effect of Repair
gions were selected. Figure 14A–D
present the microstructures at region
Energy on
1 of the joints repaired with 3, 4, 5, Cosmetic
and 6 kJ, respectively. As shown, while Quality of
the weld at region 1 grew in both di- Repaired Joints
ameter and depth, it contained signifi-
cant pores with a repair energy of 6 kJ. One concern was
Different results were observed that while the appli- Fig. 18 — Effect of repair energy on the weld indentation depth
(Fig. 15) for the microstructures at re- of the repaired ultrasonic welded discrepant carbon fiber­
cation of the second
reinforced nylon 66 composite.
gion 2. The thickness of the melt at re- ultrasonic pulse re-
gion 2 decreased and then increased paired partially
with an increase in repair energy. Ex- bonded welds, it may degrade the cos- pieces of the repaired joints were sec-
amination of the results shown in Fig. metic quality of the workpieces. To as- tioned and the weld indentations were
16 revealed the initial decrease in melt sess the effect of ultrasonic repair on measured. Figures 17 and 18 present
thickness at region 2 was caused by the cosmetic quality, the upper work- the effect of repair energy on the weld

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indentation. As shown, the weld in- (0.03 in.) between the workpieces. The sion. Carbon 60(14): 317–325.
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with the repair energy when the repair only improved the strength but also de- tahia, M., and Du, X. 2010. Mechanical be-
energy exceeded 3 kJ. These results creased the scatter in strength of the re- havior of self-assembled carbon nanotube
reinforced nylon 6, 6 fibers. Composites Sci-
suggested melting at the faying sur- paired joints.
ence and Technology 70(9): 1401–1409.
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second pulse increased the weld area, ing the ultrasonic welds was the in- Structural hierarchy developed in injection
it also affected the surface quality. crease in weld area caused by the melt- molding of nylon 6/clay/carbon black
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cause minimal degradation on the sur- tween the workpieces influenced the on composite gear metrology. Mechanism
face quality. contact of the workpieces during ultra- and Machine Theory 43(9): 1198–1209.
11. Bigg, D. M. 1985. Effect of com-
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pounding on the properties of short fiber
sulted in variations in weld area and
Summary weld strength.
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The results presented in this study 12. Watson, M. N., Rivett, R. M., and
Acknowledgments
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dicative of conditions in vehicle as- 13. Grewell, D., and Benatar, A. 2007.
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LEI LU, QIAN ZHI, YUHAO GAO, and ZHONG­XIA LIU (liuzhongxia@zzu.edu.cn) are with the Key Lab of Materials Physics, School of Physics and
Engineering, Zhengzhou University, Zhengzhou, China. PEI­CHUNG WANG is with the Manufacturing Systems Research Lab, General Motors
Research and Development Center, Warren, Mich.

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