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Abstract
The analysis of an induction hardening process is a complex process because
induction hardening is a combination of heat transfer, electromagnetic and
metallurgical phenomenon. Now a days, steel parts are induction hardened for
better mechanical properties in case of automobile and aerospace applications.
This paper deals with the optimization of process parameters in induction
hardening process for 41Cr4 steel material. The selected process parameters
are Power (Kw), Feed rate (mm/sec), Dwell time (sec), Quench flow rate
(litre/min). The responses selected are Case Hardness (HRC) and Effective
Case depth (mm). Response surface methodology was used to determine
optimum values of process parameters and that were - Case Hardness
59.83HRc and Effective Case Depth (ECD) 2.7mm. Analysis of variance is
conducted to investigate the influence of each parameter on responses. Also
microstructure analysis is done for justification of hardening.
Keywords: induction hardening, process parameters, optimization, RSM,
Analysis of Variance, microstructure analysis.
INTRODUCTION
Induction heating is a method of heating electrically conductive materials by the
application of a varying magnetic field whose lines of force enter the work-piece. In
this process, the varying magnetic field induces an electric potential (voltage),
which can then create an electric current depending on the shape and the electrical
84 S.P. Metage and J.S. Sidhu
problem in manufacturing industry. Since time and money are involved while
performing experimentation, it is pertinent to reduce the number of runs while not
compromising the desired goals.
Experimental Technique
Based on the foregoing inputs, the complete experimental run layout (Table 2) was
produced using MINITAB software. Those performance tests involved 30 runs of
the material. After induction hardening process, surface hardness was measured by
Rockwell hardness tester for C scale at 150 Kg load, having diamond indenter at
120 degree. Additionally cylindrical samples were cut from the middle of material
for investigation of case depth.
Table 2. Experimental Data for Case hardness and Effective case depth
Sr. Power Feed rate Dwell Quench Flow Case Hardness Case Depth
No. [Kw] [mm/sec] Time [sec] rate [litre/min] [HRC] [mm]
1 12.5 300 0.1 12 55 1.8
2 12.5 400 0.2 12 53 1.7
3 12.5 300 0.3 12 56 2.1
4 12.5 200 0.2 12 54 1.9
5 12.5 300 0.2 12 53 1.6
6 12.5 300 0.2 10 54 2.2
7 15 300 0.2 12 58 2.5
8 12.5 300 0.2 14 55 2.0
9 10 300 0.2 12 50 1.4
10 12.5 300 0.2 12 55 1.6
11 10 400 0.3 14 51 1.3
12 12.5 300 0.2 12 54 1.7
13 15 400 0.3 14 58 2.3
14 10 200 0.3 10 49 2.0
15 12.5 300 0.2 12 53 1.6
16 10 200 0.1 10 48 1.3
17 15 200 0.1 14 59 2.2
18 15 200 0.1 10 58 2.4
19 12.5 300 0.2 12 55 1.8
20 10 400 0.1 14 50 1.1
21 15 200 0.3 14 60 2.9
22 15 400 0.1 14 59 2.3
23 10 200 0.1 14 51 1.3
24 12.5 300 0.2 12 55 2.1
25 10 400 0.3 10 51 1.7
26 10 200 0.3 14 53 1.9
27 15 200 0.3 10 59 2.7
28 10 400 0.1 10 50 1.0
29 15 400 0.1 10 56 2.3
30 15 400 0.3 10 58 2.5
Optimization of Process Parameters in Induction Hardening of 41Cr4 Steel… 87
Source DF Seq. SS
Power 1 288
Feed rate 1 1.389
Dwell Time 1 4.5
Quench Flow 1 9.389
rate
Table 4. ANOVA results for Case Depth
Predicator Coefficient SE Coefficient T P
Constant -0.3656 0.3736 -0.98 0.337
Power [P] 0.2022 0.0173 11.69 0.000
Feed rate [F] -0.00133 0.0004326 -3.08 0.005
Dwell Time 2.0556 0.4326 4.75 0.000
Quench
[D]Flow -0.02222 0.02163 -1.03 0.314
rate [Q] S = 0.183521 R-Sq = 87.2% R-Sq (adj) = 85.1%
Analysis of Variance
Source DF SS MS F P
Regression 4 5.7167 1.4292 42.43 0.000
Residual error 25 0.8420 0.0337
Total 29 6.5587
Source DF Seq. SS
Power 1 4.6
Feed rate 1 0.32
Dwell Time 1 0.76
Quench Flow 1 0.0356
rate
Figure 1. Main effects plot for case hardness and case depth
In ECD graph, as power increases, ECD also increases showing direct relation of
power with ECD. As feed rate increases ECD decreases, hence there is inverse
relation between ECD and feed rate. ECD increases with increase in dwell time.
ECD decreases initially with increase in quench flow rate and then increases.
90 S.P. Metage and J.S. Sidhu
Fe e d rate [mm/se c]
52 - 54
54 - 56
57.5 300 56 - 58
ase Hardness [HRC] 55.0 > 58
52.5
400
50.0
300 Hold Values
Feed rate [mm/sec] 250
10 Dwell Time [sec] 0.2
12 200
14
Power [Kw] Quench Flow rate [litre/min] 12
200
10 11 12 13 14 15
Power [Kw]
Figure 2. a) Surface and Contour Plots of Case Hardness vs Feed rate, Power
As power increases, case hardness also increases, maximum case hardness falls in
the range of 14-15 Kw. Case hardness decreases with increase in feed rate,
maximum case hardness falls in the range of 200-250 (mm/sec) keeping other
parameters constant.
Surface Plot of Case Hardness [H vs Dwell Time [sec], Feed rate [mm/se Contour Plot of Case Hardness vs Dwell Time [sec], Feed rate [mm/sec]
Hold Values
Power [Kw] 12.5
Quench Flow rate [litre/min] 12 0.30 Case
Hardness
[HRC]
0.25
Dwe ll Time [se c]
< 53.7
53.7 - 54.0
56
0.20 54.0 - 54.3
Case Hardness [HRC] 55
54.3 - 54.6
54
54.6 - 54.9
0.3
0.15 > 54.9
53 0.2
Dwell Time [sec]
200
300 0.1
400
Feed rate [mm/sec]
Hold Values
0.10
200 250 300 350 400 Power [Kw] 12.5
Feed rate [mm/sec] Quench Flow rate [litre/min] 12
Figure 2. b) Surface & Contour Plots of Case Hardness and Dwell time vs Feed rate
Figure 2b shows the effect of dwell time and feed rate on case hardness. As dwell
time increases case hardness increases, feed rate increases case hardness decreases
keeping other parameters constant power 12.5 Kw, quench flow rate 12 lit/min.
In contour plot graph feed rate (mm/sec) plotted on x axis and dwell time (sec)
plotted on y axis and dark blue colour shows max case hardness. As feed rate
Optimization of Process Parameters in Induction Hardening of 41Cr4 Steel… 91
increases case hardness decreases, maximum case hardness gets in the range of 200-
250 mm/sec whereas dwell time increases case hardness increases, maximum case
hardness gets in the range of 0.25-0.30 sec keeping other parameters constant.
Surface Plot of Case Hardness [H vs Quench Flow rate, Dwell Time [sec] Contour Plot of Case Hardness vs Quench Flow rate and Dwell Time
Hold Values 14
Power [Kw] 12.5 Case
Feed rate [mm/sec] 300 Hardness
Figure 2. c) Surface & Contour Plots of Case Hardness and Quench flow rate vs
Dwell time
Figure 2c shows the effect of quench flow rate and dwell time on case hardness. As
dwell time increases case hardness increases, quench flow rate increases case
hardness increases keeping other parameters constant power 12.5 Kw, feed rate 300
mm/sec.
The contour plot represents dwell time (sec) on x axis and quench flow rate (lit/min)
on y axis and dark blue colour shows max case hardness. As dwell time increases
case hardness increases, maximum case hardness falls in the range of 0.25-0.3 sec.
Whereas, as quench flow rate increases, case hardness increases and maximum case
hardness falls in the range of 13-14 lit/min keeping other parameters constant.
Surface Plot of Effective Case D vs Feed rate [mm/se, Power [Kw] Contour Plot of Effective Case Depth vs Feed rate and Power
Hold Values
Dwell Time [sec] 0.2
400
Quench Flow rate [litre/min] 12
Effective
Case Depth
350 [mm]
Figure 3. a) Surface and Contour Plot for Case Depth vs feed rate, power
In contour plot graph, power (Kw) is plotted on x axis and feed rate (mm/sec) on y
axis and dark blue colour shows max case depth. As power increases case depth
also increases, maximum case depth gets in the range of 14-15 Kw whereas feed
rate increases case depth decreases, maximum case depth gets in the range of 200-
250 (mm/sec) keeping other parameters constant.
Figure 3b shows the effect of dwell time and feed rate on case depth. As dwell time
increases, case depth increases, also as feed rate increases case depth decreases,
keeping other parameters constant i.e. power 12.5Kw, quench flow rate 12 lit/min.
In contour plot graph, feed rate (mm/sec) is plotted on x axis and dwell time (sec)
plotted on y axis. As feed rate increases case depth decreases, maximum case depth
gets in the range of 200 mm/sec whereas dwell time increases case depth increases,
maximum case depth gets in the range of 0.30 sec keeping other parameters
constant.
Surface Plot of Effective Case D vs Dwell Time [sec], Feed rate [mm/se Contour Plot of Effective Case Depth vs Dwell Time and Feed rate
Hold Values
Effective
Power [Kw] 12.5
Quench Flow rate [litre/min] 12
0.30 Case
Depth
[mm]
0.25
Dwell Time [sec]
< 1.6
1.6 - 1.7
2.25
0.20 1.7 - 1.8
Effective Case Depth [mm] 2.00 1.8 - 1.9
1.75
0.3
1.9 - 2.0
1.50
0.15 2.0 - 2.1
0.2
Dwell Time [sec]
200
300 0.1
2.1 - 2.2
400
Feed rate [mm/sec]
> 2.2
0.10
200 250 300 350 400
Hold Values
Feed rate [mm/sec]
Power [Kw] 12.5
Quench Flow rate [litre/min] 12
Figure 3. b) Surface and contour plot for case depth vs dwell time, feed rate
Figure 3c shows the effect of quench flow rate and dwell time on case depth. As
dwell time increases case depth increases, quench flow rate increases case depth
decreases keeping other parameters constant power 12.5Kw, feed rate 300 mm/sec.
Optimization of Process Parameters in Induction Hardening of 41Cr4 Steel… 93
Contour Plot of Effective Case Depth vs Quench Flow rate and Dwell Time
14 Effective
Case
Hold Values
Power [Kw] 12.5
10 Feed rate [mm/sec] 300
0.10 0.15 0.20 0.25 0.30
Dwell Time [sec]
Figure 3. c) Surface & contour plot for case depth vs dwell time, and quench flow
rate
In contour plot graph, dwell time (sec) is plotted on x axis and quench flow rate
(lit/min) plotted on y axis and dark blue colour shows max case depth. As dwell
time increases case depth increases, maximum case depth gets in the range of 0.25-
0.3 sec whereas quench flow rate increases case depth decreases maximum case
depth gets in the range of 10-11 lit/min keeping other parameters constant.
Multiple Response Optimizations
MINITAB software was used for maximizing (achieving target values) hardness
and ECD. The optimum values of process parameters obtained were power 15 Kw,
feed rate 200 mm/sec, dwell time 0.30 sec and quench flow rate 14 lit/min, the
maximum case hardness and ECD obtained 59.83 HRC and 2.70 MM. All the
values were within 95% prediction interval.
Table 5. Multiple response optimizations
Response Goal Lower Target
Case hardness [HRC] Maximum 48 60
E Case depth [MM] Maximum 1.4 2.8
MICROSTRUCTURE ANALYSIS
The goal of heat treatment of steel is very often to attain a satisfactory hardness. The
important micro-structural phase is then normally martensite, which is the hardest
constituent in low-alloy steels. The hardness of martensite is primarily dependent on
its carbon content. If the micro-structure is not fully martensitic, its hardness is
lower. In practical heat treatment, it is important to achieve full hardness to a certain
minimum depth after cooling, that is, to obtain a fully martensitic microstructure to
a certain minimum depth, which also represents a critical cooling rate.
A finely distributed structure like tempered martensite is more rapidly transformed
to austenite than, for instance, a ferritic-pearlitic structure. This is particularly true
for alloyed steels with carbide-forming alloying elements such as chromium and
molybdenum
In case of induction hardening process uniform distribution of carbon cannot be
assumed, the time spent at the austenitizing temperature can be so brief that carbon
cannot diffuse to a uniform concentration throughout the microstructure.
Determination of 100% martensite is subjective and difficult to determine optically
(Tartaglia Eldis 1984). The figure shows microstructure image light microscope
photograph at 20X of the surface of sample piece of low hardness at 48 HRc and of
optimum hardness at 60 HRc of induction hardened 41Cr4 steel, polished and
etched at 3% Nital solution. No micro cracks observed in the induction hardened
zone.
CONCLUSIONS
From this experimentation study it has been concluded that
1. The most influencing parameters for the case hardness (CH) are the power;
quench flow rate and Dwell time, in descending order.
2. The most influencing parameters for the Effective case depth (ECD) are the
power; Dwell time and feed rate, in descending order.
3. The common optimum values of the process parameters for both responses case
hardness (CH) and Effective case depth (ECD) are: Power = 15kw; Feed rate =
200 mm/sec; Dwell time = 0.3 sec; Quench flow rate = 14 litre/min. As the error
between the experimental and predicted values is less than 5%, validates the
experiment.
4. In the hardened region, complete martensitic phase was observed which confirms
the hardening of the material
ACKNOWLEDGEMENTS
Authors express their sincere gratitude towards Mr. P. Hurdale, Pune Heat, Bhosari,
Pune for their resource courtesy.
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