atom weight Mass percent (%)

molecule weight
Fe 55.85 Fe Si
O 16 Fe3O4 231.55 72.4 -
Si 28 SiO2 60 - 46.7

id# Time Reading No Size fraction Duration Fe (ppm) Fe Error

1 2015-08-18 15:55 2338 -150+125/20 121 67217.188 338.476
2 2015-08-18 15:58 2339 -150+125/20 121 48153.75 284.715
3 2015-08-18 16:03 2340 -150+125/20 121 56401.148 313.304
4 2015-08-18 16:06 2341 -45+38/20 121 170728 638.104
5 2015-08-18 16:11 2342 -45+38/20 121 158398.58 609.617
6 2015-08-18 16:14 2343 -45+38/20 121 145533.16 581.897
7 2015-08-18 16:17 2344 -45+38/20 121 133085 551.841
8 2015-08-18 16:21 2345 -45+38/20 121 162684.89 620.022
9 2015-08-18 16:26 2346 sticky tape 121 11271.615 670.337
10 2015-08-18 16:30 2347 -106+90/20 121 62590.191 332.639
11 2015-08-18 16:33 2348 -106+90/20 121 49286.109 286.414
12 2015-08-18 16:35 2349 -106+90/20 121 47086.629 273.61
13 2015-08-18 16:38 2350 -125+106/20 121 57037.867 316.846
14 2015-08-18 16:41 2351 -125+106/20 121 55937.328 310.47
15 2015-08-18 16:43 2352 -125+106/20 121 42685.195 267.703
16 2015-08-19 10:34 2355 -90+75/20 121 57507.957 316.223
17 2015-08-19 10:37 2356 -90+75/20 121 67363.227 350.548
18 2015-08-19 10:40 2357 -90+75/20 121 58240.313 319.691
19 2015-08-19 10:47 2358 -75+63/20 121 111626.46 479.96
20 2015-08-19 10:50 2359 -75+63/20 121 104440.49 461.885
21 2015-08-19 10:52 2360 -75+63/20 121 91285.375 424.565
22 2015-08-19 10:55 2361 -63+53/20 121 85585.781 414.71
23 2015-08-19 10:58 2362 -63+53/20 121 150268.28 593.763
24 2015-08-19 11:00 2363 -63+53/20 121 115409.4 500.096
25 2015-08-19 11:03 2364 -53+45/20 121 108121.44 475.785
26 2015-08-19 11:06 2365 -53+45/20 121 114720 495.383
27 2015-08-19 11:08 2366 -53+45/20 121 134332.53 559.686
28 2015-08-19 11:12 2367 -150+125/10 121 26667.59 195.522
29 2015-08-19 11:14 2368 -150+125/10 121 33483.813 222.194
30 2015-08-19 11:17 2369 -150+125/10 121 27644.318 196.883
31 2015-08-19 11:19 2370 -125+106/10 121 29660.494 209.604
32 2015-08-19 11:22 2371 -125+106/10 121 19070.338 161.59
33 2015-08-19 11:25 2372 -125+106/10 121 28034.566 199.309
34 2015-08-19 11:27 2373 -106+90/10 121 31314.072 218.49
35 2015-08-19 11:30 2374 -106+90/10 121 27750.35 204.509
36 2015-08-19 11:33 2375 -106+90/10 121 31488.758 212.827
37 2015-08-19 11:37 2376 -90+75/10 121 21661.816 178.01
38 2015-08-19 11:40 2377 -90+75/10 121 26130.805 193.512
39 2015-08-19 11:42 2378 -90+75/10 121 25275.695 189.195
40 2015-08-19 11:45 2379 -75+63/10 121 25106.547 192.747
41 2015-08-19 11:48 2380 -75+63/10 121 42360.316 263.611
 42 2015-08-19 11:51 2381 -75+63/10 121 35353.148 229.945
43 2015-08-19 11:54 2382 -63+53/10 121 42365.258 278.281
44 2015-08-19 11:57 2383 -63+53/10 121 41289.309 261.219
45 2015-08-19 11:59 2384 -63+53/10 121 39608.84 251.472
46 2015-08-19 12:02 2385 -53+45/10 121 51867.355 288.667
47 2015-08-19 12:05 2386 -53+45/10 121 55579.434 312.094
48 2015-08-19 12:08 2387 -53+45/10 121 69676.406 351.728
49 2015-08-19 12:11 2388 -45+38/10 121 49533.68 289.849
50 2015-08-19 12:15 2389 -45+38/10 121 44707.754 273.485
51 2015-08-19 12:18 2390 -45+38/10 121 63889.398 328.78

Stdev Deviation
Size fraction (µm) Mean Size (µm) Fe3O4 SiO2 Fe3O4 SiO2
-150+125 137.5 1.321240117 5.2674319 6.6062006 6.5842899
-125+106 115.5 1.103894004 2.0532735 5.51947 2.5665918
-106+90 98 1.159263516 1.6818037 5.7963176 2.1022546
20% -90+75 82.5 0.758808714 0.8934057 3.7940436 1.1167572
Magnetite -75+63 69 1.425574392 3.7167178 7.127872 4.6458972
-63+53 58 4.473993495 5.5386963 22.369967 6.9233704
-53+45 49 1.88409897 1.9432498 9.4204949 2.4290622
-45+38 41.5 2.053905891 1.478104 10.270456 2.1454053

Stdev Deviation
Size fraction (µm) Mean Size (µm) Fe3O4 SiO2 Fe3O4 SiO2
-150+125 137.5 0.509380619 1.277887 5.0938062 1.4198744
-125+106 115.5 0.788155135 3.9240652 7.8815513 4.3600724
-106+90 98 0.29156258 1.0565966 2.9156258 1.1739963
10% -90+75 82.5 0.327828352 0.6552447 3.2782835 0.7280497
Magnetite -75+63 69 1.199198307 3.4114291 11.991983 3.7904767
-63+53 58 0.191985886 9.2038145 1.9198589 10.226461
-53+45 49 1.298452179 2.8618969 12.984522 3.1798854
-45+38 41.5 1.378876046 0.98731 13.78876 1.0970111
 MEASURED CALCULATED
Si (ppm) Si Error Fe (%) Si (%) Fe3O4 (%) stdev SiO2 (%) stdev Fe3O4 (%)
317955.91 1596.047 6.7217188 31.795591 9.29 68.13 20
356564.63 1728.582 4.815375 35.656463 6.65 7.91 76.41 74.15 20
363618.44 1766.398 5.6401148 36.361844 7.79 1.32 77.92 5.27 20
366708.84 1807.611 17.072797 36.670884 23.59 2.05 78.58 1.48 20
360906.5 1778.451 15.839858 36.09065 21.89 77.34 20
373830.88 1849.953 14.553316 37.383088 20.11 80.11 20
382110.94 1824.738 13.3085 38.211094 18.39 20.33 81.88 80.31 20
368414.75 1789.087 16.268489 36.841475 22.48 2.05 78.95 1.48 20
26085.213 4947.707 1.1271615 2.6085213 1.56 5.59
365133 1743.956 6.2590191 36.513303 8.65 1.16 78.24 1.68 20
377337.53 1781.18 4.9286109 37.733753 6.81 7.32 80.86 80.16 20
379784 1759.846 4.7086629 37.9784 6.51 1.16 81.38 1.68 20
350951.91 1723.72 5.7037867 35.095191 7.88 1.10 75.20 2.05 20
356845.31 1704.679 5.5937328 35.684531 7.73 7.17 76.47 76.96 20
369690.75 1750.425 4.2685195 36.969075 5.90 1.10 79.22 2.05 20
363302.69 1775.893 5.7507957 36.330269 7.95 0.76 77.85 0.89 20
360437 1741.986 6.7363227 36.043697 9.31 8.44 77.24 78.03 20
368651.28 1757.343 5.8240313 36.865128 8.05 0.76 79.00 0.89 20
315560.38 1683.439 11.162646 31.556038 15.43 1.43 67.62 3.72 20
332305.31 1738.943 10.444049 33.230531 14.43 14.16 71.21 71.29 20
350242.91 1733.459 9.1285375 35.024291 12.62 1.43 75.05 3.72 20
408122.78 1848.435 8.5585781 40.812278 11.83 4.47 87.45 5.54 20
356667.44 1760.499 15.026828 35.666744 20.77 16.18 76.43 82.25 20
386696.47 1787.347 11.54094 38.669647 15.95 4.47 82.86 5.54 20
388694.13 1847.046 10.812144 38.869413 14.94 1.88 83.29 1.94 20
372690.47 1790.34 11.472002 37.269047 15.85 16.45 79.86 81.05 20
373301.41 1806.596 13.433253 37.330141 18.56 1.88 79.99 1.94 20
361947.25 1706.159 2.666759 36.194725 3.69 0.51 77.56 1.28 10
357148.38 1677.941 3.3483813 35.714838 4.63 4.04 76.53 77.72 10
369003.88 1711.875 2.7644318 36.900388 3.82 0.51 79.07 1.28 10
357774.66 1711.115 2.9660494 35.777466 4.10 0.79 76.67 3.92 10
391363.41 1814.196 1.9070338 39.136341 2.64 3.54 83.86 79.36 10
361925.13 1747.176 2.8034566 36.192513 3.87 0.79 77.56 3.92 10
368968.75 1727.586 3.1314072 36.896875 4.33 0.29 79.06 1.06 10
376953.31 1754.675 2.775035 37.695331 3.84 4.17 80.78 79.56 10
367948.75 1726.593 3.1488758 36.794875 4.35 0.29 78.85 1.06 10
393074.19 1822.866 2.1661816 39.307419 2.99 0.33 84.23 0.66 10
397763.22 1785.907 2.6130805 39.776322 3.61 3.37 85.23 84.49 10
392018.66 1796.401 2.5275695 39.201866 3.49 0.33 84.00 0.66 10
415472.31 1884.476 2.5106547 41.547231 3.47 1.20 89.03 3.41 10
388290.75 1791.743 4.2360316 38.829075 5.85 4.74 83.21 85.09 10
387521.47 1782.341 3.5353148 38.752147 4.89 1.20 83.04 3.41 10
483659.72 2009.487 4.2365258 48.365972 5.85 0.19 103.64 9.20 10
407451 1819.019 4.1289309 40.745103 5.71 5.68 87.31 93.02 10
411225 1847.863 3.960884 41.122497 5.47 0.19 88.12 9.20 10
406541.59 1805.641 5.1867355 40.654159 7.17 1.30 87.12 2.86 10
400317.06 1785.354 5.5579434 40.031706 7.68 8.16 85.78 84.84 10
380933.75 1748.359 6.9676406 38.093375 9.63 1.30 81.63 2.86 10
404530.44 1844.434 4.953368 40.453044 6.85 1.38 86.69 0.99 10
401519.31 1795.169 4.4707754 40.151931 6.18 7.28 86.04 85.82 10
395482.63 1780.172 6.3889398 39.548263 8.83 1.38 84.75 0.99 10

5
4.5
4
3.5
3
2.5 20% magnetite
10% magnetite
2
1.5
1
0.5
0
20 40 60 80 100 120 140 160
CALCULATED Error
SiO2 (%) Fe3O4 SiO2 Notes
80 6.6062006 6.5842899 each sample is testted three times, cup was shaken between measurements
80
80
80 10.270456 2.1454053
80 small marks on the surface
80 small marks on the surface
80
80

80 5.7963176 2.1022546 the surface hasn't been cleaned

80
80
80 5.51947 2.5665918
80
80
80 3.7940436 1.1167572
80
80
80 7.127872 4.6458972
80
80
80 22.369967 6.9233704
80
80
80 9.4204949 2.4290622
80
80
90 5.0938062 1.4198744
90
90
90 7.8815513 4.3600724
90
90
90 2.9156258 1.1739963
90
90
90 3.2782835 0.7280497
90
90
90 11.991983 3.7904767
90
90
90 1.9198589 10.226461
90
90
90 12.984522 3.1798854
90
90
90 13.78876 1.0970111
90
90
measurements
 atom weight
molecule weight
Fe 55.85
O 16 Fe3O4 231.55
Si 28 SiO2 60

id# Time size Reading No Size fraction Duration

1 2015-08-18 15:55 16 2338 -150+125/20 121
2 2015-08-18 15:58 16 2339 -150+125/20 121
3 2015-08-18 16:03 16 2340 -150+125/20 121
13 2015-08-18 16:38 15 2350 -125+106/20 121
14 2015-08-18 16:41 15 2351 -125+106/20 121
15 2015-08-18 16:43 15 2352 -125+106/20 121
10 2015-08-18 16:30 14 2347 -106+90/20 121
11 2015-08-18 16:33 14 2348 -106+90/20 121
12 2015-08-18 16:35 14 2349 -106+90/20 121
16 2015-08-19 10:34 13 2355 -90+75/20 121
17 2015-08-19 10:37 13 2356 -90+75/20 121
18 2015-08-19 10:40 13 2357 -90+75/20 121
19 2015-08-19 10:47 12 2358 -75+63/20 121
20 2015-08-19 10:50 12 2359 -75+63/20 121
21 2015-08-19 10:52 12 2360 -75+63/20 121
22 2015-08-19 10:55 11 2361 -63+53/20 121
23 2015-08-19 10:58 11 2362 -63+53/20 121
24 2015-08-19 11:00 11 2363 -63+53/20 121
25 2015-08-19 11:03 10 2364 -53+45/20 121
26 2015-08-19 11:06 10 2365 -53+45/20 121
27 2015-08-19 11:08 10 2366 -53+45/20 121
4 2015-08-18 16:06 9 2341 -45+38/20 121
5 2015-08-18 16:11 9 2342 -45+38/20 121
6 2015-08-18 16:14 9 2343 -45+38/20 121
7 2015-08-18 16:17 9 2344 -45+38/20 121
8 2015-08-18 16:21 9 2345 -45+38/20 121
28 2015-08-19 11:12 8 2367 -150+125/10 121
29 2015-08-19 11:14 8 2368 -150+125/10 121
30 2015-08-19 11:17 8 2369 -150+125/10 121
31 2015-08-19 11:19 7 2370 -125+106/10 121
32 2015-08-19 11:22 7 2371 -125+106/10 121
33 2015-08-19 11:25 7 2372 -125+106/10 121
34 2015-08-19 11:27 6 2373 -106+90/10 121
35 2015-08-19 11:30 6 2374 -106+90/10 121
36 2015-08-19 11:33 6 2375 -106+90/10 121
37 2015-08-19 11:37 5 2376 -90+75/10 121
38 2015-08-19 11:40 5 2377 -90+75/10 121
39 2015-08-19 11:42 5 2378 -90+75/10 121
40 2015-08-19 11:45 4 2379 -75+63/10 121
41 2015-08-19 11:48 4 2380 -75+63/10 121
42 2015-08-19 11:51 4 2381 -75+63/10 121
 43 2015-08-19 11:54 3 2382 -63+53/10 121
44 2015-08-19 11:57 3 2383 -63+53/10 121
45 2015-08-19 11:59 3 2384 -63+53/10 121
46 2015-08-19 12:02 2 2385 -53+45/10 121
47 2015-08-19 12:05 2 2386 -53+45/10 121
48 2015-08-19 12:08 2 2387 -53+45/10 121
49 2015-08-19 12:11 1 2388 -45+38/10 121
50 2015-08-19 12:15 1 2389 -45+38/10 121
51 2015-08-19 12:18 1 2390 -45+38/10 121
9 2015-08-18 16:26 2346 stiky tape 121

3 gram of silica 80:20 magnetite XRF measurement

Size fraction (µm) Mean Size (µm) Fe3O4 SiO2
-150+125 137.5 7.9 74.2
-125+106 115.5 7.2 77.0
-106+90 98 7.3 80.2
20% -90+75 82.5 8.4 78.0
Magnetite -75+63 69 14.2 71.3
-63+53 58 16.2 82.2
-53+45 49 16.5 81.0
-45+38 41.5 20.3 78.7

3 gram of silica 90:10 magnetite Measured

Size fraction (µm) Mean Size (µm) Fe3O4 SiO2
-150+125 137.5 4.0 77.7
-125+106 115.5 3.5 79.4
-106+90 98 4.2 79.6
10% -90+75 82.5 3.4 84.5
Magnetite -75+63 69 4.7 85.1
-63+53 58 5.7 93.0
-53+45 49 8.2 84.8
-45+38 41.5 7.3 85.8
 Mass percent (%)
Fe Si
72.4 -
- 46.7

MEASURED
Fe (ppm) Fe Error Si (ppm) Si Error Fe (%) Si (%) Fe3O4 (%) stdev
67217.188 338.476 317955.91 1596.047 6.72 31.80 9.29
48153.75 284.715 356564.63 1728.582 4.82 35.66 6.65 7.91
56401.148 313.304 363618.44 1766.398 5.64 36.36 7.79 1.32
57037.867 316.846 350951.91 1723.72 5.70 35.10 7.88
55937.328 310.47 356845.31 1704.679 5.59 35.68 7.73 7.17
42685.195 267.703 369690.75 1750.425 4.27 36.97 5.90 1.10
62590.191 332.639 365133 1743.956 6.26 36.51 8.65
49286.109 286.414 377337.53 1781.18 4.93 37.73 6.81 7.32
47086.629 273.61 379784 1759.846 4.71 37.98 6.51 1.16
57507.957 316.223 363302.69 1775.893 5.75 36.33 7.95
67363.227 350.548 360437 1741.986 6.74 36.04 9.31 8.44
58240.313 319.691 368651.28 1757.343 5.82 36.87 8.05 0.76
111626.461 479.96 315560.38 1683.439 11.16 31.56 15.43
104440.492 461.885 332305.31 1738.943 10.44 33.23 14.43 14.16
91285.375 424.565 350242.91 1733.459 9.13 35.02 12.62 1.43
85585.781 414.71 408122.78 1848.435 8.56 40.81 11.83
150268.281 593.763 356667.44 1760.499 15.03 35.67 20.77 16.18
115409.398 500.096 386696.47 1787.347 11.54 38.67 15.95 4.47
108121.438 475.785 388694.13 1847.046 10.81 38.87 14.94
114720.016 495.383 372690.47 1790.34 11.47 37.27 15.85 16.45
134332.531 559.686 373301.41 1806.596 13.43 37.33 18.56 1.88
170727.969 638.104 366708.84 1807.611 17.07 36.67 23.59
158398.578 609.617 360906.5 1778.451 15.84 36.09 21.89
145533.156 581.897 373830.88 1849.953 14.55 37.38 20.11
133085 551.841 382110.94 1824.738 13.31 38.21 18.39 20.33
162684.891 620.022 368414.75 1789.087 16.27 36.84 22.48 2.05
26667.59 195.522 361947.25 1706.159 2.67 36.19 3.69
33483.813 222.194 357148.38 1677.941 3.35 35.71 4.63 4.04
27644.318 196.883 369003.88 1711.875 2.76 36.90 3.82 0.51
29660.494 209.604 357774.66 1711.115 2.97 35.78 4.10
19070.338 161.59 391363.41 1814.196 1.91 39.14 2.64 3.54
28034.566 199.309 361925.13 1747.176 2.80 36.19 3.87 0.79
31314.072 218.49 368968.75 1727.586 3.13 36.90 4.33
27750.35 204.509 376953.31 1754.675 2.78 37.70 3.84 4.17
31488.758 212.827 367948.75 1726.593 3.15 36.79 4.35 0.29
21661.816 178.01 393074.19 1822.866 2.17 39.31 2.99
26130.805 193.512 397763.22 1785.907 2.61 39.78 3.61 3.37
25275.695 189.195 392018.66 1796.401 2.53 39.20 3.49 0.33
25106.547 192.747 415472.31 1884.476 2.51 41.55 3.47
42360.316 263.611 388290.75 1791.743 4.24 38.83 5.85 4.74
35353.148 229.945 387521.47 1782.341 3.54 38.75 4.89 1.20
42365.258 278.281 483659.72 2009.487 4.24 48.37 5.85
41289.309 261.219 407451 1819.019 4.13 40.75 5.71 5.68
39608.84 251.472 411225 1847.863 3.96 41.12 5.47 0.19
51867.355 288.667 406541.59 1805.641 5.19 40.65 7.17
55579.434 312.094 400317.06 1785.354 5.56 40.03 7.68 8.16
69676.406 351.728 380933.75 1748.359 6.97 38.09 9.63 1.30
49533.68 289.849 404530.44 1844.434 4.95 40.45 6.85
44707.754 273.485 401519.31 1795.169 4.47 40.15 6.18 7.28
63889.398 328.78 395482.63 1780.172 6.39 39.55 8.83 1.38
11271.615 670.337 26085.213 4947.707 1.13 2.61 1.56

Quantitative determination stdev

Fe3O4 SiO2 Fe3O4 SiO2 100.0
20 80 1.3 5.3 90.0
20 80 1.1 2.1
80.0
20 80 1.2 1.7
20 80 0.8 0.9 70.0

XRF measurement (%)

20 80 1.4 3.7 60.0
20 80 4.5 5.5
20 80 1.9 1.9 50.0
20 80 2.1 1.5 40.0

30.0
Quantitative determination stdev
Fe3O4 SiO2 Fe3O4 SiO2 20.0
10 90 0.5 1.3 10.0
10 90 0.8 3.9
0.0
10 90 0.3 1.1
30 50 70 90 110
10 90 0.3 0.7
10 90 1.2 3.4 Size (micron)
10 90 0.2 9.2
20% magnetite 10% magnetite 80% silica
10 90 1.3 2.9
10 90 1.4 1.0
 68.08
CALCULATED
SiO2 (%) stdev Fe3O4 (%) SiO2 (%) Notes
68.13 20 80 each sample is testted three times, cup was shaken between measurement
76.41 74.15 20 80
77.92 5.27 20 80
75.20 20 80
76.47 76.96 20 80
79.22 2.05 20 80
78.24 20 80 the surface hasn't been cleaned
80.86 80.16 20 80
81.38 1.68 20 80
77.85 20 80
77.24 78.03 20 80
79.00 0.89 20 80
67.62 20 80
71.21 71.29 20 80
75.05 3.72 20 80
87.45 20 80
76.43 82.25 20 80
82.86 5.54 20 80
83.29 20 80
79.86 81.05 20 80
79.99 1.94 20 80
78.58 20 80 small marks on the surface
77.34 20 80 small marks on the surface
80.11 20 80
81.88 80.31 20 80
78.95 1.48 20 80
77.56 10 90
76.53 77.72 10 90
79.07 1.28 10 90
76.67 10 90
83.86 79.36 10 90
77.56 3.92 10 90
79.06 10 90
80.78 79.56 10 90
78.85 1.06 10 90
84.23 10 90
85.23 84.49 10 90
84.00 0.66 10 90
89.03 10 90
83.21 85.09 10 90
83.04 3.41 10 90
 103.64 10 90
87.31 93.02 10 90
88.12 9.20 10 90
87.12 10 90
85.78 84.84 10 90
81.63 2.86 10 90
86.69 10 90
86.04 85.82 10 90
84.75 0.99 10 90
5.59

70 90 110 130 150

Size (micron)

10% magnetite 80% silica 90% silica

as shaken between measurements
 Mass percent (%)
molecule weight
Fe Si
Fe3O4 231.55 72.36 -
SiO2 60.09 - 46.74 46.74256

MEASURED
Reading No Size fraction Fe (ppm) Fe Error Si (ppm) Si Error Fe (%) Si (%)
2393 +125/20/ 2/8 58744.28 329.482 397878.8 1841.488 5.87 39.79
2394 +125/20/ 2/8 57752.57 316.886 374490.3 1779.728 5.78 37.45
2395 +125/20/ 2/8 57181.88 316.839 377267.2 1788.215 5.72 37.73
2396 +125/20/ 1/8 81004.77 605.428 469617.2 2049.721 8.10 46.96
2397 +125/20/ 1/8 89566.27 679.823 486170.6 2098.004 8.96 48.62
2398 +125/20/ 1/8 79870.04 606.589 493333.7 2111.065 7.99 49.33
2399 +106/20 2/8 58538.04 311.632 390884.3 1790.46 5.85 39.09
2400 +106/20 2/8 56979.03 314.406 390376.8 1796.787 5.70 39.04
2401 +106/20 2/8 62179.1 327.697 391077 1796.725 6.22 39.11
2402 +90/20 2/8 63461.68 341.538 400012.1 1837.184 6.35 40.00
2403 +90/20 2/8 69933.89 367.296 411032.4 1897.729 6.99 41.10
2404 +90/20 2/8 75304.61 385.274 390889.4 1867.669 7.53 39.09
2405 +90/20 1/8 74788.43 549.267 499454.3 2054.455 7.48 49.95
2406 +90/20 1/8 66079.88 365.058 449403.7 1929.456 6.61 44.94
2407 +90/20 1/8 70761.81 381.807 448589.4 1953.791 7.08 44.86
2408 +75/20 2/8 64760.76 359.899 446460.1 1928.723 6.48 44.65
2409 +75/20 2/8 94244.88 449.195 420559.5 1890.71 9.42 42.06
2410 +75/20 2/8 82702.34 407.759 396059.9 1843.713 8.27 39.61
2411 +75/20 1/8 121759.1 880.486 525484 2093.95 12.18 52.55
2412 +75/20 1/8 92903.58 445.502 446593 1941.325 9.29 44.66
2413 +75/20 1/8 93805.52 655.019 488285 2051.885 9.38 48.83
2416 +125/10/ 2/8 28669.83 212.329 424565.7 1892.65 2.87 42.46
2417 +125/10/ 2/8 30701.53 218.869 423330.9 1890.028 3.07 42.33
2418 +125/10/ 2/8 31158.72 217.869 415835.7 1854.486 3.12 41.58
2419 +125/10/ 1/8 83437.46 903.707 690314.9 2110.021 8.34 69.03
2420 +125/10/ 1/8 37561.06 260.911 488385.5 2030.211 3.76 48.84
2421 +125/10/ 1/8 60123.17 544.073 596584.4 2209.731 6.01 59.66
2422 +106/10 2/8 32486.97 224.91 448627.8 1895.281 3.25 44.86
2423 +106/10 2/8 29155.22 211.22 436428.3 1858.686 2.92 43.64
2424 +106/10 2/8 26905.46 206.017 448381.1 1934.708 2.69 44.84
2425 +106/10 1/8 33391.81 248.801 524318.9 2051.527 3.34 52.43
2426 +106/10 1/8 37024.88 270.187 547086.5 2098.958 3.70 54.71
2427 +106/10 1/8 76004.51 744.552 656989.5 2056.837 7.60 65.70
2428 +90/10 2/8 32107.1 218.276 420568.9 1853.267 3.21 42.06
2429 +90/10 2/8 28828.89 211.379 453529.8 1880.414 2.88 45.35
2430 +90/10 2/8 32502.77 229.115 470817.4 1977.715 3.25 47.08
2431 +90/10 1/8 45207.74 314.061 548378.3 2123.021 4.52 54.84
2432 +90/10 1/8 46497.54 301.927 533110.3 2039 4.65 53.31
2433 +90/10 1/8 46722.85 298.222 491854.1 1990.974 4.67 49.19
2434 +75/10 2/8 48883 304.397 517518.5 2028.999 4.89 51.75
2435 +75/10 2/8 49634.33 300.759 499173.5 1957.597 4.96 49.92
2436 +75/10 2/8 35709.34 236.527 465150 1957.07 3.57 46.51
2437 +75/10 1/8 59778.15 507.496 608226.7 2090.314 5.98 60.82
2438 +75/10 1/8 61041.6 758.883 741724.6 2058.03 6.10 74.17
2439 +75/10 1/8 53253.61 458.981 594301.9 2124.48 5.33 59.43
EASURED CALCULATED
Fe3O4 (%) stdev SiO2 (%) stdev Fe3O4 (%) SiO2 (%)
8.12 85.12 20 80 For -150 +125 fraction,
7.98 8.00 80.12 81.98 20 80
7.90 0.11 80.71 2.73 20 80
11.19 100.47 20 80
12.38 11.54 104.01 103.34 20 80
11.04 0.73 105.54 2.60 20 80
8.09 83.62 20 80 umarked container
7.87 8.19 83.52 83.60 20 80 umarked container
8.59 0.37 83.67 0.08 20 80 umarked container
8.77 85.58 20 80
9.66 9.61 87.94 85.71 20 80
10.41 0.82 83.63 2.16 20 80
10.34 106.85 20 80
9.13 9.75 96.14 99.66 20 80
9.78 0.60 95.97 6.23 20 80
8.95 95.51 20 80
13.02 11.13 89.97 90.07 20 80
11.43 2.05 84.73 5.39 20 80
16.83 112.42 20 80
12.84 14.21 95.54 104.14 20 80
12.96 2.27 104.46 8.44 20 80
3.96 90.83 10 90
4.24 4.17 90.57 90.12 10 90
4.31 0.18 88.96 1.01 10 90
11.53 147.68 10 90
5.19 8.34 104.48 126.60 10 90
8.31 3.17 127.63 21.62 10 90
4.49 95.98 10 90
4.03 4.08 93.37 95.09 10 90
3.72 0.39 95.93 1.49 10 90
4.61 112.17 10 90
5.12 6.75 117.04 123.26 10 90
10.50 3.26 140.55 15.18 10 90
4.44 89.98 10 90
3.98 4.30 97.03 95.91 10 90
4.49 0.28 100.73 5.46 10 90
6.25 117.32 10 90
6.43 6.38 114.05 112.20 10 90
6.46 0.11 105.23 6.26 10 90
6.76 110.72 10 90 there are less dark dotts and more grey than
6.86 6.18 106.79 105.67 10 90
4.93 1.08 99.51 5.68 10 90
8.26 130.12 10 90
8.44 8.02 158.68 138.65 10 90
7.36 0.58 127.14 17.41 10 90
5 fraction,

dotts and more grey than in previous samples

 Mass percent (%)
molecule weight
Fe Si
Fe3O4 231.55 72.36 -
SiO2 60.09 - 46.74

MEASURED
Reading No Size fraction Fe (ppm) Fe Error Si (ppm) Si Error Fe (%) Si (%) Fe3O4 (%)
2338 +125/20/ 8/8 67217.19 338.476 317955.9 1596.047 6.72 31.80 9.29
2339 +125/20/ 8/8 48153.75 284.715 356564.6 1728.582 4.82 35.66 6.65
2340 +125/20/ 8/8 56401.15 313.304 363618.4 1766.398 5.64 36.36 7.79
2393 +125/20/ 2/8 58744.28 329.482 397878.8 1841.488 5.87 39.79 8.12
2394 +125/20/ 2/8 57752.57 316.886 374490.3 1779.728 5.78 37.45 7.98
2395 +125/20/ 2/8 57181.88 316.839 377267.2 1788.215 5.72 37.73 7.90
2396 +125/20/ 1/8 81004.77 605.428 469617.2 2049.721 8.10 46.96 11.19
2397 +125/20/ 1/8 89566.27 679.823 486170.6 2098.004 8.96 48.62 12.38
2398 +125/20/ 1/8 79870.04 606.589 493333.7 2111.065 7.99 49.33 11.04
2350 +106/20 8/8 57037.87 316.846 350951.9 1723.72 5.70 35.10 7.88
2351 +106/20 8/8 55937.33 310.47 356845.3 1704.679 5.59 35.68 7.73
2352 +106/20 8/8 42685.2 267.703 369690.8 1750.425 4.27 36.97 5.90
2399 +106/20 2/8 58538.04 311.632 390884.3 1790.46 5.85 39.09 8.09
2400 +106/20 2/8 56979.03 314.406 390376.8 1796.787 5.70 39.04 7.87
2401 +106/20 2/8 62179.1 327.697 391077 1796.725 6.22 39.11 8.59
2347 +90/20 8/8 62590.19 332.639 365133 1743.956 6.26 36.51 8.65
2348 +90/20 8/8 49286.11 286.414 377337.5 1781.18 4.93 37.73 6.81
2349 +90/20 8/8 47086.63 273.61 379784 1759.846 4.71 37.98 6.51
2402 +90/20 2/8 63461.68 341.538 400012.1 1837.184 6.35 40.00 8.77
2403 +90/20 2/8 69933.89 367.296 411032.4 1897.729 6.99 41.10 9.66
2404 +90/20 2/8 75304.61 385.274 390889.4 1867.669 7.53 39.09 10.41
2405 +90/20 1/8 74788.43 549.267 499454.3 2054.455 7.48 49.95 10.34
2406 +90/20 1/8 66079.88 365.058 449403.7 1929.456 6.61 44.94 9.13
2407 +90/20 1/8 70761.81 381.807 448589.4 1953.791 7.08 44.86 9.78
2355 +75/20 8/8 57507.96 316.223 363302.7 1775.893 5.75 36.33 7.95
2356 +75/20 8/8 67363.23 350.548 360437 1741.986 6.74 36.04 9.31
2357 +75/20 8/8 58240.31 319.691 368651.3 1757.343 5.82 36.87 8.05
2408 +75/20 2/8 64760.76 359.899 446460.1 1928.723 6.48 44.65 8.95
2409 +75/20 2/8 94244.88 449.195 420559.5 1890.71 9.42 42.06 13.02
2410 +75/20 2/8 82702.34 407.759 396059.9 1843.713 8.27 39.61 11.43
2411 +75/20 1/8 121759.1 880.486 525484 2093.95 12.18 52.55 16.83
2412 +75/20 1/8 92903.58 445.502 446593 1941.325 9.29 44.66 12.84
2413 +75/20 1/8 93805.52 655.019 488285 2051.885 9.38 48.83 12.96
2367 +125/10/ 8/8 26667.59 195.522 361947.3 1706.159 2.67 36.19 3.69
2368 +125/10/ 8/8 33483.81 222.194 357148.4 1677.941 3.35 35.71 4.63
2369 +125/10/ 8/8 27644.32 196.883 369003.9 1711.875 2.76 36.90 3.82
2416 +125/10/ 2/8 28669.83 212.329 424565.7 1892.65 2.87 42.46 3.96
2417 +125/10/ 2/8 30701.53 218.869 423330.9 1890.028 3.07 42.33 4.24
2418 +125/10/ 2/8 31158.72 217.869 415835.7 1854.486 3.12 41.58 4.31
2419 +125/10/ 1/8 83437.46 903.707 690314.9 2110.021 8.34 69.03 11.53
2420 +125/10/ 1/8 37561.06 260.911 488385.5 2030.211 3.76 48.84 5.19
2421 +125/10/ 1/8 60123.17 544.073 596584.4 2209.731 6.01 59.66 8.31
2370 +106/10 8/8 29660.49 209.604 357774.7 1711.115 2.97 35.78 4.10
2371 +106/10 8/8 19070.34 161.59 391363.4 1814.196 1.91 39.14 2.64
2372 +106/10 8/8 28034.57 199.309 361925.1 1747.176 2.80 36.19 3.87
2422 +106/10 2/8 32486.97 224.91 448627.8 1895.281 3.25 44.86 4.49
2423 +106/10 2/8 29155.22 211.22 436428.3 1858.686 2.92 43.64 4.03
2424 +106/10 2/8 26905.46 206.017 448381.1 1934.708 2.69 44.84 3.72
2425 +106/10 1/8 33391.81 248.801 524318.9 2051.527 3.34 52.43 4.61
2426 +106/10 1/8 37024.88 270.187 547086.5 2098.958 3.70 54.71 5.12
2427 +106/10 1/8 76004.51 744.552 656989.5 2056.837 7.60 65.70 10.50
2373 +90/10 8/8 31314.07 218.49 368968.8 1727.586 3.13 36.90 4.33
2374 +90/10 8/8 27750.35 204.509 376953.3 1754.675 2.78 37.70 3.84
2375 +90/10 8/8 31488.76 212.827 367948.8 1726.593 3.15 36.79 4.35
2428 +90/10 2/8 32107.1 218.276 420568.9 1853.267 3.21 42.06 4.44
2429 +90/10 2/8 28828.89 211.379 453529.8 1880.414 2.88 45.35 3.98
2430 +90/10 2/8 32502.77 229.115 470817.4 1977.715 3.25 47.08 4.49
2431 +90/10 1/8 45207.74 314.061 548378.3 2123.021 4.52 54.84 6.25
2432 +90/10 1/8 46497.54 301.927 533110.3 2039 4.65 53.31 6.43
2433 +90/10 1/8 46722.85 298.222 491854.1 1990.974 4.67 49.19 6.46
2376 +75/10 8/8 21661.82 178.01 393074.2 1822.866 2.17 39.31 2.99
2377 +75/10 8/8 26130.81 193.512 397763.2 1785.907 2.61 39.78 3.61
2378 +75/10 8/8 25275.7 189.195 392018.7 1796.401 2.53 39.20 3.49
2434 +75/10 2/8 48883 304.397 517518.5 2028.999 4.89 51.75 6.76
2435 +75/10 2/8 49634.33 300.759 499173.5 1957.597 4.96 49.92 6.86
2436 +75/10 2/8 35709.34 236.527 465150 1957.07 3.57 46.51 4.93
2437 +75/10 1/8 59778.15 507.496 608226.7 2090.314 5.98 60.82 8.26
2438 +75/10 1/8 61041.6 758.883 741724.6 2058.03 6.10 74.17 8.44
2439 +75/10 1/8 53253.61 458.981 594301.9 2124.48 5.33 59.43 7.36

Conclusion
1 For coarse fractions (+106) with 10% magnetite, Silica (silicon) reading 2/8 of 3 gram sub sam
2 For middle fractions (-106 +75) with 10% magnetite, Silica (silicon) reading 8/8 of 3 gram sub
3 1/8 gives the closest results for Iron reading for middle size fraction (-106 +75) with 10% mag
4 the silicon reading results do not make sense with 1/8 sub samples (Silica > 100%)
 CALCULATED (TARGET)
stdev SiO2 (%) stdev Fe3O4 (%) SiO2 (%)
68.13 20 80
7.91 76.41 74.15 20 80
1.32 77.92 5.27 20 80
85.12 20 80
8.00 80.12 81.98 20 80
0.11 80.71 2.73 20 80
100.47 20 80
11.54 104.01 103.34 20 80
0.73 105.54 2.60 20 80
75.20 20 80
7.17 76.47 76.96 20 80
1.10 79.22 2.05 20 80
83.62 20 80 umarked container
8.19 83.52 83.60 20 80 umarked container
0.37 83.67 0.08 20 80 umarked container
78.24 20 80 the surface hasn't been cleaned
7.32 80.86 80.16 20 80
1.16 81.38 1.68 20 80
85.58 20 80
9.61 87.94 85.71 20 80
0.82 83.63 2.16 20 80
106.85 20 80
9.75 96.14 99.66 20 80
0.60 95.97 6.23 20 80
77.85 20 80
8.44 77.24 78.03 20 80
0.76 79.00 0.89 20 80
95.51 20 80
11.13 89.97 90.07 20 80
2.05 84.73 5.39 20 80
112.42 20 80
14.21 95.54 104.14 20 80
2.27 104.46 8.44 20 80
77.56 10 90
4.04 76.53 77.72 10 90
0.51 79.07 1.28 10 90
90.83 10 90
 4.17 90.57 90.12 10 90
0.18 88.96 1.01 10 90
147.68 10 90
8.34 104.48 126.60 10 90
3.17 127.63 21.62 10 90
76.67 10 90
3.54 83.86 79.36 10 90
0.79 77.56 3.92 10 90
95.98 10 90
4.08 93.37 95.09 10 90
0.39 95.93 1.49 10 90
112.17 10 90
6.75 117.04 123.26 10 90
3.26 140.55 15.18 10 90
79.06 10 90
4.17 80.78 79.56 10 90
0.29 78.85 1.06 10 90
89.98 10 90
4.30 97.03 95.91 10 90
0.28 100.73 5.46 10 90
117.32 10 90
6.38 114.05 112.20 10 90
0.11 105.23 6.26 10 90
84.23 10 90
3.37 85.23 84.49 10 90
0.33 84.00 0.66 10 90
110.72 10 90 there are less dark dotts and more grey than in previous samp
6.18 106.79 105.67 10 90
1.08 99.51 5.68 10 90
130.12 10 90
8.02 158.68 138.65 10 90
0.58 127.14 17.41 10 90

ding 2/8 of 3 gram sub samples are showing the closest results with calculated value
reading 8/8 of 3 gram sub samples are showing the closest results with calculated value
n (-106 +75) with 10% magnetite. Deviations are high on coarse fractions (+106)
s (Silica > 100%)
more grey than in previous samples
 Mass percent (%)
molecule weight
Fe Si O
Fe3O4 231.55 72.36 - 27.64
SiO2 60.08 - 46.69 53.31
60.09 46.74

XRF READING
Reading No Size retain (µm) Sample weight (gr) Fe (ppm) Fe Error Si (ppm) Si Error Fe (%)
2444 21548.08 173.44 379198.2 1729.785 2.15
2445 125 3 19641.42 161.905 386459.8 1722.766 1.96
2446 22438.59 178.162 389682.8 1755.447 2.24
2447 21007.44 167.115 373442.7 1712.976 2.10
2448 125 2 21248.37 168.481 387222.2 1739.225 2.12
2449 23372.73 176.399 382590 1739.227 2.34
2450 21584.67 169.84 378681.3 1714.733 2.16
2451 106 3 21416.85 173.355 388363.9 1756.31 2.14
2452 19137.02 161.23 394050.6 1759.936 1.91
2453 23076.77 176.635 381234.6 1756.362 2.31
2454 106 2 23999.85 184.799 386257.9 1763.05 2.40
2455 29453.48 205.057 383205 1718.883 2.95
2456 16217.49 146.958 407061.8 1848.375 1.62
2457 90 3 18518.87 161.092 402217.1 1830.159 1.85
2458 18696.02 161.355 401439.9 1767.874 1.87
2459 23051.06 177.112 401103.4 1813.215 2.31
2460 90 2 21924.82 175.539 408790.9 1790.879 2.19
2461 17508.8 151.463 418942.6 1872.904 1.75
2462 24797.54 185.424 410314.8 1798.098 2.48
2463 75 3 24829.37 185.171 407709 1807.272 2.48
2464 26861.22 191.555 401130 1743.245 2.69
2465 28783.81 200.867 417448.3 1792.108 2.88
2466 75 2 22978.37 178.656 441183.6 1832.76 2.30
2467 27419.09 195.273 436625.8 1805.445 2.74
2468 25910.66 192.81 426279.2 1895.521 2.59
2469 63 3 34692.03 229.575 417735 1817.554 3.47
2470 38317.77 246.373 404388 1770.554 3.83
2471 36337.26 231.559 428203 1842.915 3.63
2472 63 2 37372.1 233.02 418828.5 1782.388 3.74
2473 31965.49 221.084 435681.8 1906.727 3.20

10% Magnetite XRF reading

10.00
9.00
8.00
7.00
% Magnetite

6.00
5.00
4.00
3.00
2.00 3 gram
1.00 2 gram
0.00
40 50 60 70 80 90 100 110 120 130

Size (micron)
 7.00

% Magnetite
6.00
5.00
4.00
3.00
2.00 3 gram
1.00 2 gram
0.00
40 50 60 70 80 90 100 110 120 130

Size (micron)

weight % density volume volume % surface

magnetite 10 5.1 1.960784 5.45829
silica 90 2.65 33.96226 94.54171
35.92305
 XRF READING MEASURED (CALCULATED)
Si (%) Fe3O4 (%) aver/stdev SiO2 (%) aver/stdev Fe3O4 (gr) SiO2 (gr) Fe3O4 (%)
37.92 2.98 81.22
38.65 2.71 2.93 82.77 82.48 0.3011 2.7023 10.03
38.97 3.10 0.20 83.46 1.15
37.34 2.90 79.98
38.72 2.94 3.02 82.93 81.62 0.2003 1.8012 10.01
38.26 3.23 0.18 81.94 1.50
37.87 2.98 81.11
38.84 2.96 2.86 83.18 82.89 0.3005 2.7031 10.00
39.41 2.64 0.19 84.40 1.66
38.12 3.19 81.65
38.63 3.32 3.53 82.73 82.15 0.2009 1.8009 10.04
38.32 4.07 0.48 82.07 0.54
40.71 2.24 87.18
40.22 2.56 2.46 86.15 86.44 0.3016 2.7040 10.03
40.14 2.58 0.19 85.98 0.65
40.11 3.19 85.91
40.88 3.03 2.88 87.55 87.73 0.2016 1.8027 10.06
41.89 2.42 0.40 89.73 1.92
41.03 3.43 87.88
40.77 3.43 3.52 87.32 87.04 0.3008 2.7001 10.02
40.11 3.71 0.16 85.91 1.01
41.74 3.98 89.41
44.12 3.18 3.65 94.49 92.47 0.2020 1.8015 10.08
43.66 3.79 0.42 93.52 2.70
42.63 3.58 91.30
41.77 4.79 4.56 89.47 89.13 0.3012 2.7015 10.03
40.44 5.30 0.88 86.61 2.36
42.82 5.02 91.71
41.88 5.16 4.87 89.70 91.58 0.2020 1.8021 10.08
43.57 4.42 0.40 93.31 1.81

90% Silica XRF reading

Silica (gr) Magnetite (gr) Silica (%) Magnetite (%)
100.00 2.7023 0.3011 89.97 10.03
90.00
80.00 1.8012 0.2003 89.99 10.01
70.00 2.7031 0.3005 90.00 10.00
60.00 1.8009 0.2009 89.96 10.04
% Silica

50.00 2.7040 0.3016 89.97 10.03

40.00
30.00
1.8027 0.2016 89.94 10.06
20.00 3 gram
10.00 2 gram
0.00
30 40 50 60 70 80 90 100 110 120 130

Size (micron)
 70.00
60.00

% Silica
50.00
40.00
30.00
20.00 3 gram
2.7001 0.3008 89.98 10.02
10.00 1.8015
2 gram 0.2020 89.92 10.08
0.00 2.7015
30 40 50 60 70 0.3012
80 90 89.97 10.03130
100 110 120
1.8021 0.2020 89.92 10.08
Size (micron)

size volume (sphere) surface ratio

150
125 136.93 1343631.90 58875 22.821773
106 115.11 798182.52 41605 19.184774
90 97.67 487641.84 29955.6 16.278821
75 82.16 290224.49 21195 13.693064
63 68.74 169973.46 14836.5 11.456439
53 57.78 100972.48 10484.46 9.6306801
45 48.84 60955.23 7488.9 8.1394103
38 41.35 37006.04 5369.4 6.8920244
CALCULATED)
SiO2 (%) O(ppm) O (%) O from Magnetite O from sili O (mag+sil)
587996.6 58.8 0.82 43.29633 44.12
89.97 582754.2 58.3 0.75 44.12545 44.88
576739.5 57.7 0.86 44.49345 45.35
594770.4 59.5 0.80 42.63918 43.44
89.99 580125.1 58.0 0.81 44.2125 45.02
581196.3 58.1 0.89 43.6836 44.58
588176.9 58.8 0.82 43.23732 44.06
90.00 579364.3 57.9 0.82 44.34286 45.16
574725.9 57.5 0.73 44.99216 45.72
584435.4 58.4 0.88 43.52884 44.41
89.96 578110 57.8 0.92 44.1024 45.02
574757.8 57.5 1.13 43.75382 44.88
567632.8 56.8 0.62 46.47776 47.10
89.97 569752.7 57.0 0.71 45.92459 46.63
570304.8 57.0 0.71 45.83586 46.55
565079.4 56.5 0.88 45.79744 46.68
89.94 558597.7 55.9 0.84 46.67518 47.51
554346.9 55.4 0.67 47.83429 48.50
554884.8 55.5 0.95 46.84918 47.80
89.98 557366.1 55.7 0.95 46.55165 47.50
561445.4 56.1 1.03 45.80048 46.83
542528.6 54.3 1.10 47.66367 48.76
89.92 526219.1 52.6 0.88 50.37374 51.25
525070.2 52.5 1.05 49.85333 50.90
538613.4 53.9 0.99 48.67197 49.66
89.97 537314.1 53.7 1.33 47.69641 49.02
547326.3 54.7 1.46 46.17247 47.64
525158.1 52.5 1.39 48.89163 50.28
89.92 533045 53.3 1.43 47.82127 49.25
522772.4 52.3 1.22 49.74554 50.97
O (mag+sil)
14.6802410587021
13.3997108710802
12.3233993135524
16.0354286125631
12.9883699223198
13.5432436264913
14.7558969106269
12.7754970377735
11.7494478179425
14.0332195822212
12.7918677134622
12.5969076178474
9.6660485556425
10.3432985103991
10.4804790319529
9.8300042389879
8.3471109308587
6.9316113499224
7.6920921133740
8.2365320768243
9.3180355893803
5.4897205562576
1.3704525565183
1.6063489708469
4.1996458817485
4.7098443183278
7.0965170683402
2.2361919529136
4.0557115379357
1.3106907088168
 97 2015-08-2 2444 ppm 1 1 13.913 1.497 9.624 1.043
98 2015-08-2 2445 ppm 1 1 52.65 2.02 8.774 1
99 2015-08-2 2446 ppm 0 1.083 22.097 1.643 9.849 1.056
100 2015-08-2 2447 ppm 0 1.131 11.111 1.413 9.491 1.014
101 2015-08-2 2448 ppm 1.293 1.568 12.363 1.44 9.789 1.025
102 2015-08-2 2449 ppm 1.718 1.584 22.637 1.612 13.246 1.106
103 2015-08-2 2450 ppm 0 1.126 12.083 1.446 13.209 1.108
104 2015-08-2 2451 ppm 0 1.082 24.291 1.678 12.299 1.113
105 2015-08-2 2452 ppm 0 1.146 13.042 1.473 12.692 1.106
106 2015-08-2 2453 ppm 0 1.558 31.171 1.742 10.785 1.054
107 2015-08-2 2454 ppm 0 1.618 17.694 1.586 12.454 1.126
108 2015-08-2 2455 ppm 0 1.361 30.244 1.779 10.778 1.083
109 2015-08-2 2456 ppm 0 1.417 9.405 1.388 9.836 1.025
110 2015-08-2 2457 ppm 1 1 11.037 1.451 9.638 1.046
111 2015-08-2 2458 ppm 1 1 11.888 1.463 9.598 1.043
112 2015-08-2 2459 ppm 1.16 1.579 11.879 1.442 9.19 1.018
113 2015-08-2 2460 ppm 2.297 1.619 9.503 1.429 10.532 1.07
114 2015-08-2 2461 ppm 0 1.109 10.1 1.385 9.286 1.002
115 2015-08-2 2462 ppm 0 1.133 10.979 1.436 7.177 1
116 2015-08-2 2463 ppm 1 1 12.166 1.453 7.397 1
117 2015-08-2 2464 ppm 1 1 8.117 1.372 6.522 1
118 2015-08-2 2465 ppm 0 1.413 18.739 1.576 7.616 1
119 2015-08-2 2466 ppm 1.963 1.611 13.419 1.484 8.399 1.01
120 2015-08-2 2467 ppm 2.311 1.628 22.892 1.642 8.75 1.019
121 2015-08-2 2468 ppm 0 1.106 21.224 1.626 4.327 1
122 2015-08-2 2469 ppm 0 1.123 23.47 1.716 6.09 1
123 2015-08-2 2470 ppm 0 1.147 52.365 2.183 3.572 1
124 2015-08-2 2471 ppm 1.753 1.665 21.603 1.653 4.734 1
125 2015-08-2 2472 ppm 1.074 1.654 30.73 1.785 4.422 1
126 2015-08-2 2473 ppm 1.474 1.711 36.957 1.925 5.041 1
2.326 2.788 1 1 2.459 2.095 0 3.194 0 1.098
2.338 2.754 1 1 1.19 1.999 0 3.139 0 1.045
0.615 2.776 1 1 2.341 2.111 0 3.178 0 1.057
2.07 2.727 1 1 2.718 2.062 0 3.147 0 1.062
1.989 2.758 1 1 1.873 2.018 0 3.043 0 1.147
0.389 2.677 1.07 1 0.514 1.953 0 3.084 0 1.011
1.377 2.748 1 1 4.595 2.172 0 3.161 0 1.013
2.15 2.815 1 1 5.978 2.295 0 3.295 0 1.134
2.123 2.791 1 1 3.199 2.129 0 3.344 0 1.057
2.539 2.791 1 1 2.33 2.063 0 3.118 0 1.049
1.461 2.854 1.509 1 2.109 2.103 0 3.173 0 1.126
0.026 2.757 1 1 2.213 2.118 0 3.271 0 1.142
1.873 2.742 1 1 2.804 2.077 0 3.229 0 1.065
2.734 2.852 1 1 1.536 2.063 0 3.329 0 1.174
1.265 2.755 1 1 1.943 2.074 0 3.274 0 1.036
1.597 2.737 1 1 3.926 2.154 0 3.208 1 1
0.026 2.736 1 1 2.021 2.075 0 3.077 0 1.077
1.84 2.691 1 1 2.543 2.034 0 3.053 0 1.037
4.573 2.892 1 1 2.971 2.122 0 3.199 0 1.192
3.122 2.836 1 1 2 2.066 0 3.189 0 1.212
0.572 2.682 1 1 2.656 2.1 0 3.282 0 1.038
1.869 2.813 1 1 2.482 2.13 0 3.458 0 1.133
1.377 2.755 1 1 2.955 2.121 0 3.19 0 1.113
2.935 2.803 1 1 4.665 2.201 0 3.086 0 1.094
5.544 2.977 1 1 1.899 2.128 0 3.513 0 1.182
1.132 2.881 1 1 2.955 2.245 0 3.609 0 1.249
2.567 3.015 1 1 1.454 2.21 0 3.543 0 1.313
1.354 2.811 1 1 2.329 2.156 0 3.401 0 1.245
2.4 2.852 1 1 3.046 2.198 0 3.534 0 1.249
4.321 2.994 1 1 0.793 2.117 0 3.476 0 1.235
0 3.181 -4.741 4.015 0 12.039 14.373 5.143 23.537 15.704
0 3.07 -0.852 3.966 0 11.896 0 5.362 13.052 14.904
0 3.158 -3.463 4.132 0 12.304 0 5.486 0 32.074
0 3.126 -1.309 3.869 0 11.128 0 5.408 8.192 14.65
0 3.089 0.877 3.974 0 11.842 11.827 4.87 0 31.064
0 2.89 -6.146 3.866 0 11.409 19.279 5.204 21.437 15.297
0 3.013 1.306 4.009 0 11.925 0 5.411 9.074 14.831
0 3.257 -4.252 4.019 0 11.961 0 5.569 22.726 15.578
0 3.153 -1.164 4.033 0 12.211 0 5.547 16.961 15.249
0 3.024 0.219 3.97 0 10.967 13.685 4.978 8.329 14.894
0 3.142 0.461 4.09 0 11.785 0 5.588 8.091 15.238
0 3.065 -2.095 4.086 0 11.716 11.785 5.079 13.697 15.597
0 3.02 -1.147 4.019 0 12.304 0 5.388 0 31.751
0 3.169 2.51 4.112 0 12.064 0 5.588 6.612 15.079
0 3.121 -0.359 4.005 0 11.308 0 5.478 10.418 15.122
0 3.06 -2.614 4.025 0 11.626 0 5.403 21.723 15.388
0 3.075 -1.372 4.044 0 12.008 0 5.328 9.827 15.29
0 3.016 -2.353 4.018 0 11.53 0 5.41 31.996 15.341
0 3.071 1.044 4.187 0 11.84 15.539 5.191 21.363 15.64
0 3.177 0.087 4.123 0 11.904 13.563 5.089 18.548 15.472
0 3.086 -2.254 4.059 0 12.092 0 5.38 0 31.456
0 3.288 -0.747 4.229 0 11.937 0 5.488 28.344 15.967
0 3.117 -2.706 4.134 0 11.714 12.989 5.108 28.144 15.877
0 3.018 -5.857 4.066 0 11.744 0 5.577 29.801 15.992
0 3.428 -0.746 4.329 0 12.517 10.65 5.139 0 33.01
0 3.496 0.482 4.373 0 12.914 17.236 5.523 12.757 16.304
0 3.589 -3.856 4.506 0 12.993 0 5.961 32.956 17.53
0 3.227 -0.073 4.481 0 12.156 0 5.652 38.586 16.901
0 3.247 -2.385 4.322 0 12.47 0 5.665 0 32.814
0 3.367 -3.843 4.318 0 12.646 0 6.203 23.453 16.736
 0 9.914 0 19.887 0 66.409 21548.08 173.44 152.307 37.252
0 9.574 0 19.006 0 62.575 19641.42 161.905 120.503 35.261
0 9.834 0 19.979 0 68.367 22438.59 178.162 177.152 38.392
0 9.054 0 18.621 0 64.099 21007.44 167.115 132.648 35.596
0 9.512 0 18.611 0 64.108 21248.37 168.481 116.521 35.04
0 9.147 0 18.745 0 65.924 23372.73 176.399 150.212 36.498
0 9.342 0 19.589 0 65.394 21584.67 169.84 154.864 37.673
0 9.93 0 19.366 0 66.594 21416.85 173.355 150.05 37.606
0 9.742 0 19.761 0 63.115 19137.02 161.23 183.341 38.703
0 9.25 0 18.751 0 66.172 23076.77 176.635 104.556 35.761
0 9.545 0 19.389 0 69.38 23999.85 184.799 159.141 39.094
0 9.652 0 19.393 0 74.096 29453.48 205.057 138.195 40.155
0 9.604 0 18.881 115.031 52.79 16217.49 146.958 120.643 34.633
0 10.074 0 19.773 0 63.172 18518.87 161.092 108.002 35.603
29.562 9.093 0 19.771 0 63.874 18696.02 161.355 105.899 36.409
0 9.666 0 18.975 114.167 62.806 23051.06 177.112 148.677 37.187
0 9.809 0 19.678 111.986 62.326 21924.82 175.539 142.833 37.63
0 9.246 0 18.438 112.79 54.213 17508.8 151.463 135.885 34.593
0 9.691 0 19.973 260.754 66.865 24797.54 185.424 130.794 36.86
0 9.781 0 19.542 128.477 65.646 24829.37 185.171 138.191 37.244
0 9.682 0 19.417 152.465 67.948 26861.22 191.555 144.252 37.564
31.282 9.306 0 19.407 154.072 71.125 28783.81 200.867 92.011 37.261
0 9.594 0 19.34 219.414 64.301 22978.37 178.656 88.999 35.304
0 9.728 0 19.142 158.172 69.278 27419.09 195.273 96.529 36.328
0 10.07 0 20.44 276.333 69.532 25910.66 192.81 94.85 37.063
0 10.113 0 21.051 355.146 82.413 34692.03 229.575 102.424 39.776
0 10.343 0 21.8 108.845 86.502 38317.77 246.373 151.55 42.945
28.716 9.582 0 20.123 319.954 82.708 36337.26 231.559 120.03 39.69
33.412 9.665 0 20.336 88.993 82.477 37372.1 233.02 134.063 40.325
0 10.432 0 21.038 313.199 79.315 31965.49 221.084 131.883 40.582
 0 15.907 2.781 8.5 131.233 9.53 3.548 14.997 3441.995 80.095
2.975 7.917 4.624 8.351 151.528 9.666 2.023 13.103 2612.507 69.828
0 15.844 12.143 8.719 123.413 9.179 -3.649 13.757 2969.483 73.957
11.964 16.283 17.734 8.677 130.24 9.503 0.684 13.451 2642.443 71.79
0 17.02 10.995 8.852 180.918 10.903 6.159 14.957 3456.794 79.709
38.65 17.378 12.049 8.799 161.142 10.438 -5.084 16.16 4454.729 87.928
180.702 10.837 13.111 9.057 168.311 10.524 9.996 15.004 3145.931 79.069
3.466 8.171 27.838 8.984 132.191 9.382 18.115 13.86 2683.317 71.758
179.611 10.277 13.487 9.003 261.802 11.788 13.115 15.036 3626.6 79.713
40.952 8.695 14.342 8.675 159.166 10.287 5.062 13.679 2695.91 72.202
153.725 10.458 13.623 9.132 162.842 10.681 8.796 14.617 2949.176 76.789
284.504 12.575 7.731 9.506 137.629 10.807 1.716 15.913 3345.574 84.375
11.595 16.738 6.801 8.538 264.83 11.816 7.072 11.786 1918.532 61.435
10.702 16.367 2.932 8.237 198.129 10.593 0.702 11.817 1946.448 62.299
146.83 9.799 18.487 8.652 173.256 10.168 18.632 11.891 1655.28 59.834
31.21 8.501 12.595 8.924 153.481 10.239 18.464 13.355 2361.439 68.234
64.859 8.871 6.592 8.623 191.731 11.061 19.413 13.008 2193.64 66.187
20.974 8.024 14.819 8.383 157.757 10.019 3.176 11.39 1712.925 59.538
0 16.391 11.58 9.038 205.958 11.178 0.142 11.012 1294.086 56.413
0 16.668 7.027 8.444 99.295 9.024 9.118 12.084 1686.318 61.464
12.926 17.052 10.407 9.034 170.206 10.704 10.774 12.598 1785.401 63.796
48.505 9.096 23.792 9.264 132.817 10.258 5.201 13.263 2219.103 68.719
0 18.046 13.328 8.294 143.421 10.196 5.594 10.707 1256.473 54.348
0 18.557 9.173 8.721 133.657 10.449 7.727 12.561 1933.88 64.408
0 17.373 14.694 8.231 98.548 9.211 -2.764 8.917 457.983 44.02
0 18.572 15.925 9.554 136.642 10.852 -0.076 10.969 887.965 54.114
0 19.327 14.309 9.71 88.574 10.273 17.756 12.303 915.011 57.603
0 19.176 7.046 9.757 196.242 12.327 6.05 11.312 897.893 54.72
7.765 9.224 14.532 10.392 276.435 14.213 -10.006 11.849 1158.49 60.494
27.839 9.133 7.407 9.174 93.077 10.068 0.521 9.763 365.462 46.407
262.894 44.931 0 64.336 0 30.635 -61.129 10.297 -87.935 21.556
526.771 51.201 0 65.768 0 30.249 -84.261 10.053 -105.669 21.103
449.474 49.38 0 66.578 0 30.031 -69.831 9.796 -113.03 20.365
382.92 49.564 0 69.102 0 29.279 -116.873 9.876 -142.807 20.694
303.99 48.078 0 75.537 0 28.965 -136.611 9.836 -187.349 20.362
350.286 49.901 0 68.626 0 29.108 -143.451 9.744 -180.369 20.309
397.73 49.657 0 64.488 0 30.398 -69.124 10.079 -83.854 21.222
444.004 49.343 0 67.951 0 29.821 -77.198 9.869 -92.08 20.782
511.61 51.476 0 69.972 0 30.688 -46.709 9.99 -66.638 20.981
437.706 51.452 0 66.123 0 28.646 -129.753 9.623 -174.831 19.981
394.728 51.341 0 68.254 0 29.535 -91.249 9.915 -138.487 20.568
327.649 51.686 0 69.952 0 29.523 -129.227 10.011 -187.433 20.651
315.464 45.432 0 66.045 0 30.238 -85.83 10.138 -116.134 21.2
300.424 44.892 0 73.735 0 30.694 -66.047 10.354 -91.621 21.686
315.315 45.017 0 73.452 0 30.199 -70.501 10.098 -110.209 21.023
237.917 45.42 0 79.436 0 29.811 -118.864 9.976 -161.842 20.737
299.56 47.885 0 80.208 0 29.799 -129.002 9.923 -174.367 20.603
339.471 47.014 0 82.831 0 29.201 -132.879 9.772 -187.914 20.197
222.962 43.438 0 66.278 0 30.432 -71.546 10.208 -92.799 21.421
206.411 43.033 0 61.738 0 31.587 -72.872 10.318 -102.36 21.583
230.985 45.004 0 64.252 0 31.205 -76.846 10.352 -112.004 21.592
229.619 45.997 0 73.912 0 29.279 -127.496 9.86 -176.89 20.425
194.67 43.019 0 69.261 0 29.618 -164.814 9.706 -220.81 20.035
181.374 44.982 0 73.015 0 29.396 -163.999 9.947 -227.316 20.457
103.422 39.741 0 69.141 0 32.576 -56.871 10.863 -78.784 22.781
124.161 43.453 0 67.611 0 32.129 -58.895 10.671 -83.857 22.351
46.575 42.262 0 62.642 0 33.721 -47.968 11.092 -65.992 23.303
89.915 43.227 0 67.018 0 31.129 -128.24 10.398 -181.545 21.498
135.954 46.45 0 69.493 0 31.717 -103.642 10.685 -151.738 22.148
97.431 43.146 0 66.439 0 31.928 -108.806 10.393 -168.289 21.42
 2.01 9.54 2.423 11.621 4.381 5.356 0 13.76 0 2.448
0 8.749 0 11.335 2.044 5.252 0 13.578 4.095 2.746
0 8.645 18.276 11.6 3.162 5.222 0 13.486 1.831 2.636
0 8.638 0 10.507 7.077 5.281 0 13.248 4.893 2.735
1.267 9.198 7.989 11.186 14.562 5.404 0 13.061 4.395 2.694
2.665 9.278 6.965 11.196 11.648 5.367 0 13.041 1.951 2.609
0 8.807 5.727 11.64 0 4.641 0 13.703 1.285 2.67
0 8.576 7.946 11.427 4.601 5.243 0 13.427 0 2.124
0 8.835 12.281 11.801 3.201 5.34 0 13.868 0 2.021
3.873 9.126 10.624 11.11 8.868 5.212 0 12.925 1.572 2.554
4.121 9.282 12.657 11.4 7.065 5.256 0 13.308 3.136 2.659
2.75 9.35 13.549 11.457 9.818 5.37 0 13.291 2.806 2.669
0 8.819 16.949 11.741 6.555 5.4 0 13.644 2.528 2.713
0 8.933 11.997 11.798 5.574 5.419 0 13.81 1.666 2.702
1.176 9.447 11.204 11.583 9.216 5.413 0 13.538 3.139 2.713
0 8.748 11.208 11.517 9.263 5.396 0 13.434 3.758 2.726
0 8.718 8 11.463 8.945 5.405 0 13.391 4.635 2.766
0 8.525 13.884 11.287 10.176 5.317 0 13.078 3.492 2.666
0 9.324 15.204 11.747 5.521 5.379 0 13.665 3.865 2.759
0 9.141 13.72 12.152 0 4.747 0 14.22 2.662 2.807
4.866 9.784 2.93 11.868 2.798 5.434 0 14.037 0 2.065
0 8.873 9.605 11.246 8.86 5.279 0 13.094 4.975 2.717
0 8.728 9.764 11.434 8.487 5.379 0 13.307 5.316 2.788
1.571 9.337 7.645 11.351 15.763 5.523 0 13.262 4.917 2.761
4.082 10.206 13.994 12.558 4.953 5.723 0 14.724 1.392 2.85
3.456 10.048 12.015 12.326 2.71 5.584 0 14.427 0 2.475
0 9.749 10.808 12.867 0 5.106 0 15.143 0 2.254
4.011 9.835 10.72 11.973 12.842 5.698 0 13.964 3.678 2.83
0 9.682 12.788 12.163 8.531 5.637 0 14.209 3.348 2.841
11.513 10.055 12.506 12.216 9.752 5.691 0 14.29 3.277 2.852
587996.6 4416.18 1 1 0 1.906 0 1 0 1
582754.2 4431.809 0 1.065 0 1.849 0 1 0 1
576739.5 4502.699 0 1.324 0 1.969 0 1 0 1
594770.4 4643.058 1.308 1.333 0 1.962 0 1 0 1
580125.1 4787.372 1.454 1.341 0 1.87 0 1 0 1
581196.3 4454.764 2.258 1.352 0 1.878 0 1 0 1
588176.9 4310.434 1.549 1.34 0 2.033 0 1 0 1
579364.3 4535.412 1 1 0 2.165 0 1 0 1
574725.9 4520.213 1 1 0 2.019 0 1 0 1
584435.4 4668.453 1.425 1.345 0 1.87 0 1 0 1
578110 4585.383 0 1.282 0 1.997 0 1 0 1
574757.8 4680.03 1.298 1.382 0 2.004 0 1 0 1
567632.8 4613.618 1.314 1.337 0 1.976 0 1 0 1
569752.7 4310.558 1 1 0 1.967 0 1 0 1
570304.8 4482.685 1.159 1.364 0 1.961 0 1 0 1
565079.4 4713.829 1.949 1.36 0 2.028 0 1 0 1
558597.7 4897.864 1.773 1.381 0 1.96 0 1 0 1
554346.9 4759.875 1.453 1.328 0 1.901 0 1 0 1
554884.8 4751.468 1 1 0 2.017 0 1 0 1
557366.1 4662.537 1.1 1.357 0 1.937 0 1 0 1
561445.4 4728.15 1 1 0 1.975 0 1 0 1
542528.6 5046.358 2.112 1.383 0 2.008 0 1 0 1
526219.1 5021.718 3.669 1.405 0 1.995 0 1 0 1
525070.2 4964.795 3.489 1.402 0 2.053 0 1 0 1
538613.4 4897.386 0 1.264 0 2.03 0 1 0 1
537314.1 5016.329 1.001 1.421 0 2.197 0 1 0 1
547326.3 4813.551 1 1 0 2.112 0 1 0 1
525158.1 4954.462 2.862 1.431 0 2.006 0 1 0 1
533045 5296.291 1.139 1.391 0 2.069 0 1 0 1
522772.4 5059.079 1.584 1.436 0 1.97 0 1 0 1
0 1 0 688.75 0 249.131 379198.2 1729.785 83.081 43.384
0 1 720.88 712.866 0 253.638 386459.8 1722.766 86.29 44.402
0 1 0 712.847 0 258.778 389682.8 1755.447 61.181 44.422
0 1 0 702.681 0 252.772 373442.7 1712.976 124.09 45.501
0 1 0 739.14 0 266.474 387222.2 1739.225 17.442 46.465
0 1 0 717.908 0 256.954 382590 1739.227 110.593 45.255
0 1 234.386 710.074 0 253.501 378681.3 1714.733 137.686 44.492
0 1 78.184 722.325 0 259.816 388363.9 1756.31 44.122 44.976
0 1 537.637 742.586 0 267.524 394050.6 1759.936 5.295 44.543
0 1 0 725.406 0 259.835 381234.6 1756.362 34.827 45.863
0 1 0 743.406 0 267.226 386257.9 1763.05 96.222 46.339
0 1 0 728.095 0 257.657 383205 1718.883 125.461 45.52
0 1 0 719.267 0 274.221 407061.8 1848.375 17.309 46.665
0 1 0 695.46 0 259.689 402217.1 1830.159 47.666 44.191
0 1 0 710.098 0 261.758 401439.9 1767.874 126.958 44.858
0 1 0 758.978 0 276.356 401103.4 1813.215 65.188 47.666
0 1 103.216 772.52 0 279.719 408790.9 1790.879 35.278 47.374
0 1 0 770.354 0 289.848 418942.6 1872.904 0 47.397
0 1 0 775.284 0 282.84 410314.8 1798.098 0 45.56
0 1 0 729.092 0 265.504 407709 1807.272 0 42.75
0 1 0 742.95 0 272.88 401130 1743.245 1.929 45.677
0 1 0 806.208 0 288.377 417448.3 1792.108 0 47.298
0 1 0 804.9 0 296.979 441183.6 1832.76 0 48.147
0 1 0 814.934 0 298.973 436625.8 1805.445 85.538 49.805
0 1 0 795.117 0 292.988 426279.2 1895.521 17.638 49.196
0 1 0 805.445 0 289.167 417735 1817.554 98.45 48.75
0 1 0 749.752 0 265.592 404388 1770.554 59.744 44.972
0 1 0 787.621 0 287.721 428203 1842.915 0 46.057
0 1 0 820.705 0 295.992 418828.5 1782.388 11.645 49.25
0 1 0 811.091 0 290.602 435681.8 1906.727 0 46.836
0 3852.664 1.#IO 0
0 3857.573 1.#IO 0
0 3923.825 1.#IO 0
0 4112.444 1.#IO 0
0 4242.21 1.#IO 0
0 3932.478 1.#IO 0
0 3737.103 1.#IO 0
0 3958.831 1.#IO 0
0 3926.27 1.#IO 0
0 4158.352 1.#IO 0
0 4006.696 1.#IO 0
0 4127.284 1.#IO 0
0 4090.378 1.#IO 0
0 3760.961 1.#IO 0
0 3894.417 632.435 0
0 4188.755 1.#IO 0
0 4316.515 1.#IO 0
0 4237.311 1.#IO 0
0 4183.656 1.#IO 0
0 4146.339 1.#IO 0
0 4161.659 1.#IO 0
0 4490.801 920.142 0
0 4453.446 1.#IO 0
0 4391.49 1.#IO 0
0 4359.427 1.#IO 0
0 4441.584 1.#IO 0
0 4225.861 1.#IO 0
0 4426.522 1265.391 0
0 4722.675 1118.526 0
0 4523.818 1.#IO 0
size/gram Silica (gr) Magnetite (gr) Silica (%) Magnetite (%)
125/3 2.7023 0.3011 89.97 10.03
125/2 1.8012 0.2003 89.99 10.01
106/3 2.7031 0.3005 90.00 10.00
106/2 1.8009 0.2009 89.96 10.04
90/3 2.7040 0.3016 89.97 10.03
90/2 1.8027 0.2016 89.94 10.06
75/3 2.7001 0.3008 89.98 10.02
75/2 1.8015 0.2020 89.92 10.08
63/3 2.7015 0.3012 89.97 10.03
63/2 1.8021 0.2020 89.92 10.08