ANEXO

CUADRO Nro. 1

Test conditions Summary

Test 1 Resin loading
Resin Dowex-Minix Au
Feed solution Comarsa
Resin volume l 1.04 Ag
Diameter cm 2.6
Height m 1.96 Mass transfer zone height
Flowrate ml/min 316 80% breakthrough
Linear velocit cm/s 1.0 Au
Temperature deg C 13.3 Ag

Date Time Runtime Flowrate Solution

(h) (ml/min) Feed 0.04m 0.29m 0.54m
2-Sep 15:30 0.00 320
16:00 0.50 325 10.84 10.85 10.87 10.82
16:30 1.00 320
18:00 2.50 320 10.75 10.55 10.41
3-Sep 6:00 14.50 320
12:00 20.50 320
18:00 26.50 320 11.02 11.07 11.00 11.06
4-Sep 6:00 38.50 300
6:50 39.33 315
8:00 40.50 315
11:35 44.08 300
12:00 44.50 330
16:00 48.50 330
16:15 48.75 325
18:00 50.50 325 10.68 11.05 10.96 10.75
5-Sep 6:00 62.50
6:30 63.00 305
6:45 63.25 305
7:10 63.67 360
7:15 63.75 350
9:35 66.08 330
11:45 68.25 335 10.21 10.59 10.18 10.54
14:00 70.50 327
15:35 72.08 325
17:30 74.00 320
6-Sep 6:00 86.50 330
8:45 89.25 290
9:00 89.50 290
9:20 89.83 295
10:05 90.58 305
10:30 91.00 305
 10:45 91.25 310
11:35 92.08 315 10.82 10.63 10.74 10.61
14:40 95.17 317
16:20 96.83 325
7-Sep 6:20 110.83 260
6:30 111.00 265
8:20 112.83 265
9:30 114.00 270
9:45 114.25 280
10:10 114.67 290
10:40 115.17 285
10:50 115.33 375
11:00 115.50 360
11:15 115.75 350
12:00 116.50 340 10.89 10.99 11.04 10.93
13:20 117.83 345
14:05 118.58 340
14:40 119.17 330
15:55 120.42 322
18:15 122.75 317
8-Sep 6:15 134.75 310
9:00 137.50 315
9:50 138.33 320
11:30 138.67 315
11:45 138.92 320
14:35 141.75 310
14:55 142.08 312
15:05 142.25 317
15:30 142.67 312
18:00 145.17 300
9-Sep 6:20 157.50 180
6:30 157.67 185
8:00 159.17 195
8:30 159.67 182
 mg/l 7094
kg/t 22
mg/l 1543
kg/t 5

m 0.67
m 1.35

Solution pH Temperature
0.79m 1.04m 1.29m 1.54m 1.79m 1.96m deg C

10.74 10.27

10.77

18
11.06 11.02 10.96 10.91 11.05 11.08

12.5

10.96 10.69 10.87 10.86 10.81 11.00 13.5

11

10.62 10.60 10.68 10.50 10.66 10.73

16.5

11
10.74 10.60 10.74 10.78 10.76 10.61
16.5

10.8

11.03 11.00 10.94 11.06 10.99 11.08

11

15.5

10
ANEXO
CUADRO Nro. 2

Analysis during test - Au

Date Time Runtime Au in solution (mg/l)
h Feed 0.04m 0.29m 0.54m 0.79m
2-Sep 15:30 0
16:00 0.5 0.873 0.305 0.000 0.000 0.000
18:00 2.5 0.873 0.487 0.041 0.020 0.000
3-Sep 6:00 14.5 0.879 0.710 0.131 0.018 0.018
12:00 20.5 0.873 0.713 0.139 0.039 0.019
18:00 26.5 0.872 0.752 0.198 0.019 0.000
4-Sep 6:00 38.5 0.870 0.767 0.320 0.058 0.000
12:00 44.5 0.940 0.854 0.380 0.090 0.018
18:00 50.5 0.940 0.864 0.426 0.130 0.019
5-Sep 6:00 62.5 0.964 0.883 0.505 0.180 0.018
12:00 68.5 0.964 0.911 0.536 0.180 0.018
18:00 74.5 0.968 0.915 0.556 0.233 0.072
6-Sep 6:00 86.5 0.961 0.908 0.611 0.314 0.122
12:00 92.5 0.967 0.943 0.716 0.367 0.140
18:00 98.5 0.963 0.940 0.734 0.405 0.165
7-Sep 6:00 110.5 0.961 0.908 0.699 0.419 0.192
12:00 116.5 0.961 0.926 0.489 0.489 0.227
18:00 122.5 0.960 0.929 0.761 0.513 0.265
8-Sep 6:00 134.5 0.987 0.951 0.787 0.555 0.327
12:00 140.5 0.988 0.963 0.800 0.555 0.327
18:00 146.5 0.990 0.966 0.797 0.559 0.383
9-Sep 6:00 158.50 0.990 0.947 0.751 0.473 0.261
8:30 161.00 0.990 0.941 0.752 0.472 0.269
Au in solution (mg/l)
1.04m 1.29m 1.54m 1.79m 1.96m

0.000 0.000 0.000 0.000 0.000

0.000 0.000 0.000 0.000 0.000
0.018 0.000 0.000 0.000 0.000
0.019 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000 0.000
0.036 0.027 0.018 0.000 0.000
0.035 0.017 0.000 0.000 0.000
0.044 0.035 0.017 0.000 0.000
0.055 0.037 0.018 0.000 0.000
0.052 0.017 0.009 0.000 0.000
0.070 0.035 0.009 0.000 0.000
0.097 0.035 0.018 0.008 0.000
0.139 0.066 0.016 0.000 0.000
0.148 0.066 0.016 0.000 0.000
0.153 0.051 0.025 0.017 0.000
0.114 0.049 0.016 0.000 0.000
0.118 0.067 0.340 0.017 0.000
ANEXO
CUADRO Nro. 3

Test conditions Summary

Test 2 Resin loading
Resin Dowex-Minix Au
Feed solution Comarsa
Resin volume l 1.04 Ag
Diameter cm 2.6
Height m 1.96 Mass transfer zone height
Flowrate ml/min 607 80% breakthrough
Linear velocity cm/s 1.9 Au
Temperature deg C 13.4 Ag

Date Time Runtime Flowrate Solution

h ml/min Feed 0.04m 0.29m 0.54m
3-Sep 9:20 0.00 630
10:25 1.08 640
12:00 2.67
14:00 4.67 615
14:15 4.92 615
14:20 5.00 630
15:40 5.33 600
17:20 7.00 600
18:00 8.67 11.02 11.05 11.05 11.09
4-Sep 6:00 20.67 630
8:00 22.67 615
8:05 22.75 610
8:45 23.42 600
11:50 26.50 605
13:00 27.67 600
16:00 30.67 600
17:20 32.00 595
18:00 32.67 10.68 10.91 11.04 11.08
5-Sep 6:40 45.33 600
9:40 48.33 610
11:30 50.17 610
12:00 50.67 10.21 10.71 10.8 10.66
14:00 52.67 610
15:35 54.25 610
17:30 56.17 600
6-Sep 6:30 69.17 580
8:45 71.42 580
9:00 71.67 590
9:20 72.00 600
10:10 72.83 610
11:35 74.25 610
12:00 74.83 10.82 10.8 10.79 10.85
14:45 77.58 605
16:20 79.17 620
18:00 80.83 600
7-Sep 6:20 93.17 545
8:00 94.83 535
9:20 96.17 520
9:30 96.33 525
9:45 96.58 545
10:10 97.00 550
10:40 97.50 570
10:55 97.75 560
11:00 97.83 575
11:15 98.08 585
12:00 98.83 605 10.89 11.02 10.46 10.93
13:20 100.17 605
15:55 102.75 590
18:00 104.83 580
8-Sep 6:25 117.25 545
9:00 119.83 540
9:10 120.00 530
9:20 120.17 520
9:35 120.42 460
9:40 120.50 500
10:00 120.83 560
11:30 122.33 520
11:50 122.67 540
14:35 125.42 510
18:00 126.83 465
9-Sep 6:20 139.17 380
8:00 140.83 350
11:30 144.33 350
 mg/l 6244
kg/t 20
mg/l 1378
kg/t 4

m 1.23
m 1.63

Solution pH Temperature
0.79m 1.04m 1.29m 1.54m 1.79m 1.96m deg C

18
14

11.01 10.97 11.06 11.04 11.06 10.99

12.5

11.1 11.09 11.05 11.08 11.14 11.1 13.5

11

10.61 10.33 10.62 10.7 10.72 10.5

16.5

11

10.74 10.73 10.78 10.78 10.77 10.75

16.5
 10.8

10.89 10.85 10.87 10.91 10.9 11.04

11

15.5

10
ANEXO
CUADRO Nro. 4

Analysis during test - Au

Date Runtime Au in solution (mg/l)
Feed 0.04m 0.29m 0.54m 0.79m 1.04m
3-Sep 0.6 0.873 0.563 0.009 0.000 0.000 0.000
2.6 0.873 0.673 0.059 0.019 0.000 0.000
8.6 0.872 0.733 0.218 0.059 0.000 0.000
4-Sep 20.6 0.870 0.816 0.466 0.175 0.078 0.049
26.6 0.940 0.873 0.507 0.235 0.063 0.000
32.6 0.940 0.882 0.597 0.290 0.090 0.000
5-Sep 44.6 0.964 0.919 0.667 0.414 0.198 0.054
50.6 0.964 0.929 0.679 0.446 0.232 0.071
56.6 0.968 0.915 0.700 0.466 0.251 0.105
6-Sep 68.6 0.961 0.908 0.751 0.559 0.349 0.192
74.6 0.967 0.943 0.769 0.576 0.367 0.175
80.6 0.963 0.944 0.789 0.624 0.422 0.239
7-Sep 92.6 0.961 0.908 0.769 0.611 0.454 0.279
98.6 0.961 0.926 0.821 0.664 0.507 0.314
104.6 0.961 0.929 0.832 0.690 0.513 0.354
8-Sep 116.6 0.987 0.951 0.820 0.689 0.557 0.393
122.6 0.988 0.963 0.849 0.718 0.571 0.424
128.6 0.990 0.975 0.849 0.716 0.559 0.390
on (mg/l)
1.29m 1.54m 1.79m 1.96m
0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000
0.029 0.019 0.019 0.019
0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000
0.000 0.000 0.000 0.000
0.018 0.000 0.000 0.000
0.054 0.018 0.000 0.000
0.087 0.017 0.000 0.000
0.087 0.017 0.000 0.000
0.110 0.046 0.018 0.000
0.157 0.070 0.017 0.000
0.175 0.087 0.035 0.000
0.230 0.106 0.044 0.018
0.246 0.148 0.082 0.049
0.278 0.163 0.098 0.057
0.254 0.169 0.120 0.068