−−−− PROCESSING PARAMETERS −−−−

dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
trapezoid3 : 0[%] : 80[%] : 100[%]
zerofill : 1
fft : 1 : TRUE : TRUE
3.0

machinephase
ppm
Derived from: RIKY−single_pulse_dec−3.jd

Filename = RIKY−single_pulse_dec
Author = delta
Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
Creation_time = 2−JAN−2017 09:45:55
Revision_time = 6−JAN−2017 12:02:53
2.0

Current_time = 6−JAN−2017 12:03:26

Content = single pulse decouple
Data_format = 1D COMPLEX
Dim_size = 26214
Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
Site = ECA 500
Spectrometer = DELTA2_NMR
Field_strength = 11.7473579[T] (500[MH
X_acq_duration = 0.83361792[s]
X_domain = 13C
X_freq = 125.76529768[MHz]
X_offset = 100[ppm]
1.0

X_points = 32768
X_prescans = 4
X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
Clipped = FALSE
Mod_return = 1
Scans = 87650
(thousandths)

Total_scans = 87650
X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
220.0 210.0 200.0 190.0 180.0 170.0 160.0 150.0 140.0 130.0 120.0 110.0 100.0 90.0 80.0 70.0 60.0 50.0 40.0 30.0 20.0 10.0 0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60

5.8090
2.4515
2.3943
90.1469
84.3858
82.3732

56.2095
48.0066
47.8349
47.6632
47.4915
47.3198

31.4576

23.0543

11.0074
201.0681
199.8281
197.1097

179.7785
177.1937
176.2589

149.5421

143.1991
137.3139
135.4635
130.3796

123.2163
123.1304
118.5711

Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C

 −−−− PROCESSING PARAMETERS −−−−
dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
trapezoid3 : 0[%] : 80[%] : 100[%]
zerofill : 1
fft : 1 : TRUE : TRUE
3.0

machinephase
ppm
Derived from: RIKY−single_pulse_dec−3.jd

Filename = RIKY−single_pulse_dec
Author = delta
Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
Creation_time = 2−JAN−2017 09:45:55
Revision_time = 6−JAN−2017 12:02:53
2.0

Current_time = 6−JAN−2017 12:03:33

Content = single pulse decouple
Data_format = 1D COMPLEX
Dim_size = 26214
Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
Site = ECA 500
Spectrometer = DELTA2_NMR
Field_strength = 11.7473579[T] (500[MH
X_acq_duration = 0.83361792[s]
X_domain = 13C
X_freq = 125.76529768[MHz]
X_offset = 100[ppm]
1.0

X_points = 32768
X_prescans = 4
X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
Clipped = FALSE
Mod_return = 1
Scans = 87650
(thousandths)

Total_scans = 87650
X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
210.0 200.0 190.0 180.0 170.0 160.0 150.0 140.0 130.0 120.0 110.0 100.0 90.0 80.0 70.0 60.0 50.0 40.0 30.0 20.0 10.0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60
90.1469
84.3858
82.3732

56.2095
48.0066
47.8349
47.6632
47.4915
47.3198

31.4576

23.0543

11.0074
201.0681
199.8281
197.1097

179.7785
177.1937
176.2589

149.5421

143.1991
137.3139
135.4635
130.3796

123.2163
123.1304
118.5711

Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C

 2.5
2.4
2.3
2.2

−−−− PROCESSING PARAMETERS −−−−

dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
2.1

trapezoid3 : 0[%] : 80[%] : 100[%]

zerofill : 1
2.0

fft : 1 : TRUE : TRUE

machinephase
ppm
1.9

Derived from: RIKY−single_pulse_dec−3.jd

1.8
1.7
1.6

Filename = RIKY−single_pulse_dec
Author = delta
1.5

Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
1.4

Creation_time = 2−JAN−2017 09:45:55

Revision_time = 6−JAN−2017 12:02:53
1.3

Current_time = 6−JAN−2017 12:03:41

Content = single pulse decouple
1.2

Data_format = 1D COMPLEX
Dim_size = 26214
1.1

Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
1.0

Site = ECA 500

Spectrometer = DELTA2_NMR
0.9

Field_strength = 11.7473579[T] (500[MH

X_acq_duration = 0.83361792[s]
0.8

X_domain = 13C
X_freq = 125.76529768[MHz]
0.7

X_offset = 100[ppm]
X_points = 32768
X_prescans = 4
0.6

X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
0.5

Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
0.4

Clipped = FALSE
Mod_return = 1
0.3

Scans = 87650
(thousandths)

Total_scans = 87650
0.2

X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
0.1

X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
210.0 200.0 190.0 180.0 170.0 160.0 150.0 140.0 130.0 120.0 110.0 100.0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60
201.0681
199.8281
197.1097

179.7785
177.1937
176.2589

149.5421

143.1991

137.3139
135.4635

130.3796

123.2163
123.1304

118.5711

Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C

 2.5
2.4
2.3
2.2

−−−− PROCESSING PARAMETERS −−−−

dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
2.1

trapezoid3 : 0[%] : 80[%] : 100[%]

zerofill : 1
2.0

fft : 1 : TRUE : TRUE

machinephase
ppm
1.9

Derived from: RIKY−single_pulse_dec−3.jd

1.8
1.7
1.6

Filename = RIKY−single_pulse_dec
Author = delta
1.5

Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
1.4

Creation_time = 2−JAN−2017 09:45:55

Revision_time = 6−JAN−2017 12:02:53
1.3

Current_time = 6−JAN−2017 12:03:47

Content = single pulse decouple
1.2

Data_format = 1D COMPLEX
Dim_size = 26214
1.1

Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
1.0

Site = ECA 500

Spectrometer = DELTA2_NMR
0.9

Field_strength = 11.7473579[T] (500[MH

X_acq_duration = 0.83361792[s]
0.8

X_domain = 13C
X_freq = 125.76529768[MHz]
0.7

X_offset = 100[ppm]
X_points = 32768
X_prescans = 4
0.6

X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
0.5

Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
0.4

Clipped = FALSE
Mod_return = 1
0.3

Scans = 87650
(thousandths)

Total_scans = 87650
0.2

X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
0.1

X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
110.0 100.0 90.0 80.0 70.0 60.0 50.0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60
90.1469

84.3858

82.3732

56.2095
Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C

 2.5
2.4
2.3
2.2

−−−− PROCESSING PARAMETERS −−−−

dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
2.1

trapezoid3 : 0[%] : 80[%] : 100[%]

zerofill : 1
2.0

fft : 1 : TRUE : TRUE

machinephase
ppm
1.9

Derived from: RIKY−single_pulse_dec−3.jd

1.8
1.7
1.6

Filename = RIKY−single_pulse_dec
Author = delta
1.5

Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
1.4

Creation_time = 2−JAN−2017 09:45:55

Revision_time = 6−JAN−2017 12:02:53
1.3

Current_time = 6−JAN−2017 12:03:58

Content = single pulse decouple
1.2

Data_format = 1D COMPLEX
Dim_size = 26214
1.1

Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
1.0

Site = ECA 500

Spectrometer = DELTA2_NMR
0.9

Field_strength = 11.7473579[T] (500[MH

X_acq_duration = 0.83361792[s]
0.8

X_domain = 13C
X_freq = 125.76529768[MHz]
0.7

X_offset = 100[ppm]
X_points = 32768
X_prescans = 4
0.6

X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
0.5

Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
0.4

Clipped = FALSE
Mod_return = 1
0.3

Scans = 87650
(thousandths)

Total_scans = 87650
0.2

X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
0.1

X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
50.0 40.0 30.0 20.0 10.0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60

5.8090

2.4515
2.3943
48.1687
48.0066
47.8349
47.7586
47.6632
47.5869
47.4915
47.4152
47.3198
47.1481

39.8036

31.4576

23.0543

11.0074

Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C

 2.5
2.4
2.3
2.2

−−−− PROCESSING PARAMETERS −−−−

dc_balance : 0 : FALSE
sexp : 2.0[Hz] : 0.0[s]
2.1

trapezoid3 : 0[%] : 80[%] : 100[%]

zerofill : 1
2.0

fft : 1 : TRUE : TRUE

machinephase
ppm
1.9

Derived from: RIKY−single_pulse_dec−3.jd

1.8
1.7
1.6

Filename = RIKY−single_pulse_dec
Author = delta
1.5

Experiment = single_pulse_dec
Sample_id = RIKY
Solvent = METHANOL−D3
1.4

Creation_time = 2−JAN−2017 09:45:55

Revision_time = 6−JAN−2017 12:02:53
1.3

Current_time = 6−JAN−2017 12:04:05

Content = single pulse decouple
1.2

Data_format = 1D COMPLEX
Dim_size = 26214
1.1

Dim_title = 13C
Dim_units = [ppm]
Dimensions = X
1.0

Site = ECA 500

Spectrometer = DELTA2_NMR
0.9

Field_strength = 11.7473579[T] (500[MH

X_acq_duration = 0.83361792[s]
0.8

X_domain = 13C
X_freq = 125.76529768[MHz]
0.7

X_offset = 100[ppm]
X_points = 32768
X_prescans = 4
0.6

X_resolution = 1.19959034[Hz]
X_sweep = 39.3081761[kHz]
0.5

Irr_domain = 1H
Irr_freq = 500.15991521[MHz]
Irr_offset = 5.0[ppm]
0.4

Clipped = FALSE
Mod_return = 1
0.3

Scans = 87650
(thousandths)

Total_scans = 87650
0.2

X_90_width = 10.925[us]
X_acq_time = 0.83361792[s]
X_angle = 30[deg]
0.1

X_atn = 7.9[dB]
X_pulse = 3.64166667[us]
0

Irr_atn_dec = 21.238[dB]
Irr_atn_noe = 21.238[dB]
Irr_noise = WALTZ
46.0 45.0 44.0 43.0 42.0 41.0 40.0 39.0 38.0 37.0 36.0 35.0 34.0 33.0 32.0 31.0 30.0 29.0 28.0 27.0 26.0 25.0 24.0 23.0 22.0 21.0 Decoupling = TRUE
Initial_wait = 1[s]
Noe = TRUE
Noe_time = 2[s]
Recvr_gain = 60
45.3740

44.4106

42.9990

39.8036

31.4576

23.0543
Relaxation_delay = 2[s]
Repetition_time = 2.83361792[s]
Temp_get = 403.3[dC]

X : parts per Million : 13C