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Major Experiments:
Miner Experiments:
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INSTRUCTIONS:
SALT: 1
Wet test
SALT: 2
Experiment Observation Inference
Dry tests
Observe colour of salt If Salt is coloured Cu+2, Cr+3, Mn+2,Fe+2 or
Fe+3 May be present
Cation indication from salt Salt is light pink
colour Mn+2 is present
Wet tests
Aq. Sol. of salt + BaCl2 sol. White ppts are formed Group I is present
SALT : 4
Experiment Observation Inference
Aq. Sol of salt + BaCl2 sol. No White ppts are formed Group I is absent hence
Group II is present
Aq.sol of salt + AgNO3 White ppts are formed Cl1- is present
CONFIRMATORY TESTS:
Chromyl chloride test : Heavy red vapours of
Solid salt + solid K2Cr2O7 + Chromyl chloride (CrO2Cl2) Chloride is confirmed
conc. H2SO4 +heat are evolved. On passing
these vapours through
NaOH solution a yellow
solution is formed which
gives a yellow ppt. Of lead
chromate on adding acetic
acid and lead acetate
.
Salt + MnO2 + conc. H2SO4 Greenish-yellow gas,
+ heat chlorine, evolves with
bleaches litmus. Chloride is confirmed
SALT : 5
Aq. Sol of salt + BaCl2 sol. ppts are formed Group I is present
CONFIRMATORY
TESTS:
Yellow ppts. are formed CrO4 2- radical is confirmed
Aq. Solution of salt + Dil
H2SO4 solution Red ppts. are formed CrO4 2- radical is confirmed
Aq. Solution of salt +
AgNO3 solution