 Preparation of the First 0.

01 M EDTA Solution

Mass of disodium dihydrogen EDTA used 5.604 g

Mass of MgCl2 ∙ 6H2O used 0.2511 g

 Standardization of EDTA Solution: First Preparation

Corrected mass of CaCO3 used: 0.2050 g x 99.5%= 0.2040 g
Molar mass of EDTA: 292.4 g/mol
Molar mass of CaCO3: 100.09 g/mol

Trials 1 2 3
Volume of standard CaCO3 50 50 50
solution: (ml)

Final Reading EDTA (ml) 45.7 45.4 46.3

Initial Reading EDTA (ml) 1.00 1.00 1.00
Net Volume of EDTA (ml) 44.7 44.4 45.3
Molarity of EDTA (M) 9.12 x 10-3 9.18 x 10-3 9.00 x 10-3
9.10 x 10-3
Average Molarity of EDTA
(M)

 Preparation of the Second 0.01 M EDTA Solution

Mass of disodium dihydrogen EDTA used 5.6151 g

Mass of MgCl2 ∙ 6H2O used 0.3336 g

 Standardization of EDTA Solution: Second Preparation

Corrected mass of CaCO3 used: 0.2073 g x 99.5%= 0.2063 g
Molar mass of EDTA: 292.4 g/mol
Molar mass of CaCO3: 100.09 g/mol

Trials 1 2 3
Volume of standard CaCO3 50 50 50
solution: (ml)

Final Reading EDTA (ml) 64.2 42.9 43.4

Initial Reading EDTA (ml) 3.00 1.00 1.00
Net Volume of EDTA (ml) 61.2 41.9 42.4
Molarity of EDTA (M) 6.74 x 10-3 9.83 x 10-3 9.72 x 10-3
8.76 x 10-3
Average Molarity of EDTA
(M)