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Laboratory Manual
September 2004
TABLE OF CONTENTS
1. INTRODUCTION............................................................................................................... 1
7 APPENDIX ......................................................................................................................... 17
Sample Title Page ................................................................................................................ A1
Sample Data Table .............................................................................................................. A2
Sample Data Plot ................................................................................................................ A3
Sample Format for Field Notes ..........................................................................................A4
Checklist for Report Submission .......................................................................................A5
ii
1. INTRODUCTION
This manual provides the student with a detailed description of what is required for a
laboratory report for ME3415, ME3423, ME3435, ME3515, ME3522, and ME5463. It includes a
format for the entire report as well as detailed instructions on the preparation of figures and tables,
and a discussion of errors and laboratory practice. Reports which do not conform to these
guidelines will not be accepted. Help in the preparation of a formal written report may be found in
the Department of Mechanical Engineering Document "Guidelines for a Comprehensive Written
Report" or in "How to Write and Publish a Scientific Document" by Robert A. Day.
1
(vi) a statement of the conclusions and any recommendations resulting from the study,
(vii) a list of references in proper form,
(viii) appendices as required.
4. The report should have a cover sheet (an example is provided in the appendix) and pages
should be numbered.
5. Voluminous raw data (more than 2 pages) should be placed in an appendix but reference
must be made to the appendix in the text.
6. All symbols should be defined; units should be clearly indicated.
In addition to the above, a table of contents may be desirable. A letter of transmittal may also be
A Letter Report conveys the results of the experiment in an informal but concise manner
between two individuals who are familiar with the context of the work. It is at least 2 pages long
(not including enclosures) and written in business letter form with 1½ spacing. It explains the
assignment being reported upon, describes generally how it was carried out and presents the final
results with emphasis on their significance and conclusions or recommendations resulting from them.
· The Letter Report should be on 8 ½” x 11" white bond paper giving the author’s name,
group, address and date on the front page.
· The Letter Report must be signed.
· The first paragraph of the Letter Report serves as a letter of transmittal.
· The report should be carefully organized, this being reflected through the paragraphing and
perhaps through the use of side headings.
· Tables or plots of final results may be attached as enclosures or attachments. If so these must
be referred to in the text of the letter.
· While organization and form is a matter of personal taste, the following points should be
covered:
2
· the objective
· list, sketch and accuracies of the apparatus used (in an appendix)
· brief procedure (possibly in an appendix)
· a brief description of the method of calculation of the results (including assumptions
and reference to sample calculations)
· tables of required final results and required graphs (the raw data should be in an
appendix)
· a complete set of ORIGINAL sample calculations done by hand (no photocopies)
· a discussion of the results, error analysis, sources of error and any other information
requested in the lab handout
· a brief statement of the conclusions and recommendations drawn from the lab
Things to not put in your letter report:
· abstract
· discussion of relevant theory
· derivation of equations
· distinct section headings such as Results, Conclusions, etc.
3
7. Tables should read across the top of the page; if column requirements necessitate having the
table read across the side of the page, the top of the table should be the left side of the page.
1. Each figure should have a proper descriptive title and should be numbered if there is more
than one. The title should not merely repeat the co-ordinate labels.
2. The abscissa (x-axis) and ordinate (y-axis) of each figure should be properly labelled with
the scale of the graph and the variables names.
3. Units should be clearly shown.
4. Scales for each co-ordinate axis should be carefully chosen for good display of the data.
5. Data points should be marked clearly, and lines should be clear and bold. Figures should
be kept simple - not more than two or three curves on each.
6. If there is more than one graph on a figure, data points and curves should be carefully
identified. For example, , ∆, , ∇, may be used for four different lines.
4
7. Elaborate drafting is not important, but neatness and good appearance are very important.
All curves should be drawn in fine, smooth lines, with the use of a straight edge or french
curve if done manually.
8. Lettering on each figure should be of a generous size - at least twice that of normal type.
Ample margins should be allowed. This may mean that the axes have to be drawn inside the
printed margin of the graph paper.
9. Each figure must be referred to and explained in the text of the report.
10. Use quality graph paper with 1 cm squares.
These standards must be met whether the graph is drawn manually or using a computer and printer.
Although, the appearance of computer generated plots can be substantially improved by printing
them directly on graph paper, few computer graphics packages are adequate for the task.
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diagrams, it is customary to plot the independent variables as ordinates. The scales
should be chosen so that the entire range of the data to be represented can be shown
within the limits of the graph and so that each division on the co-ordinate paper
represents 1, 2, or 5 units, or some power of ten multiplied by 1, 2, or 5.
STEP 3. Mark the unit values along the axes. All numbering should be clear and distinct and
readable from the bottom, not from the side. If decimal fractions are shown, a zero
should precede the decimal point, thus: 0.10 or 0.050.
STEP 4. Plot the points representing the data. Show the points by dots and enclose each dot
with a small circle, triangle, or square, etc. If more than three curves are shown on
the same chart, additional symbols should be used; for example, crosses, double
circles, etc.
STEP 5. Draw the curves. Draw a smooth curve through the plotted points. If the points vary
significantly from such a curve, connect them by a broken line and then draw the
required curve to intersect the broken line so that the sum of the areas of the triangles
formed by the broken line on one side of the curve is approximately equal to the sum
of the areas of the triangles formed on the other side of the curve. Note that these
broken lines are only construction lines. Alternatively a line or curve may be
statistically fitted to the data (see Section 4.3).
STEP 6. Letter the chart. The axes and the curves should be lettered so that their use and
meaning are clear to the reader. When the curves of the chart fall close together, it is
best to differentiate between the curves by means of leaders. (Note that labelling
each curve is preferable to using a legend).
STEP 7. Prepare the title. The title should be displayed prominently, near the top or bottom of
the chart, depending on available space. The title should not repeat information
which is already provided on the axes; this is redundant. The title should give other
pertinent information about the nature of the subject represented.
The name of the student, date, and other relevant data should be placed in the lower
right hand corner of the graph.
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4.3 Correlating Data
There often may be a theory available to which experimental data are expected to conform.
This may be described by an equation in which the dependent variable, y, is a function of an
independent variable, x, in the experiment.
y = f(x)
In some cases the equation can be rewritten or manipulated algebraically so that it becomes the
equation of a straight line, and if possible this should be done.
The equation of a straight line is
y = a + bx
If y is the ordinate and x is the abscissa on a graph, a straight line results whose slope is b and whose
intercept on the y axis (that is, where x = 0) is a.
For example, in thermodynamics, an equation of the form
1
log10 P = a + b
T
is used to correlate the vapour pressure of a pure substance against temperature. If log10 P is plotted
on the ordinate and 1/T is plotted on the abscissa, vapour pressure data are expected to fall on a
straight line. This is a semi-logarithmic plot.
In fluid mechanics for non-newtonian fluids which obey the "power law", the rate of strain,
du/dy, is related to the shear stress, τ, by
τ = K (du/dy )n
Taking the logarithms of both sides we find
log10τ = log10 K + n log10 (du/dy)
If log10τ is plotted on the ordinate and log10 (du/dy) is plotted on the abscissa, a straight line with
slope n is expected to result. This is a logarithmic plot.
Plotting experimental vapour pressure data or shear stress data on the appropriate axis
permits an immediate judgement to be made whether the data points fall on a straight line and, then,
whether there appears to be serious experimental errors in any of the data. Furthermore, having
7
determined the best straight line to put through the data points it is possible to calculate a and b in a
vapour pressure correlation or K and n for a power law fluid. This fact allows a considerable
reduction in the space required to report your results since the tabular and graphical data can now be
represented by a single equation.
The slope and intercept of a straight line fit may be determined from the graph by fitting a
line as described in the previous section. However, this may be made more objective by employing
the statistical method of linear regression. Many electronic calculators and computer graphics
packages have this routine. The basis of the method is that it minimizes the sum of the square of the
difference between the data for the dependent variable and its mathematical representation. This
approach has some basis in measurement theory but in practice it is popular because it provides an
objective procedure for fitting curves to the data. The use of this method should be limited to straight
lines and low order polynomials. More complex curves should be fit manually because statistical fits
of high order polynomials are almost always unrealistic. When quoting an equation fit by statistical
regression include the root mean square error.
5.2 Errors
Systematic errors are caused by the instrumentation and method of experimentation. These
errors invariably arise because the conditions of the experiment do not match the theoretical design
of the experiment. Repeated measurements do not show their presence. They can only be revealed by
8
comparing the results from different experimental methods. The elimination of systematic errors
often requires considerable physical insight.
Accidental errors are usually due to the observer and can be revealed by repeated
measurements. Examples of errors of this type are many, perhaps the most obvious being, reading
the magnitude of the measurement incorrectly, incorrectly recording the measurement value, or
making a measurement when the experimental equipment is not at the desired conditions.
The precision of a measurement process is determined by the degree of mutual agreement
between independent measurements of a single quantity performed several times under controlled
conditions. It is therefore a measure of only the accidental errors.
For example, consider the measurement of the length of a nominal three centimetre long
metal cube using a ruler with least graduation of 1 mm. Suppose all the measurements are to be
made at 20°C with the same ruler. On seven different occasions the following results are obtained.
3.05, 3.03, 3.01, 2.99, 3.12, 3.00, 3.04 cm at 20°C
Since the ruler is graduated in 10ths, the second place of decimals is estimated and will have
some error of estimation which could be systematic or accidental in nature. As well, on looking over
the values recorded, it is noted that a value of 3.12 appears once, with the bulk of the measurements
having values much less than this. It could be suspected that this value is the result of an accidental
measurement, and as such should be discarded since the resolution of the measurement tool is 0.1 cm
and our own resolution is estimated to be 0.01 cm with some possible error.
The mean value m, of our measurement is thus
1 n 1
m= ∑
n i=1
mi = (3.05 + 3.03 + 3.01 + 2.99 + 3.00 + 3.04)
6
= 3.02 cm at 20°C,
and the maximum spread of the measurements may be stated as ± 0.03 cm or on a percentage basis
as
0.03 x 100
± = + - 1%
3.0
Thus the length may be stated as L and the maximum spread;
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L = 3.02 ± 0.03 cm or 3.02 cm ± 1%
A more widely used indicator of the measurement precision is the RMS error, σ, defined as
1/2
1 n
σ = ∑ d 2s
n1 s=1
where d1, d2, ... are the deviations from the mean of the data sample. The factor (n-1) in the
denominator arises because of the uncertainty of m̄ which is derived from the finite sample. If the
measurement errors are normally distributed the 67% of all measurements will lie within ±σ of the
mean value.
For the example;
1/2
1
σ = ((+0.03 )2 + (0.01 )2 + (-0.01 )2 + (-0.03 )2 + (-0.02 )2 + (+0.02 )2 )
5
1/2
1
σ = (0.009 + 0.0001 + 0.0001 + 0.009 + 0.0004 + 0.0004)
5
1/2
0.0028
σ= = 0.024
5
Hence, L = 3.02 ± 0.02 cm. Giving a precision of .02 cm.
In the preceding example we assumed that the ruler used was accurate, that is that the cm and
mm graduations were true. If this were not the case, the measurements above would systematically
deviate from the true value. The fact that a measurement is precise does not necessarily mean it is
accurate (i.e. approaches the true value) although for accurate results precise measurements must be
available.
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z = f (x, y)
where z is the derived quantity and x and y are directly measured to an accuracy of ±δx and ±δy.
Assuming that δx and δy are relatively small, for example,
δx δy
, < 10%
x y
The error, δz, corresponding to a give δx and δy is
∂f ∂f
δz = (x, y) δx + (x, y) δy .
∂x ∂y
This depends on the values of x and y, and not just δx and δy. It could be then the errors produced
by δx and δy exactly cancel giving δz=0; but this should not be expected. The largest δz results
when the errors produced by δx and δy are additive. However, assuming δx and δy are independent
and normally distributed, the most likely range of δz is then calculated as the RMS error.
2 2
∂f ∂f
δz = ± ∂x + ∂y
∂x ∂y
In principle δz should be calculated over the full range of the measured values. In practice it is often
sufficient to choose two or three points indicating the maximum and minimum errors.
Consider the example of the steel cube in the previous section. The volume of the cube can
estimated by the product of the lengths of the three sides
V = abc
But as shown, the "true" length of the three sides is unknown and only an approximation can be
made. Given the errors described previously for the measurement of the three sides, the error in the
volume estimate would be
∂V ∂V ∂V
δV = δa + δb + δc = (bc)δa + (ac)δb + (ab)δc
∂a ∂b ∂c
Substitution of the numerical values (assuming all errors are additive) gives
11
The estimated value of V is therefore (3.02)3=27.5 ± .8 cm3
Now, consider a more complicated example. The surface tension of a liquid may be estimated
from its rise in a capillary tube using the formula
γrh
σ=
2 cos θ
where θ is the wetting angle
r is the radius of the tube
γ is the specific weight of the liquid
h is the rise height of the column
Given errors δθ, δr, δγ and δh the error in estimating σ from this formula is
2 2 2 2
rh γh γr γrh(- sin θ )
δσ = ± δγ + δr + δh + δθ
2 cos θ 2 cos θ 2 cos θ 2 cos θ
2
or in relative terms
2 2 2
δσ δγ δr δh
=± + + + (- tan θ δθ )2
σ γ r h
γrh
This last expression was achieved by dividing the left side by σ and the right side by . The
2 cos θ
maximum absolute error occurs when all contributions are either positive or negative. Notice the
insensitivity of δσ/σ to δθ when θ ~ 0°, and the sensitivity where θ ~ 90°.
12
The typical pocket calculator has more precision than could ever practically be used in
engineering calculations. While this is good for intermediate calculations, the final result should
only be reported to the number of significant figures which is justified by the precision of the data.
6. LABORATORY PRACTICE
6.1 Precautions to be Observed in the Laboratory
Carelessness in personal conduct or in handling equipment may result in serious injury to the
individual or the equipment. Do not run near moving machinery. Always be on the alert for strange
sounds and find the cause of them. Guard against entangling clothes in moving parts of machinery.
No piece of equipment should be started or stopped except under the direct supervision of the
instructors or upon specific instructions from them. Do not open or close any valve, switch, etc.
13
without first learning its function and trying to determine what will happen when the operation is
completed.
In particular observe the following:
1. Open and close all valves (water, steam, air, ammonia) slowly.
2. While a piece of equipment is "warming up", see that proper lubrication is obtained, and that
all gauges are reading normally.
3. Apply and remove loads slowly and uniformly.
4. When starting a steam-driven prime mover fitted with a condenser, see that the condenser is
supplied with cooling water before steam is admitted to the prime mover.
5. Leave instruments and equipment in a clean and orderly condition upon completion of the
experiment.
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(b) a brief but complete description of the equipment or apparatus used and the
procedure followed,
(c) a schematic diagram of the equipment and connections (with dimensions) drawn
freehand, but neatly,
(d) a tabulation of the raw data to serve as checks on its consistency (see item 6),
(e) an outline of the method of treatment of the raw data with sample calculations,
(f) a tabulation of the results derived from the raw data,
(g) suitable plot(s) of the results (see item 6), and
(h) a statement of the conclusions that may be drawn of the work completed.
5. The record should be permanent.
6. Where desirable for any reason, as for the inclusion of plots, and recorded data sheets, the
record for an assignment may include separate sheets permanently attached in the bound
book by rubber cement or scotch tape. These should be attached to blank pages of the
notebook and should carry the number of those pages.
7. The written text should be in the form of terse but complete and understandable notes.
8. The record should not be untidy; but, time should not be wasted to make it elegant.
Emphasis should be on completeness rather than formality.
9. Ideally the notebook record for an assignment should be completed during the laboratory
period. In no case should completion of the record be delayed beyond the day following.
10. The notebook record for an assignment should be submitted to the instructors for grading as
they request.
An example of field note arrangement is shown at the end of the report.
15
APPENDIX
16
University of New Brunswick
Department of Mechanical Engineering
ME____ ___________________
Author:
Title:
Date:
Group:
*
Abstract / 5
Introduction and Theory / 20
Apparatus and Procedure / 10
Results / 20
Discussion / 20
Conclusions / 5
Field Notes / 20
/100
Marked By:
A1
A2
0.0 1648 1.0 6.5 1.90 0.0000 0.0 7.5 0.54 93 0 0.00
6.8 1653 2.0 1.6 6.90 0.0030 3.0 5.0 1.34 232 147 0.64
7.9 1648 2.0 0.5 7.10 0.0032 3.2 4.2 1.37 236 131 0.56
0.7 1649 1.1 6.4 3.40 0.00092 0.9 7.6 0.78 134 69 0.52
0.4 1651 1.1 6.6 3.00 0.00073 0.7 7.8 0.71 123 55 0.45
0.2 1651 1.0 6.5 2.60 0.00054 0.5 7.5 0.65 112 40 0.35
2.1 1652 1.3 5.5 5.04 0.0017 1.7 7.2 1.04 180 118 0.66
0.0 0 1.0 1.0 -1.42 0.0000 0.0 2.0 0.00 0 0
0.7
10
0.6
8
0.5
6 0.4
A3
4
BP (kW), WP (kW), Eff.
0.2
2
0.1
0 0
0 0.5 1 1.5 2 2.5 3
Q (l/s)
Figure 1: Performance of Pump #2 operating at 1800 RPM. Symbols are as follows: ● efficiency, ♦ head,■ brake power, ▲
water power.
SUGGESTIONS FOR SETTING UP FIELD NOTES
OBSERVER: ________________
TEST
NO. 1
A4
Before submitting your report for grading please check that it is complete by
using this form as a guide. Attach the completed form at the end of your report.
A5