Documenti di Didattica
Documenti di Professioni
Documenti di Cultura
Published by the
AMERICAN SOCIETY FOR TESTING AND MATERIALS
1916 Race Street, Philadelphia, Pa. 19103
AN EVALUATION OF THE
YIELD, TENSILE, CREEP, AND RUPTURE STRENGTHS
OF WROUGHT 304, 316, 321, AND 347 STAINLESS
STEELS AT ELEVATED TEMPERATURES
Published by the
AMERICAN SOCIETY FOR TESTING AND MATERIALS
1916 Race Street, Philadelphia, Pa. 19103
Related Publications
Note
Data Series DS 5 S2
The American Society for Testing and Materials
Contents
Surrnnary. . . . . . . . . . . . . . . . . . . . • . . . . . . . . . • . . . . • . . . . • . . . . . . . . 1
Introduction............................................ 2
Evaluation Procedures................................... 5
Char ts • . . • . • . • . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
DS6-S2-EB/Feb. 1969
Sunnnary
304, 3041, 316, 3161, 321.,and 347. The data were previously
(1965). The evaluations have been made for the Metal Properties
various properties that commonly form the basis for the setting
were employed, and the results that were achieved. On the pages
1
Copyright © 1969 by ASTM International www.astm.org
Introduction
ASME and ASTM, and now also by the Metal Properties Council.
2
3
Since the original data were included ih ASTM STP No. 124
' A distinction has been made amongst the regular grades, the
H grades, and the L grades where possible, and where it has seemed
However, for types 321 and 347, material meeting the "H" grade
involved hot or cold wo~king; in· contrast, types 304H and 316H may
or cold worked. Moreover, in both 304H and 316H, the carbon content
is permitted to range between 0.04 and 0.10 per cent, whereas the
for the regular grades of 304 and 316, the ASME Code stress tables
the specifications for types 304H and 316H are less restrictive
4
than those for the regular grades in that all material meeting the
has been attempted in the present evaluations only for types 321
The type designations 3041 and 3161 have been assigned to all
sensitization. Some of the data in ASTM STP No. 124 and its
material. [See ASTM STP 124 and ASTM DS5-Sl and also Krebs and
had received the stabilizing heat treatment has been excluded from
and the relatively few data for material in the form of castings
data for bar and plate have been distinguished from data for
pipe and tube in the plots of this report. Data identified by donors
Evaluation Procedures
0.01% per 1000 hours or 0.1% per 1000 hours, and to cause rupture
temperature.
6
that have evolved over the years in evaluating dat~ fo~ the ASME
report.
were too few data available for the remaining grades to warrant-
Grades 316-316H and 321-321H, no data for any product form exist
for temperatures between 75° and 500°F. The data for grade 347-347H
With the exception of 304 plate and 304 pipe, the data were
the average. The procedure that has been used.to develop trend
which appeared to lie outside the general scatter band, trend curves
Except for Grade 3041, the excluded data represent test temperatures
greater than 1050°F, and hence lie above the range in which allowable
tensile properties.
analyses are drawn on the ratio plots of Figs. 14 and 15; the
The trend curves developed for grade 316-316H and for 321-321H,
for which there were no data between room temperature and 500°F,
and comparison with the other trend curves suggest that a mo~e
strength ratios has the advantage that various stress levels, e.g.
75 l . 00 l . 00 l . 00 l . 00 l . 00 l. 0 0 l . 00 l . 00 l . 00
100 .96 .96 .96 .96 .97 .97 .97 .97 .98
200 .83 .84 . 84 . 83 . 85 .86 . 85 . 85 .92
300 . 75 .75 . 75 . 75 . 77 .78 . 76 . 76 .85
400 .69 . 68 .69 .69 .70 .70 . 70 . 69 . 80
500 .65 .64 .65 . 65 .65 . 66 .64 .64 .75
600 .61 .61 . 62 .61 .62 . 63 .61 .61 . 72
700 . 58 . 58 .59 .59 .60 .60 . 58 .59 .69
800 . 55 .57 .57 . 56 . 58 .59 . 55 .57 . 68
900 .53 . 55 .54 .54 .56 . 58 .53 . 57 .67
100 0 .51 .52 .52 .52 .53 .57 .50 .56 . 67
110 0 . 48 . 49 .51 .49 .50 . 55 .47 . 55 .66
1200 . 46 .51 .47 .45 .54 .42 .53 .65
1300 .42 .44 .51 .50 . 61
1400 . 38 .39 .48 .47 .54
1500 .31 .31 .43 .40 .43
1600 .20 . 20
9
Table 2
75 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 1. 00 1. 00 1. 00
100 . 96 . 97 . 97 . 97 . 97 . 97 . 97 . 95 . 97
200 .84 . 87 . 88 .86 . 86 .91 . 88 . 82 . 87
300 . 78 .81 . 83 . 80 . 79 . 89 . 83 . 77 . 80
400 . 76 . 77 . 80 . 78 . 76 . 87 . 81 .76 . 75
500 . 76 . 75 . 79 . 77 . 75 . 87 . 80 . 79 . 73
600 . 76 . 75 . 79 . 77 . 74 . 88 . 80 . 82 . 72
700 . 77 . 74 . 79 . 77 . 73 . 87 . 80 .84 .71
800 .76 . 74 . 78 • 76 . 72 . 86 . 79 . 85 .71
900 . 74 . 73 . 76 . 74 . 70 . 83 .76 . 83 .71
1000 . 70 .69 .71 .70 .66 . 78 . 72 . 79 . 70
1100 .63 .63 .64 .63 .60 .71 .66 .71 . 67
1200 . 55 . 55 . 52 . 55 . 53 . 62 . 59 .61 .62
1300 .46 .46 .45 . 52 . 50 .49 .54
1400 .36 . 35 . 36 .41 .41 . 37 .43
1500 . 26 . 25 .26 . 30 .31 . 25 . 28
10
11
the means and also the standard deviations of the data at room
up into the creep range, and beyond which there are no data for
product forms from the average are only very slightly greater.
Unfortunately, for the other grades, there were too few data available
of the ratio plots revealed no distinction between grades 347 and 347H,
effort was made to distinguish between grades 321 and 321H in view
12
13
304 and 304H and grades 316 and 316H, it has not seemed appropriate
Not only are the trend curves similar for different product
grade exhibits ratios as much as 15 per cent higher than those for
the other grades. For the tensile strength trend ratios differences
exist amongst the grades. Grade 347 now exhibits the least ratio
the highest. The L grades of 304 and 316 exhibit slightly lower
stress in Figures 16-22. The data for grades 347 and 347H are
shown in common plots, Fig. 22, treating the data as though from
that the differences in the variances and the means were not
even more meager creep data did not suggest significant differences
from pipe-tube data by the symbols used in the plots, but in the
employed by analysts, one treating all of the data for a given grade
obtain the stress for a secondary creep rate of 0.01% per 1000
Pressure Vessel Codes. (If, however, the creep strain after some
both pro and con may be advanced. (see, for example, Joint
squares analysis of the scatter band has been used in this report
temperature.
is that of whether the variables are related linearly (on the log-
important reason for not assuming a higher degree for the relationship,
by the power terms for the long time tests. This weighting can
data were not extrapolated unless data were available for three
hours. Also, with few exceptions, the creep-rate data were not
out in both ways for each grade, and the two results are included,
secondary creep rate of 0.1% per 1000 hours, and in Figs. 24 a-g,
have been chosen for these plots because this frequently tends to
Table 4
Table 5
,.
Mean of Regression Anal. Stand. Xin. r,r
v-
18
19
for the grades for which there were more than 10 sets of data have
and since the two regression lines diverge from the centroid, the
and 24, were analyzed by the method of least squares, choosing temperature
Dulis and Houston, Trans. ASM ~' 1950 p. 935), on the basis of
The linear regression lines are shown on the data plots, and
950
1000 25.0-;\" 36.0 40.0 39.0* 43.0* 43.5 40.0* 48.0 52.7
1050 20.0 28.0 31.1 30.5 34.0 34.4 31.0* 31.5 31.5 36.0 39.5
1100 15.6 22.2 24.6 23.5 26.5 26.8 23.5 23.8 24.8 27.5 30.2
1150 12.2 17.3 19.2 18.2 20.8 21.0 17.3 17.6 19.3 20.5 22.5
1200 9.7 13.8 15.32 14.2 16.2 16.4 12.. 9 13.1 15.2 15.6 17.13
1250 7.6 10.8 12.0 11.0 12. 7 12.9 9.7 9.85 11.8 11. 9 13.1
N
0
1300 6.0 8.5 9.45 8.5 9.9 10.0 7.2 7.3 9.2 9.0 9.9
1350 4.7 6.7 7.45 6.6 7.7 7. 8 5.4 5.5 7.2 6.8 7.5
1400 3.7 5.3 5.9 5.1 6.0 6.06 4.0 4.05 5.6* 5.1 5.6
1450 2.9 4.15 4.6 3.95 4.7 4.75 3.05 3.10 4.4* 3.85 4.23
1500 2.3 3.25 3.61 3.05 3.7 3.74 2.28 2.32 3.4* 2.90 3.18
1550 1. 8
1600 1.41
(1) Adjusted by displacement of the regression line by the amount required to effect coincidence
with the mean of the visual extrapolation results at 1200 F.
Table 7
( 1) ( 1)
Temp °F 3041 304- 3 04- 3161 316- 316- 321 321H 347-
304H 304H 316H 316H Adjust. 347H 347H
Adjust. Adjust. Adjust.
900
950
1000 19.5i; 25. 8 29.0 34,5i; 3 7. 0 ~'; 2 9. 0 ~'; 3 7. 5 40.0
1050 15.0 20.0 22.6 25.0 28.0 2 8. 5 23,01: 22.7 22.5 28.0 29. 8
1100 11. 6 15.8 17.8 18.5 20. 8 21. 2 16.5 16.3 17.4 20. 8 22. 2
1150 8.9 12.5 14.1 13.7 15.1 15.35 12.0 11. 9 13.3 15. 3 16.3
1200 6.9 9. 8 11.04 10.l 11. 4 11. 6 8. 7 8. 6 10.3 11. 5 12.25
1250 5.3 7. 6 8. 6 7. 4 8. 4 8. 5 5 6.3 6. 23 7.9 8. 6 9 .15
1300 4.1 6. 0 6.8 5. 5 6.3 6. 4 4.6 4. 5 5 6 .1 6. 4 6.8
1350 3.15 4.7 5.3 4.0 4.7 4. 8 3. 3 3. 26 4.7 4.7 5.0
1400 2.4 3. 7 4.17 3. 0 3.45 3.51 2.45 2.42 3 . 6 i; 3.55~?3.78
21
Table 8
Average Stress for Secondary Creep Rate of 0.1% per 1000 hours - 1000 psi
950
1000 2 5. 5 23. 5 3 5. 5 53. 0
1050 9 . 7 ;': 20. 5 18.0 28. 0 30.0;': 26.5* 38.0
1100 7. 7 16. 5 14.0 22.5 20. 0 20. 3 27. 5
1150 6.2 13.3 10.8 18.0 13.1 15.6 20. 0
1200 4. 9 5 10. 8 8. 3 14.2 8. 8 12.0 14.8
1250 4. 00 8.7 6. 4 11. 2 5.8 9. 2 10.7
1300 3.2 7.0 4. 9 8 •9 3. 85 7 .1 7 •8
1350 2. 55 5. 7 3.8 7 .1 2. 55 5. 4 5. 6
1400 2. 0 5 4. 6 2. 9 5. 6 1. 70 4. 2 4 .1
1450 1. 63 3. 7 2.28 4. 4 1.13 3.2 3. 0
1500 1. 3 0 2. 95 1. 7 5 3. 5 5 0. 7 5 2.5 2.15
22
Table 9
Average Stress for Secondary Creep Rate of 0.01% per 1000 hours - 1000 psi
900
950
1000 7 . 8 ~·: 17.9 -2 2. 5 20.l 3 0. 5
1050 6 . 3 ~·: 14.0 16.2 15.8 13. 6~': 16.6~': 22.4
1100 5.1 11. l 12.0 12.4 9. 2 12.4 16.2
1150 4.0 8.9 8.8 9. 9 5.9 9.3 12.0
1200 3. 2 5 7.2 6.4 7.9 3. 9 7.0 8.7
1250 2.6 5.7 4.7 6.1 2. 5 5 5.25 6.4
1300 2.1 4.5 3.5 4.8 l. 7 4.00 4.7
1350 l. 7 3.6 2.5 3.8 1.1 2.95 3. 4
1400 l. 34 2.9 l. 85 3. 0 0.74 2. 2 5 2.5
1450 l. 09 2.3 l. 3 5 2. 4 0.48 l. 7 0 l. 8
1500 0.88 l. 8 l. 00 l. 9 0.32 l . 28 l. 3
23
24
rate of 0.01% per 1000 hours are compared with one another in
exactly through the average of the values of 1200°F, and for those
were relatively few data for the pipe-tube product form of type
Two methods delineating a minimum have been used, one based upon
sparsity of data.
the analyst and implicitly assumes that the minimum value derives
950
1000 18.l 19.9 21. 5 18.8 32.7 3 2. 2
1050 14.l 15. 5 23 .1 22. 8 14.52 12.0 16.7 14.6 24. 3 23. 9
1100 11. l 12.2 17.15 16.9 10.43 8. 6 12.9 11. 3 18.l 17.8
1150 8.8 9.65 12.4 12.25 7. 62 6. 28 9. 8 5 8.62 13. 3 13.l
1200 6. 9 7. 5 5 9. 4 9. 28 5. 5 4.53 7. 6 3 6. 68 10.0 9. 8 5
1250 5.37 5.9 6.91 6. 82 3. 9 9 3. 2 9 5. 8 5 5.12 7.47 7. 3 5
1300 4.25 4.65 5.18 5.11 2.91 2.40 4.52 3. 96 5. 5 5 5.45
1350 3. 31 3. 63 3. 88 3.84 2.09 l . 72 3. 48 3. 05 4.08 4.02
1400 2.61 2. 86 2.84 2.80 l. 5 5 l . 28 2. 67 2.33 3. 09 3.04
1450 2.04 2.24 2.14 2.11 1.11 . 91 2. 08 l . 82 2. 29 2.26
1500 l . 62 l . 77 l . 60 l . 58 0.81 . 66 l . 57 l . 37 l . 70 l . 68
26
27
Acknowledgment
28
1
: rl 11M
['I +-':'.t
]J
''fri'H, i =t.( ~
,
j!:;! •~ i:i ~I · r· t
... i
."!
1@
l::F [~2 i[Jtlf t .. -·+-
.±
±i \Eh'. \is\ fr 1.
[~:~(.
+-·~ :-1-;~ - -~7i -E
+·
:: ..:' '" 1-
'''ci:~; :~~; ';, ·~ .. i-
[~ ~:c:1; 1 '·
,.,
'"" ''·"'": :.i!.
•..., ±111.c; ::y; ::1:~'
~[er; .. ~:;:: ;.:· :j;] r.·
8 c,'E ,L:ifl' '}i 1! ~ - ·!"
ui "ff:lc~r:l~i:r: .:
$~ .8 'le I:~:;
.£t; ifr'f ,I!
·~.: n 11
-·-r-.1_ '..>Eftii
1
~· . . . ::::Ii.: ~ ·' filk~ J.:1 '" ':'!
":",;: :~i: '~C :;: ~~ 1 '11 1m " . E~ ~F lffi 11J:l:
~I~ .·,::ol:ti IJ41i-~'!ft ~H f~;j 1[·· . . :.:-~::. ~
'I ''· : :Air h ~;i~ ,, ;Llr " l'f":· .r~ 1" I::;.,:;:;; ""ti
· .·. · , _, , i ::tcEf.:+IEi· ll :: :;; t: ·ci :.J .. ~ i::. 1;:c Ii ti ':,: ::,;: ~
t=:'~' ':.• ;:;n' 'i~1 rm c• I ~ iFJ:l'' L~
' ~i~l'is lfi.t (f .. , ]';I~![
f.r.i ~,e;t: )ijj:
j",1'1i,EliiC!: !1J IiiI
ctr
±ti: : ·. ':Je~ ::,•;,~:
Fig. 2 - Type 3041. Effect of temperature on yield strength (0.2% offset),
tensile strength, average creep strength (0.01% per 1000 hours)
and average rupture strength (100,000 hours). Yield and
tensile strengths have been adjusted to 25,000 and 70,000
psi at 75°C.
2q
Fig. 3 - Type 316-316H. Effect of temperature on yield strength
(0.2% offset), tensile strength, average creep strength (0.01%
per 1000 hours) and average rupture strength (100,000 hours).
Yield and tensile strengths have been adjusted to 30,000
and 75,000 psi at 75°c.
30
.-++-t-·;
......,
0
0
""
0
.....
,. c
.,.,
Q)
'"'
+.I
C/l
31
--111" t ,,,.,.,.. ,,,,,".,,,,,,.,,, lt::r! r+L in
l± I ... ~ If [: i~J 1ci
·t+ - Iiilif~.J H
11 f If W.' '11i
_i- ..
,, .[.\f~
n~
i'~
u: :~!~
f x,!'JJ
::"';:=
.~ [:
~~.N;~ ,,, 11
I dii
: L ~ +1~ n
ri- IC
t-"
L
--l
I:
* -, jjJ
II
!c.;i
...
I I
!~
:
.....
~ . i' • 'l#i'1:f9 ,,:1 ii [I~ l •lli 'ii'
Cl) I JitU ,::; ' 5 "' 1, :: fr,: '', 11
, <1 l=icH ·~" '' E-JC'
0"' •t, , 1= 1:;~-.::C;;.i r:;
·;, 1 · 11
' ''' :: ' , ' ·~ iF' ' ; •: ' ·..
0
0
.....
Jui' ''IT :~: ,,_,1:i:i1'! i11:fff+ ~;: ::! _• -· • 1
1" G !ii N 'I; I' : '
-. W'1 ;;_ •.. - '' ;• i~i =;\ r::: :~ ':' " ,:~;i, :, I i i: if! II Cf 11il y: L'
1
i~i 1ij~ 1-i '. _; '.
Cl)
Cl)
. p:;; iJCC I:: I ~ l'i;111 - ;j ·, ' -- 'L . ·-~;,, •' _,,: ''i' t I " '' L~ hJHi I< ;
OJ
..,... ici I 't~l 1'1ti iJ i~! h -,, "ii : ~-• · i '.,' ~' !' :; -\ i r{j'i:1:;: I ' ::
·~ !• ~-
-·1m1 .- ~ -,
-;:!-
.-~~ i:I
ic:ti-;-]t'
~ J_ -Li
"''
J .; [ II.I ..
Ii+ f i
. + :r:n:
~: "j' 1i1:di-EI'
'.•"Tf'lt.'i
Jti" 'ii+:r:
. ;~ht-; !±
32
Fig. 6 - Type 321H. Effect of temperature on yield strength (0.2% offset),
tensile strength, average creep strength (0.01% per 1000 hours)
and average rupture strength (100,000 hours). Yield and
tensile strengths have been adjusted to 30,000 and 75,000
psi at 75°C.
33
Fig. 7 - Type 347-347H. Effect of temperature on yield strength
(0.2% offset), tensile strength, average creep strength
(0.01% per 1000 hours) and average rupture strength
(100,000). Yield and tensile strengths have been adjusted
to 30,000 and 75,000 psi at 75°C.
34
.,
r· ·.;
h ~-
35
Fig. 9 - Comparison of tensile strength trend curves for wrought
austenitic stainless steel.
36
'~=ti-:~ ~~
'.:It ~-t-71~
-
ch =
I
F,=°Jc~ :lfi
m,::;; 1 "l~1--
~$'= ,~'±~ +-·
'l
H-+-H-+-f+H - ~ u
t-t-1-++++-+-+-l+ '
~~-i>.'-'N-+++++t-++-H-t-+++f-H++f--++-l-l-l-++-l-l-l-l-1--1--W-W-W
37
0
9
8
7
5
.... .. -
4
I
9
8
'- cf-'E
,_ cf-'c i
5
'
I
9
,_
z
6
'
+-=-F
~
-
- -
I
39
Fig. 12 - Variation of yield strength (0.2% offset) with temperature.
c. Type 304-304H plate
40
Fig. 12 - Variation of yield strength (0.2% offset) with temperature.
e. Type 316
41
Fig. 12 - Variatio~of yield strength (0.2% offset) with temperature.
g. Type 321-3218
42
Fig. 13 - Variation of tensile strength with temperature.
a. Type 304-304H bar
43
Fig. 13 - Variation of tensile strength with temperature.
c. Type 304-304H plate
44
Fig. 13 - Variation of tensile strength with temperature.
e. Typ·e 316
45
Fig. 13 - Variation of tensile strength with temperature.
g. Type 321-321H
46
Fig. 14 - Variation of yield strength ratio with temperature
a. Type 304-304H bar
47
Fig. 14 - Variation of yield strength ratio with temperature
c. Type 304-304H plate
48
Fig. 14 - Variation of yield strength ratio with temperature
e. Type 316
49
Fig. 14 - Variation of yield strength ratio with temperature
g. Type 321-321H
50
Fig. 15 - Variation of tensile strength ratio with temperature.
a. Type 304-304H bar
51
Fig. 15 - Variation of tensile strength ratio with temperature.
c. Type 304-304H plate
52
Fig. 15 - Variation of tensile strength ratio with temperature.
e. Type 316
53
Fig. 15 - Variation of tensile strength ratio with temperature.
g. Type 321-321H
54
.
0
0.
100
....
10
55
'lOO
·-
0
w
0.
0
~
!LO
"'"'
i:lH
"'
56
100
~
w
0.
0
0
...
0
10
~
"'
100 f
'
10 !
'
~
00
0.
0
0
:::
~
10
57
,i ... '
100
.
'"p,
0
: I•. •
L-+ I 1.
0 i ·: ;,.
::: ., ...
'#L •·-•···
I
I~
I:
...
L1-1 .~.·~-··!+ IL' ·-f H- 10
'
~ 1---.----1------ H- r·-
'
'5 '
41--.;.......-
H- l
H I I :
' : , ..
' \! --~ ,+H .1,
I
--H· ·:- '-.
·l•···I
10
-- !
r
__:_:_!..
100
I
I
i
1-,, . t t:
1000
. .,- I:_
I.::,.:
10,000
I+ r'- ·-
100, 000
TIME FOR RUPTURE - HOURS
10 100
.
'"p,
~
10
t;
§
10
59
.
...
0.
0
0
:::
~ 1 ~
~
's
Fig. 17 - Log-log plots -of stress vs time for rupture and stress vs
secondary creep rate. Type 304L
60
.
·•
0.
0
~
"'
10
100~
.
.! 10~
0
~
61
100
10.
.
·•
0.
0
0
0
~
"'
~ 10
62
CREEP RATE PER CENT PER 100, 000 HOURS
.
'"0.
0
100
0
....0
10
63
10
1.0 10 1000
CREEP RATE PER CENT PER 100 ~ 000 HOURS
64
TIME FOR RUPTURE - HOURS
.
...
0.
0
0
;']
~
10
~ 10
66
.
·-<
0
0.
100
~
~ 10
67
100
.
...
0" 10
0
:::
~
~
68
TIME FOR RUPTIJRE - HOURS
100
10
70
·-.
0
0.
0
....0
"'
~ 10
~
71
100
10
·-."'
0
0
;::
"'"'
~
100
10
100
10 100
·-."'
0
"'
~ 10
72
0
0
.
-:;:
;:
~ 10
100
0
0
.
·~ 10
;:
10
73
Creep Rate - Per Cent per 100, 000 Hours
10
75
Fig. 23 - Variation of rupture strength (10,000 hours) and creep
strength (0.1% per 1000 hours) with temperature.
c. Type 316-316H
76
Fig. 23 - Variation of rupture strength (10,000 hours) and creep
strength (0.1% per 1000 hours) with temperature.
e. Type 321
77
Fig. 23 - Variation of rupture strength (10,000 hours) and creep
strength (0.1% per 1000 hours) with temperature.
g. Type 347-347H
78
Fig. 24 - Variation of rupture strength (100,000 hours) and creep
strength (0.01% per 1000 hours) with temperature.
a. Type 304-304H
79
Fig. 24 - Variation of rupture strength (100,000 hours) and creep
strength (0.01% per 1000 hours) with temperature.
c. Type 316-316H
80
•
81
Fig. 24 - Variation of rupture strength (100,000 hours) and creep
strength (0.01% per 1000 hours) with temperature.
g. Type 347-347H
82