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Sensors and Actuators A 263 (2017) 391–397

Contents lists available at ScienceDirect

Sensors and Actuators A: Physical


journal homepage: www.elsevier.com/locate/sna

Thin-film flexible sensor for omnidirectional strain measurements


Daniel Zymelka a,∗ , Takahiro Yamashita b , Seiichi Takamatsu c , Toshihiro Itoh a,c ,
Takeshi Kobayashi b
a
NMEMS Technology Research Organization, Chiyoda, Tokyo 101-0026, Japan
b
National Institute of Advanced Industrial Science and Technology, Tsukuba, Ibaraki 305-8564, Japan
c
Department of Human and Engineered Environment Studies, The University of Tokyo, Kashiwa, Chiba 277-8561, Japan

a r t i c l e i n f o a b s t r a c t

Article history: Conventional strain sensors are both precise and inexpensive, but can only effectively measure strain
Received 20 September 2016 in one specific direction. In this paper, we report an omnidirectional flexible strain sensor that operates
Received in revised form 21 April 2017 regardless of the orientation of its installation with respect to the direction of the applied strain. The
Accepted 27 May 2017
performance of the developed device was compared to that of conventional foil strain gauges and it was
Available online 8 July 2017
demonstrated that, in contrast to the conventional devices, the omnidirectional strain sensor developed
here shows almost uniform sensitivity at various installation angles.
Keywords:
© 2017 Elsevier B.V. All rights reserved.
Strain measurement
Omnidirectional sensor
Screen printing
Temperature compensation
Printed electronics

1. Introduction in some applications, other applications require omnidirectional


sensing, e.g., crack detection systems, or simply require monitoring
Strain measurement is an important aspect of materials testing. of the maximum strain levels in various types of engineering struc-
These measurements enable the durability of the materials under tures. Inappropriate orientation of these sensors with respect to
analysis to be determined along with detection of potential fail- the applied strain always results in very high measurement errors
ures in the engineering structures under test under the influence of [15,16]. For the latter types of applications, a sensor that enables
various types of mechanical deformations, including stress, torque, uniform detection of cracks or any other mechanical deformations,
pressure, and vibration. Strain sensors are widely used for this pur- regardless of their directions, is required.
pose. The principle of operation of these sensors is based on the Because of the difficulties involved in performing accurate strain
conversion of mechanical forces into a change in an electrical sig- measurements at different sensor orientation angles, this work
nal that can be measured using a dedicated measurement system. has focused on the development of an omnidirectional strain sen-
In terms of the output signals generated, strain sensors can gener- sor. This type of device will enable measurements that are more
ally be divided into electrically resistive [1–5], piezoresistive [6–9], accurate than those of the conventional sensors, regardless of the
capacitive [10–12], and piezoelectric [13,14] types. Among the elec- direction of its installation. To the best of the authors knowledge,
trically resistive sensors, conventional foil sensors are most widely no such sensors have been demonstrated to date. Usually, if omni-
used because of their relatively low cost and good reliability. Note directional sensing is required, rosette-type strain gauges are used.
that in this paper, the term “conventional sensors” is used to refer to However, this requires the use of three individual sensors, and
commercially available uniaxial strain sensors, which are generally thus requires more inputs into the data acquisition system. Here,
made from constantan alloy. in contrast to the rosette strain gauge solution, we demonstrate
One drawback of these conventional sensors is that they can the concept of a single sensor structure that enables omnidirec-
only effectively measure the strain in one specific direction. The tional strain measurements while using only two inputs into the
user must always define the measurement orientation. While it data acquisition system.
is desirable to measure strain selectively in a single direction One of the most challenging steps in strain sensor development
is materials selection, which defines the final characteristics of the
sensor (e.g., strain sensitivity, linearity, the temperature coefficient
∗ Corresponding author. of resistance). Conventional strain sensors are principally made
E-mail address: daniel.zymelka@aist.go.jp (D. Zymelka). of constantan, a copper–nickel alloy, which is etched on a poly-

http://dx.doi.org/10.1016/j.sna.2017.05.040
0924-4247/© 2017 Elsevier B.V. All rights reserved.
392 D. Zymelka et al. / Sensors and Actuators A 263 (2017) 391–397

imide foil. Constantan is commonly used because the fabricated The printed patterns were then cured in a conventional con-
sensors demonstrate sufficient sensitivity and, most importantly, vection oven at 150 ◦ C for 30 min according to the instructions
a low temperature coefficient of resistance, which, if high, could provided by the graphite paste manufacturer. The fabricated omni-
significantly affect the sensor output signal. directional strain sensor is shown in Fig. 3.
In this work, strain sensors were fabricated using the screen After completion of the curing process, the sensors were then
printing method. This method enables a simple and reliable fabri- attached to an object to be tested (in this study, a metal plate)
cation process that is suitable for prototyping of designed devices. using cyanoacrylate adhesive. To ensure the electrical connection of
Because printable constantan inks are not commercially available the sensor to a data acquisition system, thin electrical wires were
at present, alternative sensor materials had to be selected. Accord- attached to the sensor using a silver epoxy conductive adhesive.
ing to previously reported results for the development of printed Finally, the sensors were laminated to protect them from dust and
strain sensors, the most frequently used sensor materials are: moisture using ordinary poly(ethylene terephthalate) (PET) self-
silver [1,2,17–20], graphite [2,4,21,22], carbon nanotubes (CNTs) adhesive laminating sheets. The final electrical resistance of the
[23–26], poly(3,4-ethylenedioxythiophene) polystyrene sulfonate fabricated device was approximately 200 k.
(PEDOT:PSS) [27–29], and their composites [7,30,31]. In this paper,
materials selection was conducted based on the required pro- 2.3. Experimental setup
cessing conditions, printability and the expected properties of the
fabricated sensors. From the materials mentioned above, graphite A 2-mm-thick, 700-mm-long and 120-mm-wide metal plate
paste was selected because it exhibits sufficiently high strain sen- was installed on a rigid support, as shown in Fig. 4. Three printed
sitivity and excellent printability, and requires simple, low-cost sensors and three conventional sensors were attached to the plate
processing. While high sensitivity to temperature variations was close to the support edge. Maximum strain levels were expected
expected of this material [1,2,4,32], graphite paste is suitable for in this location. To evaluate each sensor’s performance depend-
evaluation of the proposed omnidirectional strain sensor concept ing on its direction of installation, the sensors were attached with
at a selected constant temperature. Nevertheless, we will show that three different orientations: 0◦ , 45◦ and 90◦ . Distances between the
despite the use of materials that are characterized by their high support edge and the sensors were 5 cm, measured from their geo-
temperature coefficient of resistance, the developed strain sensors metric centers. The opposing edge of the plate was mounted on a
can be used in practical applications when an appropriate temper- tensile test machine that moved the plate up and down, causing it
ature compensation method is implemented. to bend, and resulting in the generation of various strains that were
measured by the sensors.
The sensors were all individually connected to quarter Wheat-
2. Sensor development
stone bridge circuits (Fig. 5). All the Wheatstone bridges were
connected in parallel to a single 2.5 V power supply. The output
2.1. Design of the sensor
voltage was measured using a 24-bit analog input module (NI-9238,
National Instruments). The data acquisition process was controlled
The shape of the sensor that was developed in this project dif-
using a specifically prepared computer program.
fers from that of conventional strain gauges. In contrast to the
linear structure of conventional sensors, the omnidirectional sen-
3. Sensor evaluation
sor shown in Fig. 1 has a symmetrical design that enables more
uniform sensing at various sensor orientations. Rather than use the
3.1. Sensitivity to applied strain
conventional uniaxial active grid, the new sensor has 16 active ele-
ments (“arms”) that make it sensitive along eight different axes. The
The electrical resistance of the sensors that are attached to the
axes are inclined with respect to one another at an angle of 22.5◦ .
metal plate varies with the degree of axial bending. To determine
The active elements (i.e., the arms or the grid), unlike the terminals
the sensitivity of these sensors, the relative change in resistance
and end loops, are the parts of these sensors that have the greatest
( R
R0
) was measured as a function of mechanical strain (ε). The sen-
effect on their sensitivity, i.e., the electrical resistance change of the
sensor under mechanical deformation. sitivity is then defined using the so-called gauge factor (GF), which
To enable comparison of the developed sensor with a conven- is expressed using the following formula:
tional uniaxial sensor, both devices had the same length or diameter R/R0
of 10 mm. The number of arms used (16) was mainly limited by the GF = (1)
ε
desired sensor geometry. It will be possible to design a sensor with
Because the conventional strain sensors are calibrated and are
more arms within the same sensor diameter if the inner radius can
relatively stable, the conventional sensor that was installed fur-
be enlarged, which would then provide more space to implement
ther along the plate (at an angle of 0◦ ) was used to provide a
additional sensing arms. However, the lengths of these arms would
reference measurement that gives the most accurate strain mea-
have to be shorter. It is important to know that these strain sen-
surement among the six sensors that were attached to the plate.
sors measure an average strain value that corresponds to the area
This sensor was then used to calibrate the developed omnidirec-
covered by the active elements. For this reason, the sensor was
tional sensors. The measured strain values are generally very small,
designed in such a way that the arms all had a maximum possible
and thus the measurements are typically expressed as microstrains
length that lay within the defined sensor diameter.
(strain ×10−6 ).
Based on the output of the reference sensor, a maximum strain
2.2. Fabrication steps of approximately 285 microstrains was generated in the proximity
of sensors during the calibration process. The collected results are
A schematic illustration of the fabrication steps required for the shown in Fig. 6. Within the analyzed strain range, the sensors show
proposed sensor is shown in Fig. 2. First, the thermosetting graphite linear responses with no hysteresis. The average GF of the three
paste (Asahi Chemical Research Laboratory FTU-16R) was screen omnidirectional sensors was calculated to be 3.37 ± 0.08. When the
printed onto a 50 ␮m poly(ethylene naphthalate) (PEN) substrate. GF error is analyzed, it should be noted that the developed sensors
A stainless steel mesh (Asada Mesh HS-D 650/14) was used for this were installed at different orientations. Additionally, in this experi-
high-resolution printing process. ment, the omnidirectional sensor that was set at the angle of 0◦ was
D. Zymelka et al. / Sensors and Actuators A 263 (2017) 391–397 393

Fig. 1. Schematic design of a conventional strain gauge (left) and the design of the proposed omnidirectional sensor (right).

Fig. 2. Schematic illustration of the sensor fabrication process.

Fig. 3. Fabricated omnidirectional strain sensor.

attached to the plate at a distance of 7 mm from the reference sen- if the omnidirectional sensors were calibrated individually using
sor. The omnidirectional sensors that were set at angles of 45◦ and the reference sensors that were installed in their proximity. How-
90◦ were installed at distances of 28 mm and 58 mm from the refer- ever, the calculated sensitivity and measurement error are both
ence sensor, respectively. The GF error could probably be reduced acceptable.
394 D. Zymelka et al. / Sensors and Actuators A 263 (2017) 391–397

Fig. 4. Experimental setup used for analysis of the developed sensors when set at three different installation angles.

1.2x10-3
Tensile
1.0x10-3 Return
Linear fit
8.0x10-4
ΔR/R0

6.0x10-4

4.0x10-4

2.0x10-4

0.0
Fig. 5. Schematic illustration of strain sensor connected to a quarter Wheatstone 0 50 100 150 200 250 300
bridge circuit.
-6
Strain x10
3.2. Evaluation of strain measurement accuracy dependence on
Fig. 6. Calibration curve of omnidirectional strain sensor installed at an angle of 0◦
sensor orientation with respect to the applied strain orientation.

The developed sensors were evaluated in both static and


dynamic strain measurements using the experimental setup that The bending of the metal plate was varied at a constant rate of
was described in Section 2.3. In these experiments, we compared 300 mm/min using the tensile test machine. The collected results
the measured output signals from the groups of conventional and are shown in Fig. 7. These results demonstrate the significant
omnidirectional sensors. dependence of the signals measured by the conventional sensors on
the direction of their installation. The output voltage from the con-
Dynamic strain measurements ventional sensor that was installed at the angle of 45◦ was reduced
For the dynamic strain measurements, five similar bending by about 60% when compared with that from an identical sensor
cycles of up to approximately 285 microstrains were applied. that was installed further along the plate with the main strain orien-
D. Zymelka et al. / Sensors and Actuators A 263 (2017) 391–397 395

Conventional 280
strain sensors 0˚ 45˚ 90˚
240
Omnidirectional
printed sensors 200
1.2x10-3

Strain x10-6
0o 45o 90o 160 Omnidirectional
1.0x10-3 printed sensors
120
8.0x10-4
80
6.0x10-4 Conventional
ΔR/R0

40 strain sensors
-4
4.0x10 0
-4
2.0x10 -40
0.0 0 2 4 6 8 10 12
-4 Time, s
-2.0x10
0 100 200 300 400
Fig. 8. Static strain measurement characteristics when using conventional and
Time, s omnidirectional sensors installed at various angles. The relative change in each
sensors resistance was converted into a strain based on the calibration curve (Fig. 6).
Fig. 7. Relative change in resistance during dynamic strain measurements. Conven-
tional and omnidirectional sensors were installed at three different orientations.
The registered maximum values correspond to an applied strain of approximately Because the conventional sensors are designed to measure
285 × 10−6 that was oriented along the metal plate. strain precisely along a single selected direction, it is obvious that
they will perform better along their grid directions (see Fig. 1).
tation (i.e., at the angle of 0◦ ). Additionally, the conventional sensor However, the results presented here disqualify the use of conven-
that was oriented at an angle of 90◦ produced negative output volt- tional strain sensors from applications in which the orientation of
age values. This phenomenon is ascribed to the Poisson ratio. The the applied strain is unknown. In such cases, the rosette configura-
conventional sensor, when oriented at 90◦ , is much longer in the tion that enables the strain direction to be identified can be used.
direction perpendicular to the applied strain. Because the conven- However, the rosette configuration is composed of three individual
tional sensors exhibit maximum sensitivity in one direction only (in sensors and thus requires at least six inputs into the data acquisi-
this case, perpendicular to the applied strain), the sensor measures tion system. The sensor that is demonstrated in this work enables
the compressive forces related to the Poisson ratio. This explains omnidirectional strain measurements without specifying the strain
the measured negative values. direction, but in contrast to the rosette approach, this sensor only
In contrast to the conventional sensors, the outputs from the requires two inputs into the data acquisition system.
developed omnidirectional sensors are almost the same across the
entire experiment. The registered data confirm the suitability of the 3.3. Temperature sensitivity
proposed omnidirectional sensors for performing dynamic strain
measurements. Graphite is known to be highly sensitive to temperature changes
and has a negative temperature coefficient of resistance. In the sen-
Static strain measurements sor structures in this work, the graphite particles were embedded
The static strain measurements were intended to evaluate and in a thermosetting resin; the temperature dependence of the devel-
compare the accuracy and the measurement precision of the two oped sensors was thus unknown and an analysis of the temperature
types of sensors at a constant strain level. We also provide the calcu- sensitivity was carried out.
lated errors relative to the reference value that was measured using During the experiment, the measurement system that was
the conventional sensor at the angle of 0◦ when the other sensors described above was used. The sensors to be analyzed were
were installed at different angles. In contrast to the previous mea- attached to a short metal plate and were located inside an envi-
surement results (Fig. 7), the output voltages were converted into ronmental test chamber (Espec SH-221). The relative change in
strain values based on the calibration curve (Fig. 6). resistance was then measured as a function of measured temper-
During this experiment, the metal plate was bent and held in ature. The experiment was performed over the temperature range
position for a few seconds. According to output of the reference from −10 ◦ C to 40 ◦ C, where the temperature was increased at a
sensor, the applied strain was approximately 223 microstrains. The constant rate of 2 ◦ C per min.
collected results are shown in Fig. 8. Between the 3rd and the 8th The results shown in Fig. 9 indicate that the developed sensor
seconds of the measurement period, the average strain values and made from the graphite paste is extremely sensitive to temper-
the corresponding standard deviation values were calculated for ature change when it is connected to the quarter Wheatstone
each individual sensor. The results are given in Table 1. bridge circuit (Fig. 5). This electrical circuit limits the use of
On the basis of these calculated standard deviations, we see that the graphite-based sensors to measurements at a constant tem-
the conventional sensors offer slightly better precision of measured perature. However, we show that this high sensitivity to the
output signal than the omnidirectional sensors that were made temperature change can be reduced if an appropriate temperature
from graphite paste. However, when the measured strain values compensation scheme is implemented, e.g., the full Wheatstone
are analyzed with respect to the reference sensor, the omnidirec- bridge circuit shown in Fig. 10. In this configuration, four omni-
tional sensors show much greater accuracy. The measured strain directional sensors were placed inside the environmental test
values from the conventional sensors oriented at 45◦ and 90◦ were chamber. One of the sensors was considered to be the active
reduced by approximately 60% and 120%, respectively. In contrast, element (strain sensor) and the other three were only used to com-
in the case of the omnidirectional sensors, the measured values pensate for the effects of the temperature change.
were more uniform and the errors in the values measured using The collected results show that when the full Wheatstone
the reference sensor were significantly lower. bridge circuit is implemented, the temperature sensitivity of these
396 D. Zymelka et al. / Sensors and Actuators A 263 (2017) 391–397

Table 1
Results of static strain measurements performed using conventional and omnidirectional strain sensors that were installed at various angles with respect to the reference
sensor orientation. Calculations were performed using data that were registered between the 3rd and 8th seconds of the experimental characteristics shown in Fig. 8.

Sensor type Conventional Omnidirectional


Orientation 0◦ (ref. sensor) 45◦ 90◦ 0◦ 45◦ 90◦
Average strain and 222.8 ± 0.9 89.3 ± 0.8 −44.9 ± 0.6 223.1 ± 2.0 206.9 ± 2.6 214.2 ± 2.5
standard deviation (×10−6 )
Percentage error from – 59.9% 120.1% 0.1% 7.1% 3.9%
strain measured by the
reference sensor

1.0x10-1 that in the case of an unknown strain orientation, the devel-


Graphite paste (quarter W. bridge) oped device enables much more accurate measurements of both
Graphite paste (full W. bridge)
8.0x10-2 dynamic and static strain than the conventional linear sensors.
Despite the high sensitivity of the sensor material to temperature
6.0x10-2 change, this effect can be reduced by implementing the sensors
ΔR/R0

using the full Wheatstone bridge circuit. These results demon-


strate the potential of screen-printed graphite pastes for use in
8.0x10-4
cost-effective fabrication of these strain sensors.
6.0x10-4 While the sensor demonstrated in this work was made from a
4.0x10-4 screen-printed graphite-based paste, the same device can be fab-
ricated using various other materials and methods. When other
2.0x10-4
materials that show low temperature coefficients of resistance are
0.0 used, the performances of the resulting sensors may be even better
-10 0 10 20 30 40 than those demonstrated here.
o The developed sensor can be used in a diverse array of appli-
Temperature, C
cations, and particularly in applications where prediction of the
Fig. 9. Resistance–temperature relationships of printed graphite-based omni-
correct sensor installation direction is difficult, e.g., in crack detec-
directional sensors when connected in quarter- and full-Wheatstone-bridge tion systems or in the monitoring of maximum strain levels in
configurations. different types of engineering structures. Additionally, an arrange-
ment of these omnidirectional sensors in the form of an array
may enable more accurate strain distribution measurements. Such
devices would be particularly helpful in large-area health monitor-
ing of civil structures, such as bridges, tunnels and buildings.
Future research will be oriented towards detailed optimization
of the sensor structure, i.e., in terms of the number and length of
the active elements required with respect to the sensor diameter.

Acknowledgments

This work was conducted within the framework of the “Road


Infrastructure Monitoring Systems” (RIMS) project of the New
Energy and Industrial Technology Development Organization
(NEDO).

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Futaba, K. Hata, A stretchable carbon nanotube strain sensor for University of Tokyo in 1988, 1990, and 1994, respectively. He was an associate pro-
human-motion detection, Nat. Nanotechnol. 6 (5) (2011) 296–301. fessor at the Research Center for Advanced Science and Technology (RCAST) at the
[24] B. Thompson, H.S. Yoon, Aerosol printed carbon nanotube strain sensor, Proc. University of Tokyo from 1999 to 2007. He established a network MEMS group in
SPIE 8346 (2012) 83461C. AIST in 2007 and joined the BEANS project as the leader of the Macro BEANS Center
[25] T. Yamada, Y. Yamamoto, Y. Hayamizu, A. Sekiguchi, H. Tanaka, K. Kobashi, in 2008. After working as the deputy director of the Research Center for UMEMSME,
D.N. Futaba, K. Hata, Torsion-sensing material from aligned carbon nanotubes AIST, he became a professor at the University of Tokyo in 2015. His research inter-
wound onto a rod demonstrating wide dynamic range, ACS Nano 7 (4) (2013) ests are in MEMS technologies for wireless sensor network nodes and large-area
3177–3182. (macro) devices.
[26] F. Michelis, L. Bodelot, Y. Bonnassieux, B. Lebental, Highly reproducible,
hysteresis-free, flexible strain sensors by inkjet printing of carbon nanotubes, Takeshi Kobayashi received his B.S. and M.S. in materials science from the Univer-
Carbon 95 (2015) 1020–1026. sity of Tokyo, and he received his Ph.D. in the same field from the same university in
[27] V. Correia, C. Caparros, C. Casellas, L. Francesch, J.G. Rocha, S. 2002. He then worked as a researcher at the National Institute of Advanced Indus-
Lanceros-Mendez, Development of inkjet printed strain sensors, Smart Mater. trial Science and Technology (AIST). He is currently the leader of one of the research
Struct. 22 (10) (2013) 1–10. teams at UMEMSME. His research interests include piezoelectric MEMS devices and
their application to wireless sensor networks.

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