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Introduction ........................................................................................................................................ 4
Terminology ........................................................................................................................................ 5
Application .......................................................................................................................................... 5
Theoretical framework ........................................................................................................................ 6
What is hardness? ........................................................................................................................... 6
What is the definition of hardness testing? .................................................................................... 6
Definition of hardness testing loads ............................................................................................... 6
How do hardness tests work? ......................................................................................................... 7
How to select the test method ....................................................................................................... 7
Factors that influence hardness testing .......................................................................................... 8
Surface preparation requirements for hardness testing ................................................................ 9
Deformations ................................................................................................................................ 10
Indent spacing ............................................................................................................................... 11
The Rockwell hardness test........................................................................................................... 11
The Rockwell test calculation .................................................................................................... 12
Indenters ................................................................................................................................... 12
Surface preparation................................................................................................................... 12
Overview of typical applications for Rockwell scales ................................................................ 13
Vickers hardness testing................................................................................................................ 14
The Vickers hardness calculation .............................................................................................. 14
Surface preparation................................................................................................................... 15
Brinell hardness testing ................................................................................................................. 15
The Brinell hardness calculation ............................................................................................... 16
Surface preparation................................................................................................................... 16
Knoop hardness testing................................................................................................................. 16
The Knoop test calculation ........................................................................................................ 17
Surface preparation................................................................................................................... 17
Indent spacing ........................................................................................................................... 17
Standards .......................................................................................................................................... 18
Procedure .......................................................................................................................................... 18
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Example ............................................................................................................................................. 19
Acceptance or rejection criteria ........................................................................................................ 20
Requirements, recommendations and safety conditions. ................................................................ 20
Materials, tools and equipment for Vickers test............................................................................... 21
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Introduction
The hardness is a mechanical property of the materials consisting of the difficulty
that exists to scratch or create marks on the surface by micro penetration of a tip.
There are 4 different types of hardness tests, which are: Rockwell, Vickers, Brinell
and Knoop. However, we are going to focus on the Vickers hardness test.
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Terminology
Indentation: a hole or mark on the surface of something
The elastic zone: It is when the material cannot return to the first form.
Application
The applications for Vickers hardness test are the follow:
Finished parts such as Bearings, valves, nuts, bolts, gears, pulleys, rollers,
pins, pivots, stops, etc.
Cutting tools, such as saws, blades, chisels, scissors.
Formation tools.
Smelters and small slabs.
Metal sheets.
Large diameter wire.
Electrical contacts
Plastic sheets or parts.
Cemented parts.
Cemented carbides
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Thin sections, such as pipes.
Weak structures
Thickness of the veneer.
Theoretical framework
What is hardness?
Hardness is Resistance of a material to deformation, indentation, or penetration by
means such as abrasion, drilling, impact, scratching, and/or wear, measured by
hardness tests such as Brinell, Knoop, Rockwell, or Vickers. Since there is no
standard hardness scale, each test expresses its results in its unique (and
arbitrarily defined) measure. Hardness of pliable materials such as plastics and
rubbers is measured by instruments such as durometer.
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pond (p). The correlation between kgf, kp, and N is: 1.0 kgf = 1,000 gf = 1.0 kp =
9.81 N.
The term micro hardness testing is usually used when indentation loads
are below or equal to 1 kgf
The term macro hardness testing is used when loads are higher than 1 kgf
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2. Whether compliance with a standard is required
3. The approximate hardness of the material
4. The homogeneity/heterogeneity of the material
5. The size of the part
6. Whether mounting is necessary
7. The number of samples to be tested
8. The required accuracy of the result
8
Surface preparation requirements for hardness testing
9
Due to the lower loads used during hardness testing, micro hardness testing
requires a polished or electropolished surface. It is important that the
borders/corners of an optically evaluated impression are clearly visible. This can
be performed mechanically, chemically, or electrochemically. It is important that
heating or cold working does not change the surface properties of the specimen.
Deformations
For small loads (less than 300 gf1) the surface needs to be completely free of
deformations, and the specimens require oxide or electrolytic polishing to obtain
a completely damage-free surface. You should also take into account that soft
and/or ductile materials (i.e. for HV less than 120-150) are more sensitive when
it comes to introducing preparation artefacts.
In the table below, you can see the surface preparation requirements for the
different hardness tests.
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Indent spacing
During hardness testing, the indentation will deform the surrounding material and
alter its properties. In order to avoid misinterpretations of the perceived
hardness, the standards prescribe a certain distance between multiple
indentations.
Examples of indent spacing in the Vickers hardness test for metallic materials
For steel, copper, and copper alloys: Spacing between indents must be at
least three diagonal widths.
For lead, zinc, aluminum, and tin: Spacing between indents must be at
least six diagonal widths.
The Rockwell hardness test is a fast method, making it ideal for quick hardness
testing. We give a definition of the Rockwell hardness test, as well as practical
information of how to apply it in practice.
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The Rockwell test calculation
The Rockwell hardness test calculation (HR) is made by measuring the depth of
an indentation made with a diamond or tungsten carbide ball.
Indenters
Diamond cone
Tungsten ball in sizes 1/16", 1/8", 1/4", or 1/2"
Sample thickness ASTM: At least 10 times the indentation depth for both
indenters
Sample thickness ISO: Diamond indenter: At least 10 times the
indentation depth. Tungsten carbide indenter: At least 15 times the
indentation depth
Surface preparation
Before application of the Rockwell hardness test, you must prepare the surface of
the material to be tested. The required surface condition for the Rockwell hardness
test depends on the load used.
The Rockwell hardness test is used for macro hardness tests, which are generally
defined as tests that use indentation loads below or equal to 1 kgf. Therefore, a
ground surface is usually sufficient, and sometimes no preparation is required.
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Overview of typical applications for Rockwell scales
13
Vickers hardness testing
The Vickers hardness test is a versatile hardness test method, used for both
macro and micro hardness testing. It has a broad load range, and is suitable for
a wide range of applications and materials.
The Vickers hardness test is often regarded as easier to use than other
hardness tests: The process can be performed on a universal or micro hardness
tester; the required calculations are independent of the size of the indenter; and
the same indenter (a pyramidal diamond) can be used for all materials,
irrespective of hardness.
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Surface preparation
Before placing the sample material in the micro hardness testing machine, you
should ensure it is correctly prepared.
The required surface condition for the Vickers hardness test depends on the load
used.
15
The Brinell hardness calculation
The Vickers Hardness (HV) is calculated based on the area of the indentation
performed and the load applied, using the next formula:
𝑃
𝐻𝐵 = 𝜋
2 2
2 𝐷(𝐷 − √𝐷 − 𝑑 )
Surface preparation
Before the sample material is placed in the Brinell hardness test unit, it must be
either:
Machined
Ground
Lapped
Polished
The Knoop hardness test is an alternative to the Vickers test in the micro
hardness testing range. This page describes the Knoop hardness test and gives
you practical information on how to apply it in practice.
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The Knoop test calculation
It is calculated in the same way as the vickers, the applied load divided on the
lateral surface of the indentation, the only thing that changes is the constant.
𝑃
𝐻𝐾 = 0.0124229
𝑑2
Surface preparation
Before application of the Knoop hardness test, you must prepare the surface of the
material to be tested.
The Knoop hardness test is used for micro hardness testing (loads below or equal
to 1 kgf) and so the surface of the sample material should be highly polished or
electropolished before it is introduced to the micro hardness tester.
Indent spacing
Regardless of the micro hardness tester you use, when you perform a
Vickers hardness test, your indentation will deform the surrounding material and
alter its properties. In order to avoid misinterpretations of perceived hardness,
the Vickers hardness testing standards prescribe a certain distance between
multiple indentations.
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Standards
Rockwell – ASTM E18-18Standard Test Methods for Rockwell Hardness of
Metallic Materials
Brinell - ASTM E10 - 10 Standard Test Method for Brinell Hardness of
Metallic Materials
Vickers - ASTM E384 - 11e1 Standard Test Method for Knoop and Vickers
Hardness of Materials
Knoop - ASTM E384 - 11e1 Standard Test Method for Knoop and Vickers
Hardness of Materials
Procedure
According ASTM E384 the procedure is the next:
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9. After the force is removed, switch to the measuring mode, and select the
proper objective lens. Focus the image, adjust the light intensity if
necessary, and adjust the apertures for maximum resolution and contrast.
10. Examine the indentation for its position relative to the desired location and for
its symmetry.
11. Measure the long diagonal of a Knoop indentation, or both diagonals of a
Vickers indentation, in accordance with the manufacturer’s instruction
manual.
12. Compute the Knoop or Vickers hardness number using the appropriate
equation in Section 3 or using tables supplied with the tester, respectively.
Modern testers usually give an automatic readout of the hardness after the
diagonal or diagonals have been measured.
13. Spacing of Indentations—Generally, more than one indentation is made on a
test specimen. It is necessary to ensure that the spacing between
indentations is large enough so that adjacent tests do not interfere with each
other
Example
A Vickers hardness test is applied to a piece of metal that is subjected to a load of
800 kgf during 15s, a diagonal length of the indentation diagonal length of the
indentation of 1.95 mm. Calculate its HV (Hardness Vickers).
𝑭
𝑯𝑽 = 𝟏. 𝟖𝟒𝟓𝟑
𝒅𝟐
𝟖𝟎𝟎𝒌𝒈𝒇
𝑯𝑽 = 𝟏. 𝟖𝟒𝟓𝟑
𝟏. 𝟗𝟓𝟐 388 HV 800/15
𝒌𝒈𝒇
𝑯𝑽 = 𝟑𝟖𝟖
𝒎𝒎𝟐
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Acceptance or rejection criteria
The purpose of this hardness test is not to know if the sample is accepted or
rejected, in this essay what we are looking for is to know if the piece has the
adequate characteristics for its purpose of use.
However, the test should be done following the steps correctly and the
corresponding cleaning instructions.
In relation to the risks present for the members of the body, it is taken into account
to protect the most sensitive and vital areas such as the eyes and the hands,
because with such members the process can be manipulated clearly and precisely.
The cleaning habit should always be in each test, whatever the area of work, in this
way; there will be no complications or interruptions in the entire testing process.
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Correctly place the specimen in the base of the durometer.
testing machine
specimen
vinckers indenter
safety glasses
gloves
notebook
pen or pencil
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