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Approved 2005-11
Edition 2
NT FIRE 049
1(16)
COMBUSTIBLE PRODUCTS:
COMMODITY CLASSIFICATION – FIRE TEST PROCEDURE
3 REFERENCES 2 11 CLASSIFICATION 6
11.1 General 6
4 DEFINITIONS 3
11.2 Principle of classification 7
5 TEST PRINCIPLES 3 11.3 Evaluation of the test results –
6 CALORIMETER SYSTEM 3 classification 7
6.1 Hood and exhaust system 3 12 TEST REPORT 8
6.2 Instrumentation in the exhaust duct 4
6.2.1 Volume flow rate 4
6.2.2 Gas analysis 4 ANNEX A – PRINCIPLE DESIGN OF THE
CALORIMETER SYSTEM 9
7 STORAGE ARRAY 4
7.1 Rack storage arrangement 4 ANNEX B – PRINCIPLE DESIGN OF THE
7.2 Ignition source 5 WATER APPLICATOR 10
If a tested product shows fire characteristics similar to one [9] Chicarello, P. J. and Troup, J. M. A., “Fire Products
of the standard commodities, it is assumed that the same Collector Test Procedure for Determining the Commodity
protection requirements are adequate for the tested com- Classification of Ordinary Combustible Products”,
modities. Technical Report, FMRC J.I. OROE5.RR, August 1990
NORDTEST METHOD NT FIRE 049 3
Fire testing involves arranging a four-pallet load of the The calorimeter system consists of a large hood connected
particular commodity in a rack in a 2 by 1 by 2 storage to an exhaust system with a capacity of at least 25 m3/s at
arrangement, see Figure 1. A water applicator consisting of 20ºC. Exhaust system design based on natural convection is
a matrix of spray nozzles is arranged over the commodity. not permitted.
The water applicator provides a uniform water density on top The hood shall be at least 6 m in diameter with its lower rim
of the storage array, simulating the discharge density from about 8 m to 9,5 m above floor level. Additional information
a sprinkler. The entire set-up is positioned underneath a can be found in Annex A.
NORDTEST METHOD NT FIRE 049 4
6.2 Instrumentation in the exhaust duct burner or a methanol fire of relevant size. The heat release
rate calculated from the metered gas input or weighed mass
The following specifications are minimum requirements.
loss, respectively, and the measured heat release rate
Additional information can be found in Annex A.
based on oxygen consumption shall then be compared.
Equations for the calculations are given in ISO 9705 [4] and
6.2.1 Volume flow rate in SP Reports 1992:43 and 1994:29 [5, 6]. The calibration of
the convective part of the total heat release rate shall be
The volume flow rate in the exhaust duct shall be measured based on methanol pool fires assuming the average
with an accuracy of at least ±5%. convective heat flux fraction (of the theoretical heat release
rate) to be 0,80 as described in the report FMRC J.I
OC2E1.RA [7].
6.2.2 Gas analysis
The difference between the time average value, measured
Sampling line over a period of one minute, calculated from the measured
The gas samples shall be taken into the exhaust duct at a oxygen consumption and the heat release rate calculated
position where the combustion products are uniformly mixed from the metered gas input or weighed mass loss,
along the entire diameter of the duct. The sampling line respectively, must not exceed 10%. These measurements
tubes shall be made of a material which does not influence shall only be made when steady state conditions have been
the concentration of the gaseous species to be analysed. reached.
The calibration procedure shall also involve stepwise
Oxygen analyser changes of the heat release rate to verify that the time lag
The oxygen depletion shall be measured with an accuracy of of the gas concentration measurements is properly
at least ±0,01% by volume of oxygen. A suitable output accounted for to obtain results closely representing the
range is 0–21% by volume. The time delay from sampling to temporal concentration variations in the exhaust duct. The
analysis, including the time constant of the instrument, shall overall time lag associated with each analyser consists of
be reduced as much as possible and accurately controlled. two components; the gas transport time from the gas
sampling port to the analyser’s detection cell and the
response lag due to the analyser itself. The former lag is
Carbon monoxide and carbon dioxide analyser
linear and can be corrected by performing simple time shift.
The gas species shall be measured with an accuracy of at The latter lag depends on the analyser’s characteristics and
least ±0,1% by volume for carbon dioxide and ±0,02% by is generally non-linear. The characteristic response time of
volume for carbon monoxide. A suitable output range is most gas analysers is quite significant compared with the
0–1% for carbon monoxide and 0–6% for carbon dioxide. variation rate of fire development. The non-linear lag can be
The time delay from sampling to analysis, including the time corrected electronically in real time or corrected in post-test
constant of the instrument, shall be reduced as much as data processing using appropriate schemes, e.g. like those
possible and accurately controlled. proposed by Croce [8]. The concentration deduced from
simple time shift may deviate significantly from actual
Smoke obscuration measurement system concentrations if the analyser is not responsive enough.
(not compulsory) Simple time shift is only acceptable for steady or moderately
Smoke obscuration may be determined either by measuring varying fire development if the mean value is of primary
the light attenuation with a system consisting of a lamp, interest.
lenses, an aperture and a photocell or a laser equipment. A basic calibration also involves measurements of the flow
The system shall be constructed such that soot deposits profile in the exhaust duct, determination of temperature
during a test do not reduce the light transmission by more losses in the exhaust duct, etc. as described in references
than 5%. Such systems are described in ISO 9705 [4]. [5, 6] and [7].
6.3 Calibration
7 STORAGE ARRAY
The accuracy of the heat release measurements is of great
importance and a quality control system for the use of the 7.1 Rack storage arrangement
calorimeter system including calibration routines should
therefore be applied. A two tier, single rack storage segment is used to hold the
test commodity during the tests (see also Clause 9). The
A basic calibration shall be performed on a newly installed rack storage segment is placed centrally below the
calorimeter system or on any other occasion when this is calorimeter hood. The lower beam shall be located 300±50
considered necessary. A simplified calibration shall be made mm above the floor. The upper beam shall be adjusted such
prior to each test or continuous test series. that the vertical distance between the top of the commodity
The simplified calibration of the instrumentation in the on the first tier and the top of the beam is 200±50 mm, as
exhaust duct shall be performed by using e.g. a propane gas shown in Figure 1.
NORDTEST METHOD NT FIRE 049 5
The horizontal wind draught measured at a distance of 1 m • A general description of the burning behaviour.
from the storage array may not exceed 0,5 m/s. • Any collapses from the storage array.
All measurement channels for the calorimeter and water • Any other event of interest.
application system shall be scanned and checked for Usually, the test is continued for 25 minutes after ignition,
ambient conditions. but may be terminated earlier if the commodity is completely
The flow rate, pressure and the filling sequence of the water consumed.
applicator shall be adjusted to correspond to the selected The extent of damage to the commodity shall be
water density for the test. The discharge from the nozzles documented after the test. A judgement is made of each of
shall be visually examined to ensure that all nozzles are free the four pallet loads and the proportion consumed by the fire
of blockage. (by volume) is estimated. The total damage to the
The water applicator system shall be allowed to completely commodity is then calculated.
drain out. Ensure that all air relief devices are in an open
position.
10.3 Repeat of tests
The test commodity shall be placed in the rack storage
segment. The flue space shall be carefully adjusted to The first test shall be made according to Clause 11.2, using
150±10 mm. a nominal water discharge density of 5,0 mm/min. The
second test shall be made at a nominal water discharge
The height of the water applicator shall be adjusted so that density of 2,5 mm/min.
the clearance between the nozzles and the top of the
storage array is 250±50 mm. If the top surface of the storage Based on the calculated mean unit rank of the first two tests,
array is not completely even, the distance shall be the decision is to be made whether the water application
measured along the rim of the storage array. rate shall be increased to 7,5 mm/min or whether a free burn
test shall be conducted.
Prepare the igniters and place them as described in Clause
7.2.
Means for manual extinguishment of a fully developed fire 11 CLASSIFICATION
shall be ready available. 11.1 General
The classification test procedure is highly standardised. The
aim is to determine the hazard level of a commodity by
10.2 Test procedure
comparing the test results with data from identical tests on
The commodity shall be measured, weighed and well-defined “standard” commodities, with fire characteristics
photographed before testing. similar to commodities of Category I, II, III and IV. The tests,
All recording and measuring devices shall be started and forming the basis of this philosophy, are described in SP
data taken at least two minutes prior to ignition. Report 2003:03 [2]. Additional information is provided in SP
Report 1993:70 [3].
Ensure steady state temperature conditions in the test hall
and calorimeter system and that the flow through the hood If a tested product shows fire characteristics similar to one
system is at least 25 m3/s. of the standard commodities, it is assumed that the same
protection requirements are adequate for the tested
Ignite the storage array. commodity.
The fire is allowed to develop naturally until the convective It is important to note that the commodity classification tests
heat release rate reaches 2 MW. do not directly provide the protection requirements e.g.
The water applicator is activated to deliver the calibrated design water density for the commodity tested although
flow rate of water onto the burning commodity. If necessary, reference is made to a range of water discharge densities in
adjustments are made during the test to ensure that the the tests. The purpose is to determine the hazard level of the
specified tolerances in Clause 8.1 are complied with. commodity.
A photographic and/or video recording shall be made during A rack storage configuration is used in the classification
a test. A clock shall appear in all photographic records, tests. However, the results may also be applied to free-
giving time to nearest one second. During a test, records of standing, palletized rack and post-pallet storage con-
the following events including times when they occur shall figurations, using the design criteria given for these
be taken: configurations in EN 12845.
NORDTEST METHOD NT FIRE 049 7
V4 Convective energy, defined as the amount generated V4 The convective energy generated during the most
during the ten-minute period of most intense fire. intense ten-minute interval of the fire
These are considered to be important variables which can The total convective energy released during a fire is an
be measured with accuracy and give large enough important measure of the potential for causing thermal
differences in the measured values from one hazard level to damage to a construction. The higher the convective
the next, to provide a credible assessment of the hazard. energy, the greater the damage potential. Once again, a
The significance of each variable is discussed in detail in the product with a lower intensity but with a long fire duration
report FMRC J.I. OROE5.RR [9] and can be summarized as time, which thereby releases more energy in total, might
follows: cause more severe damage to a construction. The
convective energy reported from these classification tests is
V1 Maximum one-minute average of the total heat defined as the amount generated during the most intense
release rate ten-minute period of the fire or during the entire test if the fire
The maximum total heat release rate is an important duration time is less. The 10 minute value is based on the
measure of the potential for fire spread and is also an overall experience that most of the energy from the commodities
fundamental measure of fire severity. The total heat release used in the tests will be released during this period of time.
rate can be divided into two parts, the convective part and
the radiative part. Normally one-third of the energy is
released by radiation. Radiation is the primary mechanism 11.3 Evaluation of the test results –
for fire spread across aisles and other open spaces to classification
adjoining combustibles and is also, in part, responsible for In tables C1 through C4 of Annex C, rank values are listed
lateral fire spread throughout a large storage array. The total in one-quarter increments for the V1–V4 parameters at each
heat release rate is based on gas analysis of the of the water discharge densities and the fire burn test. For
combustion gases and the one-minute average value is information purposes, a graphical presentation of the tables
used to avoid the influence of spikes during the C1 through C4 is given in Annex D.
measurements due to environmental changes, non-
For each test, a mean unit rank shall be calculated as the
uniformity of storage packages, electrical noise, etc.
arithmetic average of the rank values obtained for each of
the parameters V1–V4.
V2 Maximum one-minute average of the convective heat
release rate The mean total rank shall be calculated as the arithmetic
average of the mean unit rank values obtained in each of the
The maximum convective heat release rate is one of the three tests. Based on the mean total rank, the commodity is
most important measures for characterizing fire severity. classified according to Table 2.
Approximately two-thirds of the energy generated from a fire
is released as convective energy. Both the gas velocity and Table 2. Classification of commodity.
temperature within a fire plume are related to the convective
heat release rate and these two parameters are very Mean total rank Classification of
important for the activation of sprinklers and the penetration commodity
of the water droplets. The higher the velocity and Less than 1,0 Category I
Equal to or greater than 1,0 but less than 2,0 Category II
temperature, the lower the portion of water that penetrates Equal to or greater than 2,0 but less than 3,0 Category III
the fire plume. The one-minute average is used for the same Equal to or greater than 3,0 but less than 4,0 Category IV
reason as mentioned above. Equal to or greater than 4,0 Special hazard
NORDTEST METHOD NT FIRE 049 8
In addition to Table 2, the following special requirements l) Dimensions and description of the storage array
apply: arrangement, support if any, etc
• If a tested commodity has a mean unit rank which m) Test results (see also Annex C)
exceeds the mean total rank by more than 1,00, the m:1 Total heat release rate histories (graphs)
commodity should be classified according to the highest
mean unit rank value. m:2 Convective heat release rate histories (graphs)
• If a single, or several, individual rank values exceed 4,50 m:3 Mass flow as a function of time in the exhaust duct
the commodity shall be considered a “special hazard”. m:4 Maximum one-minute average of the total heat
In Table C5, a commodity classification fire test analysis release rate (V1)
protocol is provided. m:5 Maximum one-minute average of the convective part
of the heat release rate (V2)
m:6 Effective convective heat release rate (V3)
12 TEST REPORT
m:7 Convective energy (V4)
The test report shall contain the following information:
m:8 Rank values, mean unit rank for each test and mean
a) Name and address of the testing laboratory total rank according to Clause 11 and the tables in
b) Date and identification number of the report Annex C
c) Name and address of the client m:9 Calibration results according to Clause 6.3
d) Purpose of the test When appropriate also:
e) Method of sampling m:10 The production rate of carbon monoxide as a function
f) Name of manufacturer or supplier of the commodity of time
g) Name or other identification marks and description of m:11 The production rate of carbon dioxide as a function of
the commodity time
h) Dimensions, numbers, weight, moisture content, etc m:12 The production rate of light obscuration smoke as a
of the main component in the commodity function of time
i) Conditioning of the commodity n) Deviations from the test method, if any
j) Date of test o) When not identified in the test method, equipment
k) Test method and instruments used.
NORDTEST METHOD NT FIRE 049 9
ANNEX A
1) A check valve for water, turned in the opposite flow direction and with a light
weight valve cone and the spring-load removed might be used.
NORDTEST METHOD NT FIRE 049 11
ANNEX C
V1 V2 V3 V4
Rank Maximum one-minute Maximum one-minute Effective convective Convective
total heat convective heat heat release rate energy
release rate release rate
(kW) (kW) (kW) (MJ)
0,25 0 – 800 0 – 550 0 – 425 0 – 175
0,50 801 – 1600 551 – 1100 426 – 850 176 – 350
0,75 1601 – 2400 1101 – 1650 851 – 1275 351 – 525
1,00 2401 – 3200 1651 – 2200 1276 – 1700 526 – 700
V1 V2 V3 V4
Rank Maximum one-minute Maximum one-minute Effective convective Convective
total heat convective heat heat release rate energy
release rate release rate
(kW) (kW) (kW) (MJ)
0,25 0 – 775 0 – 525 0 – 375 0 – 150
0,50 776 – 1550 526 – 1050 376 – 750 151 – 300
0,75 1551 – 2325 1051 – 1575 751 – 1125 301 – 450
1,00 2326 – 3100 1576 – 2100 1126 – 1500 451 – 600
V1 V2 V3 V4
Rank Maximum one-minute Maximum one-minute Effective convective Convective
total heat convective heat heat release rate energy
release rate release rate
(kW) (kW) (kW) (MJ)
0,25 0 – 750 0 – 500 0 – 325 0 – 125
0,50 751 – 1500 501 – 1000 326 – 650 126 – 250
0,75 1501 – 2250 1001 – 1500 651 – 975 251 – 375
1,00 2251 – 3000 1501 – 2000 976 – 1300 376 – 500
V1 V2 V3 V4
Rank Maximum one-minute Maximum one-minute Effective convective Convective
total heat convective heat heat release rate energy
release rate release rate
(kW) (kW) (kW) (MJ)
0,25 DNA DNA DNA DNA
0,50 DNA DNA DNA DNA
0,75 DNA DNA DNA DNA
1,00 DNA DNA DNA DNA
V2
V3
V4
2,5 mm/min V1
V2
V3
V4
5,0 mm/min V1
V2
V3
V4
7,5 mm/min V1
V2
V3
V4
Notes:
*) Three tests are conducted either without the application of water (free burn), and at 2,5 mm/min and 5,0 mm/min or, alternatively, at 2,5 mm/min, 5,0 mm/
min and 7,5 mm/min.
**) Average of the rank values for V1–V4 obtained with one specific water discharge density.
***) The average of the mean unit rank values obtained in the three tests.
NORDTEST METHOD NT FIRE 049 14
ANNEX D
V1
1 104
9000
Special hazard
8000
HRRtot (kW)
7000
IV
6000
5000 III
4000 II
3000
I
2000
0 2.5 5 7.5
Nominal discharge density (mm/min)
V2
6000
Special hazard
5000
IV
HRRconv (kW)
4000
III
3000
II
2000
I
1000
0 2.5 5 7.5
Nominal discharge density (mm/min)
NORDTEST METHOD NT FIRE 049 15
ANNEX D
V3
5000
4500
Special hazard
Effective HRRconv (kW)
4000
3500
IV
3000
III
2500
2000 II
1500
I
1000
0 2.5 5 7.5
Nominal discharge density (mm/min)
V4
3000
2500
Convective energy (MW)
Special hazard
2000
IV
1500
III
1000
II
500
I
0
0 2.5 5 7.5
Nominal discharge density (mm/min)
NORDTEST METHOD NT FIRE 049 16